4-IODO-2-PYRIDONE
- Product Name
- 4-IODO-2-PYRIDONE
- CAS No.
- 858839-90-4
- Chemical Name
- 4-IODO-2-PYRIDONE
- Synonyms
- 4-IODO-2-PYRIDONE;4-Iodo-2-pyridinone;4-Iodopyridin-2(1H);4-Iodo-2(1H)-pyridinone;4-iodo-2-pyridone , 97+%;4-Iodo-2-hydroxypyridine;2-Hydroxy-4-iodopyridine;2(1H)-Pyridinone, 4-iodo-;4-iodo-1,2-dihydropyridin-2-one
- CBNumber
- CB01486870
- Molecular Formula
- C5H4INO
- Formula Weight
- 221
- MOL File
- 858839-90-4.mol
4-IODO-2-PYRIDONE Property
- Melting point:
- 186-188°C
- Boiling point:
- 321.6±35.0 °C(Predicted)
- Density
- 2.12±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- pka
- 10.76±0.10(Predicted)
- color
- Pale brown
- CAS DataBase Reference
- 858839-90-4
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- I737683
- Product name
- 4-Iodopyridin-2(1H)-one
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- I737683
- Product name
- 4-Iodopyridin-2(1H)-one
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 4H17-H-01
- Product name
- 4-Iodo-1H-pyridin-2-one
- Purity
- 97%
- Packaging
- 1g
- Price
- $314
- Updated
- 2021/12/16
- Product number
- 077035
- Product name
- 4-Iodo-1,2-dihydropyridin-2-one
- Purity
- 95%
- Packaging
- 500mg
- Price
- $262
- Updated
- 2021/12/16
- Product number
- OR12279
- Product name
- 4-Iodo-1H-pyridin-2-one
- Purity
- 97%
- Packaging
- 1g
- Price
- $285
- Updated
- 2021/12/16
4-IODO-2-PYRIDONE Chemical Properties,Usage,Production
Synthesis
153034-86-7
858839-90-4
GENERAL METHOD: 2-chloro-4-iodopyridine (prepared above) was heated with sodium acetate (2.0 eq.) in 1.0 M acetic acid solution at 150°C for 72 hours in a sealed tube. After completion of the reaction, the mixture was cooled to room temperature and concentrated under reduced pressure. The residue was partitioned between ethyl acetate (3 mL/mmol) and cold water (3 mL/mmol). The aqueous layer was extracted with ethyl acetate (3 mL/mmol; 4 times). The combined organic layers were washed sequentially with saturated NaHCO3 solution (1 mL/mmol), brine, dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure. The crude product was purified by silica gel fast column chromatography to afford 4-iodo-2-pyridinone (1b/c/d), details of the specific compound are given below.
References
[1] Synlett, 2016, vol. 27, # 1, p. 67 - 69
[2] Patent: US2010/331320, 2010, A1. Location in patent: Page/Page column 89; 90
[3] Patent: WO2015/101928, 2015, A1. Location in patent: Page/Page column 48
[4] Patent: WO2012/32014, 2012, A1. Location in patent: Page/Page column 94
[5] Patent: US2012/214782, 2012, A1. Location in patent: Page/Page column 40
4-IODO-2-PYRIDONE Preparation Products And Raw materials
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View Lastest Price from 4-IODO-2-PYRIDONE manufacturers
- Product
- 4-IODO-2-PYRIDONE 858839-90-4
- Price
- US $5.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12