2-(2-BROMOETHOXY)PROPANE

Product Name: 2-(2-BROMOETHOXY)PROPANE
CAS No.: 54149-16-5
Chemical Name: 2-(2-BROMOETHOXY)PROPANE
Synonyms: Propane, 2-(2-bromoethoxy)-
CBNumber: CB01489811
Molecular Formula: C5H11BrO
Formula Weight: 167.04
MOL File: 54149-16-5.mol

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2-(2-BROMOETHOXY)PROPANE Property

Boiling point:: 139.9-140.2 °C(Press: 743 Torr)
Density: 1.2609 g/cm3
storage temp.: 2-8°C
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2909199090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B686683
Product name: 2-(2-Bromoethoxy)propane
Packaging: 1g
Price: $360
Updated: 2021/12/16

Apolloscientific

Product number: OR965620
Product name: 2-(2-Bromoethoxy)propane
Purity: 97%
Packaging: 1g
Price: $363
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0016608
Product name: 2-(2-BROMOETHOXY)PROPANE
Purity: 95.00%
Packaging: 1G
Price: $983.52
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0016608
Product name: 2-(2-BROMOETHOXY)PROPANE
Purity: 95.00%
Packaging: 2.5G
Price: $1473.14
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0016608
Product name: 2-(2-BROMOETHOXY)PROPANE
Purity: 95.00%
Packaging: 5G
Price: $1928.08
Updated: 2021/12/16

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2-(2-BROMOETHOXY)PROPANE Chemical Properties,Usage,Production

Synthesis

109-59-1

54149-16-5

General procedure for the synthesis of isopropyl-2-bromoethyl ether from isopropoxyethanol: 2-isopropoxyethanol (2 mL, 17.34 mmol) was added to a 2-necked flask equipped with a reflux condenser, a magnetic stirring bar and a septum. Phosphorus tribromide (0.52 mL, 5.45 mmol) was added slowly dropwise via syringe. The temperature increased and slight reflux occurred during the reaction. The reaction mixture was stirred under argon protection at room temperature for 24 hours. Upon completion of the reaction, the reaction was quenched with water and extracted with hexane. The organic layers were combined, dried over anhydrous magnesium sulfate and subsequently concentrated to afford 1 g (34% yield) of the target product, isopropyl-2-bromoethyl ether, as a colorless oil. The product was characterized by 1H NMR (CDCl3): δ 3.78 (t, 2H); 3.61 (m, 1H); 3.42 (t, 2H); 1.18 (d, 6H).

References

[1] Patent: US2007/219212, 2007, A1. Location in patent: Page/Page column 21
[2] Journal of the American Chemical Society, 1934, vol. 56, p. 127
[3] Zeitschrift fuer Physikalische Chemie, Abteilung A: Chemische Thermodynamik, Kinetik, Elektrochemie, Eigenschaftslehre, 1940, vol. 185, p. 91
[4] Chemistry - A European Journal, 2017, vol. 23, # 5, p. 1007 - 1012

2-(2-BROMOETHOXY)PROPANE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(2-BROMOETHOXY)PROPANE Suppliers

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54149-16-5, 2-(2-BROMOETHOXY)PROPANERelated Search:

Isopropylmalonic acid Potassium isopropenyltrifluoroborate L-Serine, 1-methylethyl ester, hydrochloride 2-(AMMONIOOXY)PROPANE CHLORIDE IPTG tert-Butyl 2-bromo-2-methylpropanoate 2-BROMOPROPIONIC ACID TERT-BUTYL ESTER TERT-BUTYL 2-BROMOBUTYRATE tert-Butyl bromoacetate 5,5-DIBROMOMELDRUM'S ACID Isopropyl 2-bromo-2-methylpropanoate Isopropyl bromoacetate ALPHA-BROMO-GAMMA-VALEROLACTONE (S)-2,2-DIMETHYL-4-BROMOMETHYL-1,3-DIOXANE 5-BROMO-2.2.5-TRIMETHYL-1.3-DIOXANE-4.6-DIONE TERT-BUTYL 2,4-DIBROMOBUTYRATE 3-(BROMOMETHYL)-2,4, 10-TRIOXAADAMANTANE T-BUTYL BROMOACETATE, [1,2-14C]

Propane, 2-(2-bromoethoxy)-

54149-16-5