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methyl (4-formylphenoxy)acetate

Product Name
methyl (4-formylphenoxy)acetate
CAS No.
73620-18-5
Chemical Name
methyl (4-formylphenoxy)acetate
Synonyms
Methyl 2-(4-formylphenoxy);methyl (4-formylphenoxy)acetate;Methyl 2-(4-forMylphenoxy)acetate;methyl 2-(4-methanoylphenoxy)ethanoate;2-(4-formylphenoxy)acetic acid methyl ester;acetic acid, (4-formylphenoxy)-, methyl ester;Acetic acid, 2-(4-formylphenoxy)-, methyl ester
CBNumber
CB01518731
Molecular Formula
C10H10O4
Formula Weight
194.18
MOL File
73620-18-5.mol
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methyl (4-formylphenoxy)acetate Property

Melting point:
40-42 °C
Boiling point:
315.2±17.0 °C(Predicted)
Density 
1.201±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
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Safety

HazardClass 
IRRITANT
HS Code 
2918999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M321383
Product name
Methyl2-(4-Formylphenoxy)acetate
Packaging
100mg
Price
$75
Updated
2021/12/16
AK Scientific
Product number
W8169
Product name
Methyl(4-formylphenoxy)acetate
Packaging
1g
Price
$62
Updated
2021/12/16
Apolloscientific
Product number
OR907093
Product name
Methyl(4-formylphenoxy)acetate
Purity
95%
Packaging
1g
Price
$160
Updated
2021/12/16
AK Scientific
Product number
W8169
Product name
Methyl(4-formylphenoxy)acetate
Packaging
5g
Price
$185
Updated
2021/12/16
Apolloscientific
Product number
OR907093
Product name
Methyl(4-formylphenoxy)acetate
Purity
95%
Packaging
5g
Price
$399
Updated
2021/12/16
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methyl (4-formylphenoxy)acetate Chemical Properties,Usage,Production

Synthesis

123-08-0

96-32-2

73620-18-5

General procedure for the synthesis of methyl (4-formylphenoxy)acetate from p-hydroxybenzaldehyde and methyl bromoacetate: K2CO3 (5.43 g, 39.3 mmol) was added to a solution of 4-hydroxybenzaldehyde (3.0 g, 25 mmol) in acetone (61.4 mL) and the mixture was stirred vigorously. Methyl bromoacetate (2.8 mL, 29 mmol) was then added and the mixture was stirred at room temperature for 3.5 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure and then washed with 110 mL of water and extracted with ethyl acetate (EtOAc). The organic layer was separated, dried with anhydrous Na2SO4, filtered and concentrated to give a colorless oil which solidified to a white solid under vacuum in 82% isolated yield. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 9.87 (s, 1H), 7.82 (d, J = 8.8 Hz, 2H), 6.98 (d, J = 8.7 Hz, 2H), 4.70 (s, 2H), 3.79 (s, 3H). eSI-MS (m/z): 195.1 [M + H]+.

References

[1] Organic Letters, 2011, vol. 13, # 20, p. 5656 - 5659
[2] Organic Letters, 2004, vol. 6, # 12, p. 2019 - 2022
[3] Chemistry - A European Journal, 2008, vol. 14, # 19, p. 5812 - 5819
[4] Patent: WO2015/65716, 2015, A1. Location in patent: Paragraph 00490
[5] Patent: WO2016/144958, 2016, A1. Location in patent: Paragraph 00296

methyl (4-formylphenoxy)acetate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from methyl (4-formylphenoxy)acetate manufacturers

Honest Joy Holdings Limited
Product
Methyl2-(4-formylphenoxy)acetate 73620-18-5
Price
US $0.00/KG
Min. Order
1KG
Purity
98.5%
Supply Ability
100 tons
Release date
2022-01-14
Zhuozhou Wenxi import and Export Co., Ltd
Product
methyl (4-formylphenoxy)acetate 73620-18-5
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-11
Zhuozhou Wenxi import and Export Co., Ltd
Product
methyl (4-formylphenoxy)acetate 73620-18-5
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09

73620-18-5, methyl (4-formylphenoxy)acetateRelated Search:

efloxate 4-FORMYL-2-METHOXY-PHENOXY-ACETIC ACID ETHYL ESTER Fenofibrate FENOFIBRIC ACID ETHYL ESTER methyl (4-formylphenoxy)acetate METHYL 2-[2-(2-CHLORO-6-FLUOROBENZYL)-4-FORMYL-3-(2-METHOXY-2-OXOETHOXY)PHENOXY]ACETATE ETHYL 2-(4-CINNAMOYLPHENOXY)ACETATE AURORA 16634 METHYL 2-(4-CINNAMOYLPHENOXY)ACETATE AKOS BBS-00000010 AKOS BBS-00000001 AURORA 15480 METHYL 2-(4-[3-(4-CHLOROPHENYL)ACRYLOYL]PHENOXY)ACETATE methyl (4-acetylphenoxy)acetate ETHYL 2-(4-[3-(4-CHLOROPHENYL)ACRYLOYL]PHENOXY)ACETATE AURORA 15517 ETHYL 2-(2,6-DIBROMO-4-FORMYLPHENOXY)ACETATE 2-Methoxyethyl (2,3-dichloro-4-(2-thienylcarbonyl)phenoxy)acetate

  • acetic acid, (4-formylphenoxy)-, methyl ester
  • 2-(4-formylphenoxy)acetic acid methyl ester
  • Methyl 2-(4-forMylphenoxy)acetate
  • methyl 2-(4-methanoylphenoxy)ethanoate
  • Methyl 2-(4-formylphenoxy)
  • methyl (4-formylphenoxy)acetate
  • Acetic acid, 2-(4-formylphenoxy)-, methyl ester
  • 73620-18-5