2-amino-6-methoxybenzonitrile
- Product Name
- 2-amino-6-methoxybenzonitrile
- CAS No.
- 1591-37-3
- Chemical Name
- 2-amino-6-methoxybenzonitrile
- Synonyms
- 2-AMino-6-Methoxy-benzonitril;2-amino-6-methoxybenzonitrile;Benzonitrile, 2-amino-6-methoxy-
- CBNumber
- CB01557600
- Molecular Formula
- C8H8N2O
- Formula Weight
- 148.16
- MOL File
- 1591-37-3.mol
2-amino-6-methoxybenzonitrile Property
- Melting point:
- 141 °C
- Boiling point:
- 339.4±27.0 °C(Predicted)
- Density
- 1.17±0.1 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 1.39±0.10(Predicted)
- Appearance
- Light brown to brown Solid
Safety
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A898193
- Product name
- 2-Amino-6-methoxybenzonitrile
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 4H56-1-618
- Product name
- 2-Amino-6-methoxybenzonitrile
- Packaging
- 1g
- Price
- $72
- Updated
- 2021/12/16
- Product number
- FA10519
- Product name
- 2-Amino-6-methoxybenzonitrile
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- Z4229
- Product name
- 2-Amino-6-methoxybenzonitrile
- Packaging
- 1g
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 126220
- Product name
- 2-Amino-6-methoxybenzonitrile
- Purity
- >95%
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
2-amino-6-methoxybenzonitrile Chemical Properties,Usage,Production
Synthesis
77326-36-4
124-41-4
1591-37-3
Sodium methanolate (25% w/w in MeOH, 325 μL, 1.42 mmol, 1.1 eq.) was added to a solution of 2-amino-6-fluorobenzonitrile (176 mg, 1.29 mmol, 1.0 eq.) dissolved in DMF (1.00 mL) at room temperature, and the reaction was stirred for 18 hours. Upon completion of the reaction, the reaction solution was concentrated in vacuum and the residue was mixed with deionized water (10 mL) and stirred to precipitate a beige colored precipitate. The precipitate was collected by filtration under reduced pressure, dissolved in ethyl acetate and then concentrated again, ground with hexane, and finally the residual solvent was removed in vacuum to give 2-amino-6-methoxybenzonitrile (158 mg, 1.07 mmol, 83% yield) as a beige amorphous solid; melting point 143-145°C, literature value 136-140°C.
References
[1] Synthesis (Germany), 2017, vol. 49, # 1, p. 135 - 144
[2] Patent: WO2005/35486, 2005, A1. Location in patent: Page/Page column 49
[3] Patent: WO2006/56433, 2006, A2. Location in patent: Page/Page column 31-32
2-amino-6-methoxybenzonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-amino-6-methoxybenzonitrile manufacturers
- Product
- 2-amino-6-methoxybenzonitrile 1591-37-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95%
- Supply Ability
- 500kg
- Release date
- 2018-08-19