ChemicalBook > CAS DataBase List > TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE

TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE

Product Name: TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE
CAS No.: 132414-81-4
Chemical Name: TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE
Synonyms: 5-N-Boc-hexahydro-pyrrolo[3,4-b]pyrrole;Tert-butyl 2,7-diazabicyclo[3.3.0]octan-7-carboxylate;tert-butyl octahydropyrrolo[3,4-b]pyrrole-5-carboxylate;t-butyl hexahydropyrrolo[3,4-b]pyrrole-5(1H)-carboxylate;5-Methyl-2-(1-Methylethoxy)-4- (4-piperidinyl)- BenzenaM;tert-Butyl hexahydropyrrolo3,4-bpyrrol-5(1H)-carboxylate;TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLAT;TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE;Hexahydropyrrolo[3,4-b]pyrrole-5-carboxylic acid tert-butyl ester;1,1-Dimethylethyl hexahydropyrrolo[3,4-b]pyrrole-5(1H)-carboxylate
CBNumber: CB0155892
Molecular Formula: C11H20N2O2
Formula Weight: 212.29
MOL File: 132414-81-4.mol

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TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE Property

Boiling point:: 295.4±13.0 °C(Predicted)
Density: 1.076±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 10.72±0.20(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: N
Risk Statements: 50/53-50
Safety Statements: 60-61
RIDADR: UN3077

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B702788
Product name: Tert-ButylHexahydropyrrolo[3,4-B]Pyrrole-5(1H)-Carboxylate
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB43593
Product name: 5-Boc-hexahydropyrrolo[3,4-b]pyrrole
Packaging: 100mg
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB43593
Product name: 5-Boc-hexahydropyrrolo[3,4-b]pyrrole
Packaging: 250mg
Price: $125
Updated: 2021/12/16

Matrix Scientific

Product number: 072206
Product name: 5-Boc-hexahydropyrrolo[3,4-b]pyrrole
Purity: 95+%
Packaging: 1g
Price: $189
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB43593
Product name: 5-Boc-hexahydropyrrolo[3,4-b]pyrrole
Packaging: 500mg
Price: $200
Updated: 2021/12/16

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TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

132414-80-3

132414-81-4

GENERAL STEPS: 1-benzyl-5-BOC-hexahydropyrrolo[3,4-B]pyrrole (1.68 g, 5.5 mmol) was dissolved in methanol (40 mL) under a nitrogen atmosphere, ammonium formate (3.5 g, 55.5 mmol) and palladium/carbon catalyst (600 mg) were added. The reaction mixture was heated to reflux for 2 h, subsequently cooled to room temperature and filtered through filter paper padded with methanol. The filtrate was concentrated under reduced pressure and the resulting residue was dissolved in dichloromethane and washed with sodium bicarbonate solution. The organic phase was separated, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give 5-Boc-hexahydropyrrolo[3,4-B]pyrrole (1.1 g, 93% yield) as a gray oil. Mass spectrum (m/z): 213.2 [M+H]+.

References

[1] Patent: WO2017/21920, 2017, A1. Location in patent: Paragraph 0637; 0638

TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE Suppliers

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View Lastest Price from TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE 132414-81-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

Career Henan Chemical Co

Product: TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE 132414-81-4
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-13

132414-81-4, TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATERelated Search:

Pyrrolo[3,4-c]pyrazole-5(1H)-carboxylic acid, 4,6-dihydro-, 1,1-dimethylethyl ester 1,4,5,6-TETRAHYDROPYRROLO[3,4-C]PYRAZOLE Vitamin B series 5-TERT-BUTYL 2-ETHYL 6,7-DIHYDROTHIENO[3,2-C]PYRIDINE-2,5(4H)-DICARBOXYLATE 2-METHYL-2,4,6,7-TETRAHYDRO-5H-PYRAZOLO[4,3-C]PYRIDINE-5-CARBOXYLIC ACID, TERT-BUTYL ESTER 5-(TERT-BUTOXYCARBONYL)-4,5,6,7-TETRAHYDROTHIENO[3,2-C]PYRIDINE-2-CARBOXYLIC ACID tert-butyl 6,7-dihydro-1H-pyrazolo[4,3-c]pyridine-5(4H)-carboxylate 5-Boc-1-Phenyl-1,4,6,7-tetrahydropyrazolo[4,3-c]pyridine (cis)-5-Boc-Hexahydro-pyrrolo[3,4-b]pyrrole TERT-BUTYL 1-BENZYLHEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE 2-Boc-aminomethylpyrrolidine 3-N-BOC-3-N-METHYL-AMINOMETHYL PYRROLIDINE OCTAHYDRO-PYRROLO[3,4-B]PYRROLE TERT-BUTYL (3AS,6AS)-HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE (3AR,6AS)-TERT-BUTYL HEXAHYDROPYRROLO[3,2-B]PYRROLE-1(2H)-CARBOXYLATE (3AS,6AS)-TERT-BUTYL HEXAHYDROPYRROLO[3,2-B]PYRROLE-1(2H)-CARBOXYLATE

Hexahydropyrrolo[3,4-b]pyrrole-5-carboxylic acid tert-butyl ester

5-N-Boc-hexahydro-pyrrolo[3,4-b]pyrrole

Tert-butyl 2,7-diazabicyclo[3.3.0]octan-7-carboxylate

Pyrrolo[3,4-b]pyrrole-5(1H)-carboxylic acid, hexahydro-, 1,1-diMethylethyl ester

Octahydro-pyrrolo[3,4-b]pyridine-6-carboxylic acid tert-butyl ester

t-butyl hexahydropyrrolo[3,4-b]pyrrole-5(1H)-carboxylate

tert-butyl octahydropyrrolo[3,4-b]pyrrole-5-carboxylate

(3aR*,6aR*)-hexahydro-pyrrolo[3,4-b]pyrrole-5-carboxylic acid tert-butyl ester

TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLAT

tert-Butyl 2,3,3a,4,6,6a-hexahydro-1H-pyrrolo[2,3-c]pyrrole-5-carboxylate

TERT-BUTYL HEXAHYDROPYRROLO[3,4-B]PYRROLE-5(1H)-CARBOXYLATE

5-Methyl-2-(1-Methylethoxy)-4- (4-piperidinyl)- BenzenaM

1,1-Dimethylethyl hexahydropyrrolo[3,4-b]pyrrole-5(1H)-carboxylate

tert-Butyl hexahydropyrrolo3,4-bpyrrol-5(1H)-carboxylate

132414-81-4