3-CYANO-5-NITROBENZOTRIFLUORIDE
- Product Name
- 3-CYANO-5-NITROBENZOTRIFLUORIDE
- CAS No.
- 20566-80-7
- Chemical Name
- 3-CYANO-5-NITROBENZOTRIFLUORIDE
- Synonyms
- BUTTPARK 100\01-72;3-CYANO-5-NITROBENZOTRIFLUORIDE;3-CYANO-5-NITROBENZOTRIFLUOROIDE;3-Cyano-5-nitrobenzotrifluoride 97%;3-NITRO-5-(TRIFLUOROMETHYL)BENZONITRILE;Benzonitrile, 3-nitro-5-(trifluoromethyl)-;3-Cyano-5-nitrobenzotrifluoride[3-Nitro-5-(trifluoroMethyl)benzonitrile]
- CBNumber
- CB0237253
- Molecular Formula
- C8H3F3N2O2
- Formula Weight
- 216.12
- MOL File
- 20566-80-7.mol
3-CYANO-5-NITROBENZOTRIFLUORIDE Property
- Boiling point:
- 241.8±40.0 °C(Predicted)
- Density
- 1.49±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light yellow to yellow Crystal
Safety
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 26-36/37/39
- RIDADR
- 3276
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C907390
- Product name
- 3-Cyano-5-nitrobenzotrifluoride
- Packaging
- 5g
- Price
- $155
- Updated
- 2021/12/16
- Product number
- PC9255
- Product name
- 3-Cyano-5-nitrobenzotrifluoride
- Purity
- 97%
- Packaging
- 1g
- Price
- $15
- Updated
- 2021/12/16
- Product number
- 4854-3-40
- Product name
- 3-Cyano-5-nitrobenzotrifluoride
- Purity
- 97%
- Packaging
- 1g
- Price
- $25
- Updated
- 2021/12/16
- Product number
- PC9255
- Product name
- 3-Cyano-5-nitrobenzotrifluoride
- Purity
- 97%
- Packaging
- 5g
- Price
- $54
- Updated
- 2021/12/16
- Product number
- 074113
- Product name
- 3-Cyano-5-nitrobenzotrifluoride
- Purity
- 95+%
- Packaging
- 5g
- Price
- $64
- Updated
- 2021/12/16
3-CYANO-5-NITROBENZOTRIFLUORIDE Chemical Properties,Usage,Production
Synthesis
20566-89-6
20566-80-7
To a solution of dichloromethane (20 mL) containing 3-nitro-5-(trifluoromethyl)benzamide (1.5 g, 6.41 mmol) was sequentially added triethylamine (1.314 mL, 9.61 mmol) and trifluoroacetic anhydride (1.357 mL, 9.61 mmol) at 20 °C. The reaction mixture was stirred continuously at 20°C for 2 hours. The progress of the reaction was monitored by thin layer chromatography (Expanding Agent: Petroleum Ether/Ethyl Acetate=3:1, Rf=0.6) to confirm that the reaction was complete. After completion of the reaction, the mixture was concentrated to give the crude product. The crude product was purified by column chromatography (eluent: petroleum ether/ethyl acetate=3:1, Rf=0.6) to afford 3-nitro-5-(trifluoromethyl)benzonitrile (1.2 g, 5.14 mmol, 80% yield). The structure of the product was confirmed by NMR hydrogen spectroscopy (400 MHz, CDCl3-d): δ 8.71 (s, 2H), 8.24 (s, 1H).
References
[1] Patent: WO2014/141187, 2014, A1. Location in patent: Page/Page column 160; 161
3-CYANO-5-NITROBENZOTRIFLUORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-CYANO-5-NITROBENZOTRIFLUORIDE Suppliers
- Tel
- --
- Fax
- --
- info@chemsworth.com
- Country
- India
- ProdList
- 6700
- Advantage
- 30
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 3-CYANO-5-NITROBENZOTRIFLUORIDE manufacturers
- Product
- 3-Cyano-5-nitrobenzotrifluoride 20566-80-7
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-10