ChemicalBook > CAS DataBase List > 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL

6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL

Product Name
6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
CAS No.
75476-86-7
Chemical Name
6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
Synonyms
5-Bromoindanol;6-Bromo-1-indanol;6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL;1H-Inden-1-ol, 6-broMo-2,3-dihydro-
CBNumber
CB02458133
Molecular Formula
C9H9BrO
Formula Weight
213.07
MOL File
75476-86-7.mol
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6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Property

Melting point:
85-86 °C(Solv: hexane (110-54-3))
Boiling point:
293.2±35.0 °C(Predicted)
Density 
1.617±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
14.15±0.20(Predicted)
Appearance
White to yellow Solid
optical activity
Consistent with structure
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B684066
Product name
6-Bromoindan-1-ol
Packaging
250mg
Price
$1055
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0318334
Product name
6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
Purity
95.00%
Packaging
5MG
Price
$500.98
Updated
2021/12/16
Matrix Scientific
Product number
153486
Product name
6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity
95%
Packaging
1g
Price
$565
Updated
2021/12/16
Ambeed
Product number
A305401
Product name
6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity
98%
Packaging
250mg
Price
$20
Updated
2021/12/16
Ambeed
Product number
A305401
Product name
6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity
98%
Packaging
1g
Price
$57
Updated
2021/12/16
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6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Chemical Properties,Usage,Production

Synthesis

14548-39-1

75476-86-7

Example 10 Part A, Synthesis of 6-bromo-2,3-dihydro-1H-inden-1-ol: 6-bromo-1-indanone (1.4 g, 6.57 mmol) was dissolved in 20 mL of methanol, and sodium borohydride (0.087 g, 2.3 mmol) was slowly added over a period of 5 minutes at room temperature. The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and then partitioned between ethyl acetate (50 mL) and 1N HCl (20 mL). The organic layer was separated, dried over sodium sulfate and subsequently concentrated under reduced pressure to afford the title compound 6-bromo-2,3-dihydro-1H-inden-1-ol as a solid (1.4 g, 99%). The product was characterized by 1H NMR (CDCl3): δ 7.45 (s, 1H), 7.3 (d, 1H), 7.0 (d, 1H), 5.2 (t, 1H), 2.9 (m, 1H), 2.7 (m, 1H), 2.4 (m, 1H), 1.9 (m, 2H).

References

[1] Patent: JP2016/29040, 2016, A. Location in patent: Paragraph 0058
[2] Patent: US2002/40022, 2002, A1
[3] Patent: WO2016/203401, 2016, A1. Location in patent: Page/Page column 58; 59; 60; 199
[4] Patent: WO2018/104766, 2018, A1. Location in patent: Page/Page column 58-60; 200-201
[5] Patent: WO2018/109648, 2018, A1. Location in patent: Page/Page column 83

6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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75476-86-7, 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OLRelated Search:

Dextromethorphan hydrobromide monohydrate DiethylaMine hydrobroMide 6-Bromo-1,1-(ethylenedioxo)-indane 2-AMINO-6-BROMO-INDAN-1-OL HYDROCHLORIDE 6-Bromo-1,1-(propylenedioxo)-indane 3-BROMO-6,6A-DIHYDRO-1AH-1-OXA-CYCLOPROPA[A]INDENE 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL

  • 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
  • 1H-Inden-1-ol, 6-broMo-2,3-dihydro-
  • 5-Bromoindanol
  • 6-Bromo-1-indanol
  • 75476-86-7