6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL

Product Name: 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
CAS No.: 75476-86-7
Chemical Name: 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
Synonyms: 5-Bromoindanol;6-Bromo-1-indanol;6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL;1H-Inden-1-ol, 6-broMo-2,3-dihydro-
CBNumber: CB02458133
Molecular Formula: C9H9BrO
Formula Weight: 213.07
MOL File: 75476-86-7.mol

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6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Property

Melting point:: 85-86 °C(Solv: hexane (110-54-3))
Boiling point:: 293.2±35.0 °C(Predicted)
Density: 1.617±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.15±0.20(Predicted)
Appearance: White to yellow Solid
optical activity: Consistent with structure

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B684066
Product name: 6-Bromoindan-1-ol
Packaging: 250mg
Price: $1055
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0318334
Product name: 6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
Purity: 95.00%
Packaging: 5MG
Price: $500.98
Updated: 2021/12/16

Matrix Scientific

Product number: 153486
Product name: 6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity: 95%
Packaging: 1g
Price: $565
Updated: 2021/12/16

AOBChem

Product number: 28900
Product name: 6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity: 97%
Packaging: 100g
Price: $4543
Updated: 2021/12/16

Ambeed

Product number: A305401
Product name: 6-Bromo-2,3-dihydro-1H-inden-1-ol
Purity: 98%
Packaging: 250mg
Price: $20
Updated: 2021/12/16

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6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Chemical Properties,Usage,Production

Synthesis

14548-39-1

75476-86-7

Example 10 Part A, Synthesis of 6-bromo-2,3-dihydro-1H-inden-1-ol: 6-bromo-1-indanone (1.4 g, 6.57 mmol) was dissolved in 20 mL of methanol, and sodium borohydride (0.087 g, 2.3 mmol) was slowly added over a period of 5 minutes at room temperature. The reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the mixture was concentrated under reduced pressure and then partitioned between ethyl acetate (50 mL) and 1N HCl (20 mL). The organic layer was separated, dried over sodium sulfate and subsequently concentrated under reduced pressure to afford the title compound 6-bromo-2,3-dihydro-1H-inden-1-ol as a solid (1.4 g, 99%). The product was characterized by 1H NMR (CDCl3): δ 7.45 (s, 1H), 7.3 (d, 1H), 7.0 (d, 1H), 5.2 (t, 1H), 2.9 (m, 1H), 2.7 (m, 1H), 2.4 (m, 1H), 1.9 (m, 2H).

References

[1] Patent: JP2016/29040, 2016, A. Location in patent: Paragraph 0058
[2] Patent: US2002/40022, 2002, A1
[3] Patent: WO2016/203401, 2016, A1. Location in patent: Page/Page column 58; 59; 60; 199
[4] Patent: WO2018/104766, 2018, A1. Location in patent: Page/Page column 58-60; 200-201
[5] Patent: WO2018/109648, 2018, A1. Location in patent: Page/Page column 83

6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL Suppliers

China 60 India 1 United States 4 Global 65

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75476-86-7