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N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE

Product Name
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
CAS No.
147356-78-3
Chemical Name
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
Synonyms
opropanecarboxamide;N-METHOXY-N-METHYL-CYCLOPROPANAMIDE;N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE;Cyclopropanecarboxamide, N-methoxy-N-methyl-;cyclopropanecarboxylic acid N-methoxy-N-methylamide;N-methoxy-N-methylcyclopropanecarboxamide(WXC04265)
CBNumber
CB02464820
Molecular Formula
C6H11NO2
Formula Weight
129.16
MOL File
147356-78-3.mol
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N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Property

Boiling point:
151.5±23.0 °C(Predicted)
Density 
1.126±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
Appearance
Colorless to light yellow Liquid
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Safety

Safety Statements 
24/25
HS Code 
29241990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
M271788
Product name
N-Methoxy-N-methylcyclopropanecarboxamide
Packaging
250mg
Price
$55
Updated
2021/12/16
Usbiological
Product number
459311
Product name
N-Methoxy-N-methylcyclopropanecarboxamide
Packaging
100mg
Price
$305
Updated
2021/12/16
AK Scientific
Product number
J93810
Product name
N-Methoxy-N-methylcyclopropanecarboxamide
Packaging
1g
Price
$25
Updated
2021/12/16
Matrix Scientific
Product number
118045
Product name
N-Methoxy-N-methylcyclopropanecarboxamide
Packaging
1g
Price
$301
Updated
2021/12/16
SynQuest Laboratories
Product number
4256-1-24
Product name
N-Methoxy-N-methylcyclopropanecarboxamide
Packaging
1g
Price
$474
Updated
2021/12/16
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N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Chemical Properties,Usage,Production

Synthesis

6638-79-5

4023-34-1

147356-78-3

To a solution of dichloromethane (60 mL) containing N,O-dimethylhydroxylamine hydrochloride (10.0 g, 95.69 mmol, 1.0 eq.) and triethylamine (19.36 g, 191.6 mmol, 2.0 eq.), the reaction mixture was stirred at 0 °C for 30 min. Subsequently, cyclopropanecarbonyl chloride (Compound 96.1) was slowly added at the same temperature. The reaction mixture was transferred to room temperature and continued stirring for 15 hours. After completion of the reaction, the organic layer was washed sequentially with water, brine, saturated sodium bicarbonate solution and 1.0 N hydrochloric acid, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. Finally, the crude product was purified by column chromatography to afford N-methoxy-N-methylcyclopropane carboxamide (Compound 96.2, 9.0 g, 72.9% yield).

References

[1] Journal of Medicinal Chemistry, 2017, vol. 60, # 12, p. 4840 - 4860
[2] Patent: WO2017/40757, 2017, A1. Location in patent: Paragraph 00466-00467
[3] Patent: US2005/197337, 2005, A1. Location in patent: Page/Page column 10
[4] Patent: WO2005/94828, 2005, A1. Location in patent: Page/Page column 19
[5] Patent: WO2008/34860, 2008, A1. Location in patent: Page/Page column 139

N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE Suppliers

China 74 India 1 United Kingdom 1 United States 8 Global 84
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
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View Lastest Price from N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE manufacturers

Career Henan Chemical Co
Product
N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE 147356-78-3
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
100kg
Release date
2018-12-22

147356-78-3, N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDERelated Search:

Cyclopropyl carbinol N-Methylformamide FORMANILIDE N-Methylbenzamide N-Methylpropionamide

  • N-methoxy-N-methylcyclopropanecarboxamide(WXC04265)
  • N-METHOXY-N-METHYL-CYCLOPROPANAMIDE
  • N-METHOXY-N-METHYLCYCLOPROPANECARBOXAMIDE
  • cyclopropanecarboxylic acid N-methoxy-N-methylamide
  • opropanecarboxamide
  • Cyclopropanecarboxamide, N-methoxy-N-methyl-
  • 147356-78-3
  • Triazines ,Thiophenes