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2-(3-bromophenyl)Naphthalene

Product Name
2-(3-bromophenyl)Naphthalene
CAS No.
667940-23-0
Chemical Name
2-(3-bromophenyl)Naphthalene
Synonyms
2-(3-broMophenyl)naphthale;2-(3-bromophenyl)phthalene;2-(3-bromophenyl)Naphthalene;Naphthalene, 2-(3-bromophenyl)-;2-(3-Bromophenyl)naphthalene,98%;2-(3-Bromophenyl)naphthalene >
CBNumber
CB02489593
Molecular Formula
C16H11Br
Formula Weight
283.16
MOL File
667940-23-0.mol
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2-(3-bromophenyl)Naphthalene Property

Melting point:
97.0 to 101.0 °C
Boiling point:
385.2±11.0 °C(Predicted)
Density 
1.381±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. 
Sealed in dry,Room Temperature
form 
Solid
color 
White to Yellow to Orange
InChI
InChI=1S/C16H11Br/c17-16-7-3-6-14(11-16)15-9-8-12-4-1-2-5-13(12)10-15/h1-11H
InChIKey
FWPXWVYUNHYGPE-UHFFFAOYSA-N
SMILES
C1=C2C(C=CC=C2)=CC=C1C1=CC=CC(Br)=C1
CAS DataBase Reference
667940-23-0
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Safety

HS Code 
2903.99.8001
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4568
Product name
2-(3-Bromophenyl)naphthalene
Purity
>95.0%(GC)
Packaging
1g
Price
$33
Updated
2025/07/31
TCI Chemical
Product number
B4568
Product name
2-(3-Bromophenyl)naphthalene
Purity
>95.0%(GC)
Packaging
5g
Price
$165
Updated
2025/07/31
TRC
Product number
B678240
Product name
2-(3-Bromophenyl)naphthalene
Packaging
50mg
Price
$60
Updated
2021/12/16
TRC
Product number
B678240
Product name
2-(3-Bromophenyl)naphthalene
Packaging
100mg
Price
$75
Updated
2021/12/16
TRC
Product number
B678240
Product name
2-(3-Bromophenyl)naphthalene
Packaging
10mg
Price
$45
Updated
2021/12/16
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2-(3-bromophenyl)Naphthalene Chemical Properties,Usage,Production

Chemical Properties

Type of white solid

Synthesis

591-18-4

32316-92-0

667940-23-0

1. Preparation of Compound 2a: 1-Bromo-3-iodobenzene (10 g, 35.35 mmol) and 2-naphthaleneboronic acid (5.47 g, 31.82 mmol) were dissolved in anhydrous tetrahydrofuran (THF, 100 mL) under dry conditions. Subsequently, tetrakis(triphenylphosphine)palladium (Pd(PPh3)4, 1.2 g, 1.06 mmol) and 2M aqueous potassium carbonate (K2CO3) (50 mL) were added. The reaction mixture was heated to reflux for 24 hours. After completion of the reaction, the organic layer was extracted with ethyl acetate and dried with anhydrous magnesium sulfate (MgSO4). After filtration to remove the desiccant, the organic layer was concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography followed by recrystallization in a solvent mixture of tetrahydrofuran (THF) and ethanol (EtOH) to afford the white solid compound 2a (8.5 g, 85% yield). Mass spectrometry analysis showed [M + H]+ peak located at 283 m/z.

References

[1] Patent: WO2008/13399, 2008, A1. Location in patent: Page/Page column 14-15
[2] Patent: US2010/331585, 2010, A1. Location in patent: Page/Page column 94-95
[3] Organic and Biomolecular Chemistry, 2017, vol. 15, # 19, p. 4096 - 4114

2-(3-bromophenyl)Naphthalene Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(3-bromophenyl)Naphthalene Suppliers

Americas 1 CHINA 114 Europe 1 India 3 Japan 1 United States 9 Global 129
Alfa Chemistry
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View Lastest Price from 2-(3-bromophenyl)Naphthalene manufacturers

Henan Fengda Chemical Co., Ltd
Product
2-(3-bromophenyl)Naphthalene 667940-23-0
Price
US $101.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-28
Hebei Xinsheng New Material Technology Co., LTD.
Product
2-(3-bromophenyl)Naphthalene 667940-23-0
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-09-14
Hebei Xinsheng New Material Technology Co., LTD.
Product
2-(3-Bromophenyl)naphthalene 667940-23-0
Price
US $0.00-0.00/Kg
Min. Order
1Kg
Purity
99.9%
Supply Ability
30000 Kg
Release date
2023-10-31

667940-23-0, 2-(3-bromophenyl)NaphthaleneRelated Search:


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  • 667940-23-0