Benzyl4-iodobenzoate

Product Name: Benzyl4-iodobenzoate
CAS No.: 136618-42-3
Chemical Name: Benzyl4-iodobenzoate
Synonyms: Benzyl4-iodobenzoate;Benzoic acid, 4-iodo-, phenylmethyl ester
CBNumber: CB02499132
Molecular Formula: C14H11IO2
Formula Weight: 338.14
MOL File: 136618-42-3.mol

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Benzyl4-iodobenzoate Property

Melting point:: 65-66°
Boiling point:: 397.6±25.0 °C(Predicted)
Density: 1.609±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B279908
Product name: Benzyl4-iodobenzoate
Packaging: 1g
Price: $195
Updated: 2021/12/16

Matrix Scientific

Product number: 074737
Product name: Benzyl 4-iodobenzoate
Purity: 95+%
Packaging: 5g
Price: $899
Updated: 2021/12/16

AK Scientific

Product number: X9951
Product name: Benzyl4-iodobenzoate
Packaging: 25g
Price: $945
Updated: 2021/12/16

Matrix Scientific

Product number: 074737
Product name: Benzyl 4-iodobenzoate
Purity: 95+%
Packaging: 10g
Price: $1286
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0368576
Product name: BENZYL-4-IODOBENZOATE
Purity: 95.00%
Packaging: 5MG
Price: $504.12
Updated: 2021/12/16

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Benzyl4-iodobenzoate Chemical Properties,Usage,Production

Synthesis

619-58-9

100-39-0

136618-42-3

General procedure: 4-Iodobenzoic acid (15.62 g, 63 mmol, 1.05 eq.) was suspended in anhydrous DMF (90 mL, 6 vol.) under nitrogen protection, potassium carbonate (8.7 g, 63 mmol, 1.05 eq.) was added, and stirred for 10 minutes. Subsequently, benzyl bromide (10.25 g, 7.13 mL, 60 mmol, 1 eq.) was slowly added dropwise for a controlled time of about 5 minutes. The reaction mixture was continued to be stirred at room temperature for 6.25 hours. Upon completion of the reaction, the mixture was transferred to a partition funnel and extracted with ether (200 mL) and water (200 mL) by partition. The aqueous phase was extracted once more with ether, and the organic phases were combined and washed sequentially with water, aqueous lithium chloride and brine. The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to afford benzyl 4-iodobenzoate (18.38 g, 86% yield) as a white crystalline solid. The product was analyzed by LCMS: tRET = 3.81 min, 70% ES + ve 376,356 (artifactual peak appeared at 1.48 min, 28%).1H NMR (400 MHz, DMSO-d6) δ ppm: 7.92 (d, 2H), 7.74 (d, 2H), 7.46 (d, 2H), 7.35-7.42 (m, 3H ), 5.34 (s, 2H).

References

[1] Patent: WO2009/74590, 2009, A1. Location in patent: Page/Page column 59-60
[2] Patent: WO2009/50220, 2009, A1. Location in patent: Page/Page column 42

Benzyl4-iodobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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136618-42-3, Benzyl4-iodobenzoateRelated Search:

Benzyl4-iodobenzoate

Benzoic acid, 4-iodo-, phenylmethyl ester

136618-42-3