5-Bromo-6-methoxybenzoimidazole

Product Name: 5-Bromo-6-methoxybenzoimidazole
CAS No.: 1008361-65-6
Chemical Name: 5-Bromo-6-methoxybenzoimidazole
Synonyms: 5-Bromo-6-methoxybenzimidazole;5-Bromo-6-methoxybenzoimidazole;6-Bromo-5-methoxy-1H-benzimidazole;5-Bromo-6-methoxybenzimidazole 97%;1H-Benzimidazole, 6-bromo-5-methoxy-;5-bromo-6-methoxy-1H-1,3-benzodiazole;5-Bromo-6-methoxy-1H-benzo[d]imidazole
CBNumber: CB02522333
Molecular Formula: C8H7BrN2O
Formula Weight: 227.06
MOL File: 1008361-65-6.mol

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5-Bromo-6-methoxybenzoimidazole Property

Boiling point:: 435.7±25.0 °C(Predicted)
Density: 1.678±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 12.43±0.30(Predicted)
Appearance: White to yellow Solid

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Safety

HS Code: 2933299090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B696598
Product name: 5-Bromo-6-methoxybenzoimidazole
Packaging: 25mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B696598
Product name: 5-Bromo-6-methoxybenzoimidazole
Packaging: 250mg
Price: $125
Updated: 2021/12/16

AK Scientific

Product number: Z3795
Product name: 5-Bromo-6-methoxy-1H-benzo[d]imidazole
Packaging: 250mg
Price: $130
Updated: 2021/12/16

Apolloscientific

Product number: OR400542
Product name: 5-Bromo-6-methoxybenzimidazole
Purity: 97%
Packaging: 250mg
Price: $135
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-9-4K
Product name: 5-Bromo-6-methoxybenzimidazole
Packaging: 250mg
Price: $160
Updated: 2021/12/16

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5-Bromo-6-methoxybenzoimidazole Chemical Properties,Usage,Production

Synthesis

64-18-6

108447-01-4

1008361-65-6

Step 2: Formic acid (1 mL) was added to a mixed solution of 4-bromo-5-methoxybenzene-1,2-diamine (3.8 g, 18 mmol) and triethyl orthoformate (50 mL) prepared in Step 1 under stirring conditions. The reaction mixture was heated to reflux for 3 hours and subsequently concentrated under reduced pressure. The concentrated residue was extracted by partitioning with ethyl acetate (200 mL) and 1N aqueous sodium carbonate solution (100 mL). The organic layer (ethyl acetate layer) was separated, washed with brine (100 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 5-bromo-6-methoxy-1H-benzo[d]imidazole (4.0 g) as a brown oil. The product was used directly in the subsequent reaction without further purification.LCMS (ESI) m/z 228 and 230 (M + H)+.

References

[1] Patent: EP2766359, 2016, B1. Location in patent: Paragraph 0472

5-Bromo-6-methoxybenzoimidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Bromo-6-methoxybenzoimidazole Suppliers

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