5-Bromo-6-methoxybenzoimidazole
- Product Name
- 5-Bromo-6-methoxybenzoimidazole
- CAS No.
- 1008361-65-6
- Chemical Name
- 5-Bromo-6-methoxybenzoimidazole
- Synonyms
- 5-Bromo-6-methoxybenzimidazole;5-Bromo-6-methoxybenzoimidazole;6-Bromo-5-methoxy-1H-benzimidazole;5-Bromo-6-methoxybenzimidazole 97%;1H-Benzimidazole, 6-bromo-5-methoxy-;5-bromo-6-methoxy-1H-1,3-benzodiazole;5-Bromo-6-methoxy-1H-benzo[d]imidazole
- CBNumber
- CB02522333
- Molecular Formula
- C8H7BrN2O
- Formula Weight
- 227.06
- MOL File
- 1008361-65-6.mol
5-Bromo-6-methoxybenzoimidazole Property
- Boiling point:
- 435.7±25.0 °C(Predicted)
- Density
- 1.678±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 12.43±0.30(Predicted)
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2933299090
N-Bromosuccinimide Price
- Product number
- B696598
- Product name
- 5-Bromo-6-methoxybenzoimidazole
- Packaging
- 25mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B696598
- Product name
- 5-Bromo-6-methoxybenzoimidazole
- Packaging
- 250mg
- Price
- $125
- Updated
- 2021/12/16
- Product number
- Z3795
- Product name
- 5-Bromo-6-methoxy-1H-benzo[d]imidazole
- Packaging
- 250mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- OR400542
- Product name
- 5-Bromo-6-methoxybenzimidazole
- Purity
- 97%
- Packaging
- 250mg
- Price
- $135
- Updated
- 2021/12/16
- Product number
- 4H56-9-4K
- Product name
- 5-Bromo-6-methoxybenzimidazole
- Packaging
- 250mg
- Price
- $160
- Updated
- 2021/12/16
5-Bromo-6-methoxybenzoimidazole Chemical Properties,Usage,Production
Synthesis
64-18-6
108447-01-4
1008361-65-6
Step 2: Formic acid (1 mL) was added to a mixed solution of 4-bromo-5-methoxybenzene-1,2-diamine (3.8 g, 18 mmol) and triethyl orthoformate (50 mL) prepared in Step 1 under stirring conditions. The reaction mixture was heated to reflux for 3 hours and subsequently concentrated under reduced pressure. The concentrated residue was extracted by partitioning with ethyl acetate (200 mL) and 1N aqueous sodium carbonate solution (100 mL). The organic layer (ethyl acetate layer) was separated, washed with brine (100 mL), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 5-bromo-6-methoxy-1H-benzo[d]imidazole (4.0 g) as a brown oil. The product was used directly in the subsequent reaction without further purification.LCMS (ESI) m/z 228 and 230 (M + H)+.
References
[1] Patent: EP2766359, 2016, B1. Location in patent: Paragraph 0472
5-Bromo-6-methoxybenzoimidazole Preparation Products And Raw materials
Raw materials
Preparation Products
5-Bromo-6-methoxybenzoimidazole Suppliers
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- India
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