Methyl 2-fluoro-3-methoxybenzoate

Product Name: Methyl 2-fluoro-3-methoxybenzoate
CAS No.: 958991-48-5
Chemical Name: Methyl 2-fluoro-3-methoxybenzoate
Synonyms: Methyl 2-fluoro-3-methoxybenzoate;methyl 2-fluoro-3-(methyloxy)benzoate;2-Fluoro-3-methoxybenzoic acid methyl ester;Benzoic acid, 2-fluoro-3-methoxy-, methyl ester;methyl 2-fluoro-3-(methyloxy)benzoate methyl 2-fluoro-3-(methyloxy)benzoate Methyl 2-fluoro-3-(methyloxy)benzoate
CBNumber: CB02565200
Molecular Formula: C9H9FO3
Formula Weight: 184.16
MOL File: 958991-48-5.mol

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Methyl 2-fluoro-3-methoxybenzoate Property

Boiling point:: 260.5±25.0 °C(Predicted)
Density: 1.184±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Safety

HS Code: 2916310090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M305413
Product name: Methyl2-Fluoro-3-methoxybenzoate
Packaging: 100mg
Price: $55
Updated: 2021/12/16

TRC

Product number: M305413
Product name: Methyl2-Fluoro-3-methoxybenzoate
Packaging: 250mg
Price: $100
Updated: 2021/12/16

TRC

Product number: M305413
Product name: Methyl2-Fluoro-3-methoxybenzoate
Packaging: 500mg
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: V9847
Product name: Methyl2-fluoro-3-methoxybenzoate
Packaging: 1g
Price: $197
Updated: 2021/12/16

Crysdot

Product number: CD12001553
Product name: Methyl2-fluoro-3-methoxybenzoate
Purity: 95+%
Packaging: 5g
Price: $344
Updated: 2021/12/16

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Methyl 2-fluoro-3-methoxybenzoate Chemical Properties,Usage,Production

Synthesis

34472-65-6

137654-20-7

958991-48-5

To a suspension of 2-fluoro-3-methoxybenzoic acid (2.0 g, 11.8 mmol) in dichloromethane (20 mL) and methanol (2 mL) was added slowly and dropwise trimethylmethylsilyl diazomethane (2M ethyl ether solution, 12.3 mmol, 6.2 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 30 min and then the solvent was removed by distillation under reduced pressure. The residue was diluted with ethyl acetate, adsorbed on silica gel and purified by silica gel column chromatography in two batches to give 2.0 g (92% yield) of methyl 2-fluoro-3-methoxybenzoate. The product was characterized by 1H NMR (CDCl3, 400 MHz): δ 7.48-7.44 (m, 1H), 7.15-7.09 (m, 2H), 3.93 (s, 3H), 3.91 (s, 3H).

References

[1] Patent: WO2009/32667, 2009, A1. Location in patent: Page/Page column 166-167

Methyl 2-fluoro-3-methoxybenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 2-fluoro-3-methoxybenzoate manufacturers

Career Henan Chemical Co

Product: Methyl 2-fluoro-3-methoxybenzoate 958991-48-5
Price: US $1.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

958991-48-5, Methyl 2-fluoro-3-methoxybenzoateRelated Search:

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Methyl 2-fluoro-3-methoxybenzoate

methyl 2-fluoro-3-(methyloxy)benzoate

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methyl 2-fluoro-3-(methyloxy)benzoate methyl 2-fluoro-3-(methyloxy)benzoate Methyl 2-fluoro-3-(methyloxy)benzoate

2-Fluoro-3-methoxybenzoic acid methyl ester

958991-48-5