ChemicalBook > CAS DataBase List > 3,5-DibroMo-biphenyl

3,5-DibroMo-biphenyl

Product Name: 3,5-DibroMo-biphenyl
CAS No.: 16372-96-6
Chemical Name: 3,5-DibroMo-biphenyl
Synonyms: PBB 14;3,5-DibroMo-biphenyl;3,5-Dibromo-1,1'-biphenyl;1,1'-Biphenyl, 3,5-dibromo-;3,5-DIBROMO-1-PHENYLBENZENE
CBNumber: CB02570622
Molecular Formula: C12H8Br2
Formula Weight: 312
MOL File: 16372-96-6.mol

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3,5-DibroMo-biphenyl Property

Melting point:: 156-157℃
Boiling point:: 208 °C(Press: 15 Torr)
Density: 1.7197 g/cm3(Temp: 25 °C)
refractive index: 1.6541 (589.3 nm 25℃)
storage temp.: Sealed in dry,Room Temperature
form: crystalline solid
color: White
InChI: InChI=1S/C12H8Br2/c13-11-6-10(7-12(14)8-11)9-4-2-1-3-5-9/h1-8H
InChIKey: HIHYAKDOWUFGBK-UHFFFAOYSA-N
SMILES: C1(C2=CC=CC=C2)=CC(Br)=CC(Br)=C1
EPA Substance Registry System: 1,1'-Biphenyl, 3,5-dibromo- (16372-96-6)

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Safety

HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

AK Scientific

Product number: X7241
Product name: 3,5-Dibromo-1,1'-biphenyl
Packaging: 25g
Price: $371
Updated: 2021/12/16

AstaTech

Product number: CX1328
Product name: 3,5-DIBROMO-BIPHENYL
Purity: 99%
Packaging: 1/ G
Price: $30
Updated: 2021/12/16

AstaTech

Product number: CX1328
Product name: 3,5-DIBROMO-BIPHENYL
Purity: 99%
Packaging: 5/ G
Price: $73
Updated: 2021/12/16

Crysdot

Product number: CD41001877
Product name: 3,5-Dibromo-1,1'-biphenyl
Purity: 97%
Packaging: 5g
Price: $74
Updated: 2021/12/16

Crysdot

Product number: CD41001877
Product name: 3,5-Dibromo-1,1'-biphenyl
Purity: 97%
Packaging: 10g
Price: $119
Updated: 2021/12/16

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3,5-DibroMo-biphenyl Chemical Properties,Usage,Production

Chemical Properties

Colorless liquid

Synthesis

626-39-1

98-80-6

16372-96-6

A suspension of EtOH-H2O (3 mL, v:v = 1:1) with 1,3,5-tribromobenzene (1.0 mmol), phenylboronic acid (1.2 mmol), potassium carbonate (276 mg, 2.0 mmol), and Pd/HCCP-DABP catalyst (20 mg, 0.3 mol%) was added to the Schlenk tube. The system was evacuated and backfilled three times with nitrogen. The reaction mixture was stirred at 50 °C for 2.5 hours. After completion of the reaction, it was cooled to room temperature and extracted with dichloromethane (CH2Cl2). The organic phases were combined, dried with anhydrous sodium sulfate, concentrated under reduced pressure and purified by silica gel column chromatography to give 1-phenyl-3,5-dibromobenzene. The aqueous phase was filtered through filter paper, the solid was washed with CH2Cl2, and the recovered catalyst could be used in subsequent reactions.

References

[1] Reactive and Functional Polymers, 2017, vol. 110, p. 38 - 46
[2] Patent: KR2016/69021, 2016, A. Location in patent: Paragraph 0155-0157
[3] Journal of the American Chemical Society, 1990, vol. 112, # 22, p. 8024 - 8034
[4] Patent: KR2015/53913, 2015, A. Location in patent: Paragraph 0533-0535
[5] Patent: KR2015/127023, 2015, A. Location in patent: Paragraph 0409; 0560; 0561; 0562; 0563; 0564

3,5-DibroMo-biphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,5-DibroMo-biphenyl manufacturers

Hebei Xinsheng New Material Technology Co., LTD.

Product: 3,5-DibroMo-biphenyl 16372-96-6
Price: US $35.00-25.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 Ton
Release date: 2023-11-07

Career Henan Chemical Co

Product: 3,5-DibroMo-biphenyl 16372-96-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2018-08-06

16372-96-6, 3,5-DibroMo-biphenylRelated Search:

ACETONE-D6 Copper(II) sulfate pentahydrate

3,5-DibroMo-biphenyl

3,5-DIBROMO-1-PHENYLBENZENE

PBB 14

1,1'-Biphenyl, 3,5-dibromo-

3,5-Dibromo-1,1'-biphenyl

16372-96-6