6-BroMo-5-chloro-pyridine-2-carboxylic acid

Product Name: 6-BroMo-5-chloro-pyridine-2-carboxylic acid
CAS No.: 1214328-42-3
Chemical Name: 6-BroMo-5-chloro-pyridine-2-carboxylic acid
Synonyms: 6-BroMo-5-chloropicolinic acid;2-BROMO-3-CHLORO-6-CARBOXYPYRIDINE;6-bromo-5-chloro-2-Pyridinecarboxylic acid;2-Bromo-3-chloropyridine-6-carboxylic acid;6-BroMo-5-chloro-pyridine-2-carboxylic acid;36-bromo-5-chloropyridine-2-carboxylic acid;2-Pyridinecarboxylic acid, 6-bromo-5-chloro-
CBNumber: CB02595320
Molecular Formula: C6H3BrClNO2
Formula Weight: 236.45
MOL File: 1214328-42-3.mol

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6-BroMo-5-chloro-pyridine-2-carboxylic acid Property

Boiling point:: 374.5±42.0 °C(Predicted)
Density: 1.917±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 3.02±0.10(Predicted)
form: solid
color: Off white

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B679308
Product name: 6-Bromo-5-chloropicolinicAcid
Packaging: 50mg
Price: $90
Updated: 2021/12/16

TRC

Product number: B679308
Product name: 6-Bromo-5-chloropicolinicAcid
Packaging: 100mg
Price: $130
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H58-D-05
Product name: 6-Bromo-5-chloropicolinic acid
Purity: 95%
Packaging: 1g
Price: $138
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: B13656
Product name: 6-Bromo-5-chloropyridine-2-carboxylicacid
Packaging: 1g
Price: $150
Updated: 2021/12/16

Matrix Scientific

Product number: 076984
Product name: 2-Bromo-3-chloropyridine-6-carboxylic acid
Purity: 98%
Packaging: 1g
Price: $233
Updated: 2021/12/16

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6-BroMo-5-chloro-pyridine-2-carboxylic acid Chemical Properties,Usage,Production

Uses

6-Bromo-5-chloro-pyridine-2-carboxylic acid is a carboxylic acid derivative used in organic synthesis and pharmaceutical experiments.

Synthesis

1415898-80-4

1214328-42-3

5-Chloro-1-yloxy-pyridine-2-carboxylic acid (3.5 g, 20 mmol) was slowly added to phosphorus trioxide (CAS 7789-59-5, 30 g) at 80 °C and the reaction was kept stirring for 2 hours. Upon completion of the reaction, the reaction mixture was quenched by careful pouring into ice water (100 mL) and subsequently extracted with ethyl acetate (3 x 50 mL). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by column chromatography (silica gel 100 g, eluent 50% petroleum ether solution of ethyl acetate) to give 2-bromo-3-chloro-6-carboxypyridine (1.12 g, 23% yield) as a gray solid. Mass spectrometry (EI) analysis showed: m/e 236.0 [M+H]+.

References

[1] Patent: US2012/316147, 2012, A1. Location in patent: Page/Page column 55
[2] Patent: WO2012/168350, 2012, A1. Location in patent: Page/Page column 119; 120

6-BroMo-5-chloro-pyridine-2-carboxylic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BroMo-5-chloro-pyridine-2-carboxylic acid Suppliers

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1214328-42-3, 6-BroMo-5-chloro-pyridine-2-carboxylic acidRelated Search:

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6-BroMo-5-chloro-pyridine-2-carboxylic acid

2-Bromo-3-chloropyridine-6-carboxylic acid

6-BroMo-5-chloropicolinic acid

6-bromo-5-chloro-2-Pyridinecarboxylic acid

2-BROMO-3-CHLORO-6-CARBOXYPYRIDINE

2-Pyridinecarboxylic acid, 6-bromo-5-chloro-

36-bromo-5-chloropyridine-2-carboxylic acid

1214328-42-3