6-BroMo-5-Methoxypicolinaldehyde

Product Name: 6-BroMo-5-Methoxypicolinaldehyde
CAS No.: 329217-74-5
Chemical Name: 6-BroMo-5-Methoxypicolinaldehyde
Synonyms: 6-BroMo-5-Methoxypicolinaldehyde;6-Bromo-5-methoxy-pyridine-2-carbaldehyde;6-Bromo-5-methoxypyridine-2-carboxaldehyde;2-Pyridinecarboxaldehyde, 6-bromo-5-methoxy-
CBNumber: CB22641027
Molecular Formula: C7H6BrNO2
Formula Weight: 216.03
MOL File: 329217-74-5.mol

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6-BroMo-5-Methoxypicolinaldehyde Property

Melting point:: 122～124℃
Boiling point:: 302.7±37.0 °C(Predicted)
Density: 1.606±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 0.44±0.10(Predicted)
Appearance: Off-white to light yellow Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B711225
Product name: 6-Bromo-5-methoxypicolinaldehyde
Packaging: 100mg
Price: $175
Updated: 2021/12/16

Matrix Scientific

Product number: 048665
Product name: 6-Bromo-5-methoxy-2-pyridinecarbaldehyde
Purity: >95%
Packaging: 500mg
Price: $231
Updated: 2021/12/16

Matrix Scientific

Product number: 048665
Product name: 6-Bromo-5-methoxy-2-pyridinecarbaldehyde
Purity: >95%
Packaging: 1g
Price: $356
Updated: 2021/12/16

AK Scientific

Product number: 3741AB
Product name: 6-Bromo-5-methoxypicolinaldehyde
Packaging: 1g
Price: $530
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-9-L2
Product name: 6-Bromo-5-methoxypyridine-2-carboxaldehyde
Packaging: 500mg
Price: $567
Updated: 2021/12/16

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6-BroMo-5-Methoxypicolinaldehyde Chemical Properties,Usage,Production

Synthesis

905562-91-6

329217-74-5

General procedure for the synthesis of 6-bromo-5-methoxypyridine-2-carboxaldehyde from (6-bromo-5-methoxypyridin-2-yl)methanol: (6-bromo-5-methoxypyridin-2-yl)methanol (2.30 g, 10 mmol) was dissolved in dichloromethane (50 mL) at room temperature, followed by addition of manganese dioxide (8.0 g). The reaction mixture was stirred continuously at room temperature for 24 hours. After completion of the reaction, the mixture was cooled to room temperature and the insoluble solids were removed by filtration. The filtrate was concentrated under reduced pressure to afford 6-bromo-5-methoxypyridine-2-carbaldehyde (1.35 g, 63% yield) as an off-white solid. Its nuclear magnetic resonance hydrogen spectrum (1H NMR, 400 MHz, CDCl3) data were as follows: δ 9.94 (s, 1H), 7.96 (d, J = 8.4 Hz, 1H), 7.27 (d, J = 8.0 Hz, 1H), 4.03 (s, 3H).

References

[1] Patent: US2014/142102, 2014, A1. Location in patent: Paragraph 0546
[2] Patent: US2014/140956, 2014, A1. Location in patent: Paragraph 0828

6-BroMo-5-Methoxypicolinaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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6-BroMo-5-Methoxypicolinaldehyde Suppliers

China 26 United Kingdom 1 United States 5 Global 32

SuZhou ShiYa Biopharmaceuticals, Inc.

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Cool Pharm, Ltd

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329217-74-5, 6-BroMo-5-MethoxypicolinaldehydeRelated Search:

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6-BroMo-5-Methoxypicolinaldehyde

6-Bromo-5-methoxypyridine-2-carboxaldehyde

6-Bromo-5-methoxy-pyridine-2-carbaldehyde

2-Pyridinecarboxaldehyde, 6-bromo-5-methoxy-

329217-74-5