11,12-Dihydro-11-phenylindolo[2,3-a]carbazole

Product Name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
CAS No.: 1024598-06-8
Chemical Name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Synonyms: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole;11,12-Dihydro-11-phenylindo;11-phenylindolo[2,3-a]carbazole;12-Phenyl-11H-indolo[2,3-a]carbazole;1-Phenyl-11,12-dihydroindolo[2,3-a]carbazole;1,12-Dihydro-11-phenylindolo[2,3-a]carbazole;11,12-Dihydro-11-phenylindolo[2,3-a]carbazole;Indolo[2,3-a]carbazole, 11,12-dihydro-11-phenyl-;11,12-Dihydro-11-phenylindolo[2,3-a]carbazole>11,12-Dihydro-11-phenyl-1H-indolo[2,3-a]carbazole
CBNumber: CB02614434
Molecular Formula: C24H16N2
Formula Weight: 332.4
MOL File: 1024598-06-8.mol

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11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Property

Boiling point:: 598.8±32.0 °C(Predicted)
Density: 1.26
storage temp.: Sealed in dry,Room Temperature
form: powder to crystal
pka: 16.78±0.30(Predicted)
color: White to Light yellow to Light orange
InChI: InChI=1S/C24H16N2/c1-2-8-16(9-3-1)26-22-13-7-5-11-18(22)20-15-14-19-17-10-4-6-12-21(17)25-23(19)24(20)26/h1-15,25H
InChIKey: IENOQUQIVSMWGP-UHFFFAOYSA-N
SMILES: N1C2=C(C=CC=C2)C2=C1C1N(C3=CC=CC=C3)C3=C(C=1C=C2)C=CC=C3
CAS DataBase Reference: 1024598-06-8

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Safety

HS Code: 2933.99.8290

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4860
Product name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Purity: >97.0%(HPLC)(N)
Packaging: 200mg
Price: $98
Updated: 2025/07/31

TCI Chemical

Product number: D4860
Product name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Purity: >97.0%(HPLC)(N)
Packaging: 1g
Price: $293
Updated: 2025/07/31

TRC

Product number: P321190
Product name: 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole
Packaging: 50mg
Price: $90
Updated: 2021/12/16

TRC

Product number: P321190
Product name: 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole
Packaging: 100mg
Price: $130
Updated: 2021/12/16

AK Scientific

Product number: 4717AL
Product name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole
Packaging: 5g
Price: $313
Updated: 2021/12/16

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11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Chemical Properties,Usage,Production

Synthesis

108-86-1

60511-85-5

1024598-06-8

General procedure for the synthesis of 11,12-dihydro-11-phenylindolo[2,3-a]carbazole from bromobenzene and 11,12-dihydroindolo[2,3-a]carbazole: Pd2(dba)3 (178.6 mg, 0.20 mmol) and t-Bu3P (78.9 mg, 0.39 mmol) were mixed with Pd2(dba)3 (178.6 mg, 0.20 mmol) and t-Bu3P (78.9 mg, 0.39 mmol) in o-xylene (50 mL) at room temperature under stirred for 10 min. Subsequently, 11,12-dihydroindolo[2,3-a]carbazole (Intermediate I-1, 5 g, 19.51 mmol), bromobenzene (3.37 g, 21.46 mmol), and t-BuONa (1.12 g, 11.71 mmol) were added and stirred at reflux for 48 hours at 160 °C. After completion of the reaction, it was cooled to room temperature, distilled water (20 mL) was added and extracted with ethyl acetate. The organic phase was dried over magnesium sulfate, filtered and the solvent evaporated. Purification by column chromatography afforded 11,12-dihydro-11-phenylindolo[2,3-a]carbazole (Intermediate I-2, 5.35 g, 83% yield).MS-EI, m/e: 332.13 (calculated), 332.19 (measured).

References

[1] Patent: KR2015/96018, 2015, A. Location in patent: Paragraph 0377-0379
[2] Patent: US2018/90690, 2018, A1. Location in patent: Paragraph 0161; 0162
[3] Patent: KR2018/32519, 2018, A. Location in patent: Paragraph 0120-0122
[4] Patent: EP2894157, 2015, A1. Location in patent: Paragraph 0198
[5] Patent: KR2015/84657, 2015, A. Location in patent: Paragraph 1642-1645

11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Suppliers

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View Lastest Price from 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole 1024598-06-8
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-10-14

Henan Fengda Chemical Co., Ltd

Product: 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole 1024598-06-8
Price: US $188.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-05

LY Global chemicals co.,ltd .

Product: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole 1024598-06-8
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%Min
Supply Ability: 1000kg
Release date: 2023-03-12

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1024598-06-8