7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde
- Product Name
- 7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde
- CAS No.
- 1060815-89-5
- Chemical Name
- 7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde
- Synonyms
- 7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde;7H-Pyrrolo[2,3-d]pyrimidine-5-carboxaldehyde;7H-Pyrrolo[2,3-d]pyrimidine-5-carbaldehyde 98%
- CBNumber
- CB02614737
- Molecular Formula
- C7H5N3O
- Formula Weight
- 147.13
- MOL File
- 1060815-89-5.mol
7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde Property
- Density
- 1.471±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 10.58±0.50(Predicted)
- Appearance
- Off-white to yellow Solid
Safety
- HS Code
- 2933599590
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H303May be harmfulif swallowed
H320Causes eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- B529865
- Product name
- 7H-Pyrrolo[2,3-d]pyrimidine-5-carbaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B529865
- Product name
- 7H-Pyrrolo[2,3-d]pyrimidine-5-carbaldehyde
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- OR301310
- Product name
- 7H-Pyrrolo[2,3-d]pyrimidine-5-carbaldehyde
- Packaging
- 250mg
- Price
- $103
- Updated
- 2021/12/16
- Product number
- 125115
- Product name
- 7H-Pyrrolo[2,3-d]pyrimidine-5-carboxaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $479
- Updated
- 2021/12/16
- Product number
- 1387AA
- Product name
- 7H-Pyrrolo[2,3-d]pyrimidine-5-carbaldehyde
- Packaging
- 1g
- Price
- $167
- Updated
- 2021/12/16
7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde Chemical Properties,Usage,Production
Synthesis
100-97-0
271-70-5
1060815-89-5
Under nitrogen protection, 7H-pyrrolo[2,3-d]pyrimidine (6 g, 50.4 mmol) and hexamethylenetetetramine (10.59 g, 76 mmol) were dissolved in a mixed solvent of acetic acid (20.00 mL) and water (40 mL). The reaction mixture was heated to reflux temperature with continuous stirring for 8 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the solid product was collected by filtration. The solid was washed three times with ether to remove impurities. After drying, 5.6 g of 7H-pyrrolo[2,3-d]pyrimidine-5-carbaldehyde was obtained in 76% yield. The product was analyzed by ESI-MS (+) showing m/z 148.1 [M+H]+. 1H NMR (methanol-d4) data were as follows: δ 10.00 (s, 1H), 9.43 (s, 1H), 8.91 (s, 1H), 8.40 (s, 1H).
References
[1] Patent: WO2017/176608, 2017, A1. Location in patent: Page/Page column 130; 131
[2] Patent: WO2012/2568, 2012, A1. Location in patent: Page/Page column 37
7H-pyrrolo[2,3-d]pyriMidine-5-carbaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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