N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE

Product Name: N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE
CAS No.: 287953-54-2
Chemical Name: N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE
Synonyms: N-CBZ-4-PIPERIDINE SULFONYL CHLORIDE;N-Cbz-piperidine-4-sulfonyl Chloride;4-(CHLOROSULFONYL)PIPERIDINE-1-CARBOXYLATE;benzyl-chlorosulfonylpiperidine-1-carboxylate;PIPERIDINE-4-SULFONYL CHLORIDE, N-CBZ PROTECTED;Piperidine-4-sulphonyl chloride, N-CBZ protected;benzyl 4-(chlorosulfonyl)piperidine-1-carboxylate;N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE;N-BENZOYLOXYCARBONYL-4-PIPERIDINE SULFONYL CHLORIDE;1-(Benzyloxycarbonyl)-4-piperidinesulfonyl chloride
CBNumber: CB0276364
Molecular Formula: C13H16ClNO4S
Formula Weight: 317.79
MOL File: 287953-54-2.mol

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N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE Property

Boiling point:: 454.9±44.0 °C(Predicted)
Density: 1.39±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -3.77±0.40(Predicted)
form: powder
color: Light beige/beige
CAS DataBase Reference: 287953-54-2(CAS DataBase Reference)

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Safety

Hazard Codes: C,Xi
Risk Statements: 43
Safety Statements: 36/37
Hazard Note: Corrosive
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

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N-Bromosuccinimide Price

TRC

Product number: B287410
Product name: N-Benzyloxycarbonyl-4-piperidinesulfonylchloride
Packaging: 500mg
Price: $110
Updated: 2021/12/16

AK Scientific

Product number: H435
Product name: N-Benzyloxycarbonyl-4-piperidinesulfonylchloride
Packaging: 1g
Price: $134
Updated: 2021/12/16

Apolloscientific

Product number: OR4649
Product name: Piperidine-4-sulphonylchloride,N-CBZprotected
Packaging: 1g
Price: $99
Updated: 2021/12/16

Apolloscientific

Product number: OR4649
Product name: Piperidine-4-sulphonylchloride,N-CBZprotected
Packaging: 500mg
Price: $57
Updated: 2021/12/16

Matrix Scientific

Product number: 119555
Product name: Benzyl 4-(chlorosulfonyl)piperidine-1-carboxylate
Purity: 95+%
Packaging: 1g
Price: $270
Updated: 2021/12/16

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N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE Chemical Properties,Usage,Production

Synthesis

146827-60-3

287953-54-2

General procedure for the synthesis of N-Benzyloxycarbonyl-4-piperidinesulfonyl chloride from benzyl 4-(acetylthio)piperidine-1-carboxylate: Benzyl 4-(acetylthio)piperidine-1-carboxylate (1.45 g, 4.94 mmol) was dissolved in a mixed solvent of dichloromethane (10 mL) and water (40 mL), and the reaction was stirred for 4 hours at 0 °C, while chlorine was passed through the reaction. After completion of the reaction, the organic layer was separated and the aqueous layer was extracted with dichloromethane. The organic layers were combined, dried with anhydrous magnesium sulfate, and concentrated under reduced pressure to remove the solvent to afford benzyl 4-(chlorosulfonyl)-1-piperidinecarboxylate (1.58 g, 100% yield).

References

[1] Patent: EP1403255, 2004, A1. Location in patent: Page 90
[2] Synthesis, 2011, # 22, p. 3669 - 3674
[3] Patent: WO2003/103669, 2003, A1. Location in patent: Page 44-45

N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE Suppliers

China 70 Germany 2 India 4 United Kingdom 1 United States 19 Global 96

J & K SCIENTIFIC LTD.

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View Lastest Price from N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE 287953-54-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: N-Cbz-4-piperidine sulfonyl chloride 287953-54-2
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-08-07

287953-54-2, N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDERelated Search:

N-CYCLOHEXYL-GUANIDINE 4-Benzyl-morpholin-2-one N-benzyl-2-broMo-2-MethylpropanaMide N-Cyclopentyl-guanidine hydrochloride N-phenylpiperidin-4-amine PICOLINIC ANILIDE N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE ISOPROPYLSULFONYL CHLORIDE

Benzyl 4-(chlorosulfonyl)tetrahydro-1(2H)-pyridinecarboxylate

1-PIPERIDINECARBOXYLIC ACID, 4-(CHLOROSULFONYL)-,PHENYLMETHYL ESTER

benzyl 4-(chlorosulfonyl)piperidine-1-carboxylate

4-CHLOROSULFONYL-PIPERIDINE-1-CARBOXYLIC ACID BENZYL ESTER

Piperidine-4-sulphonyl chloride, N-CBZ protected

N-[(Benzyloxy)carbonyl]piperidine-4-sulphonyl chloride, Benzyl 4-(chlorosulphonyl)piperidine-1-carboxylate

N-CBZ-4-PIPERIDINE SULFONYL CHLORIDE

PIPERIDINE-4-SULFONYL CHLORIDE, N-CBZ PROTECTED

N-BENZOYLOXYCARBONYL-4-PIPERIDINE SULFONYL CHLORIDE

N-(BENZYLOXYCARBONYL)-PIPERIDINE-4-SULPHONYL CHLORIDE

N-BENZYLOXYCARBONYL-4-PIPERIDINESULFONYL CHLORIDE

1-(Benzyloxycarbonyl)-4-piperidinesulfonyl chloride

4-chlorosulfonyl-1-piperidinecarboxylic acid (phenylmethyl) ester

N-Cbz-piperidine-4-sulfonyl Chloride

Benzyl 4-(chlorosulfonyl)tetrahydro-1(2H)-pyridinecarboxylat...

benzyl-chlorosulfonylpiperidine-1-carboxylate

Phenylmethyl 4-(chlorosulfonyl)-1-piperidinecarboxylate

4-(CHLOROSULFONYL)PIPERIDINE-1-CARBOXYLATE

287953-54-2

C13H16ClNO4S

C13H16NO4ClS