4-BROMO-2-CHLOROACETANILIDE
- Product Name
- 4-BROMO-2-CHLOROACETANILIDE
- CAS No.
- 3460-23-9
- Chemical Name
- 4-BROMO-2-CHLOROACETANILIDE
- Synonyms
- BUTTPARK 83\07-60;SALOR-INT L168270-1EA;4-BROMO-2-CHLOROACETANILIDE;2-chloro-4-bromo acetanilide;2-chloro-4-bromo acetanillide;4'-Bromo-2'-chloroacetanilide;2-Chloro-4-bromophenylacetamide;4'-Bromo-2'-chloroacetanilide >4-Bromo-2-chloroacetanilide, 98+%;4'-Bromo-2'-chloro-N-phenylacetamide
- CBNumber
- CB0286695
- Molecular Formula
- C8H7BrClNO
- Formula Weight
- 248.5
- MOL File
- 3460-23-9.mol
4-BROMO-2-CHLOROACETANILIDE Property
- Melting point:
- 151-152°C
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Soluble in hot methanol (very faint turbidity).
- form
- powder to crystal
- color
- White to Light yellow
- BRN
- 2719133
- CAS DataBase Reference
- 3460-23-9
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-22
- Safety Statements
- 26-37
- HS Code
- 2924297099
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- B2413
- Product name
- 4'-Bromo-2'-chloroacetanilide
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $44
- Updated
- 2025/07/31
- Product number
- B2413
- Product name
- 4'-Bromo-2'-chloroacetanilide
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $151
- Updated
- 2025/07/31
- Product number
- B124915
- Product name
- N-(4-Bromo-2-chlorophenyl)acetamide
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4648-D-02
- Product name
- 4-Bromo-2-chloroacetanilide
- Packaging
- 25g
- Price
- $176
- Updated
- 2021/12/16
- Product number
- X5258
- Product name
- 4-Bromo-2-chloroacetanilide
- Packaging
- 100g
- Price
- $308
- Updated
- 2021/12/16
4-BROMO-2-CHLOROACETANILIDE Chemical Properties,Usage,Production
Uses
It is employed as a intermediate for pharmaceutical.
Synthesis
533-17-5
3460-23-9
General procedure for the synthesis of 4-bromo-2-chloro-N-acetylaniline from N-(2-chlorophenyl)acetamide: 1. HBr (40% aqueous, 0.08 mL, 0.55 mmol) was added to a stirred suspension of N-(2-chlorophenyl)acetamide (75 mg, 0.5 mmol) and Selectfluor (213 mg, 0.6 mmol) in water (3.0 mL). 2. the mixture was stirred at room temperature for 5 minutes until the ingredients were completely consumed (monitored by TLC). 3. Upon completion of the reaction, the reaction was quenched with saturated Na2S2O3 aqueous solution (2.0 mL) and water (20.0 mL). 4. The organic phase was extracted three times with CH2Cl2 (10.0 mL) and combined. 5. After evaporation of the solvent, the residue obtained was purified by silica gel column chromatography (eluent: petroleum ether-ethyl acetate=6:1, v/v) to afford 4-bromo-2-chloro-N-acetylaniline as a white solid (108 mg, 95% yield).
References
[1] Chemistry - A European Journal, 2017, vol. 23, # 5, p. 1044 - 1047
[2] Tetrahedron Letters, 2016, vol. 57, # 48, p. 5390 - 5394
[3] Journal of Chemical Research, Synopses, 1997, # 11, p. 432 - 433
[4] European Journal of Organic Chemistry, 2018, vol. 2018, # 43, p. 5972 - 5979
[5] Gazzetta Chimica Italiana, 1908, vol. 38 II, p. 22
4-BROMO-2-CHLOROACETANILIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-BROMO-2-CHLOROACETANILIDE manufacturers
- Product
- 4-BROMO-2-CHLOROACETANILIDE 3460-23-9
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2024-11-07
- Product
- 4-BROMO-2-CHLOROACETANILIDE 3460-23-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 2000
- Release date
- 2025-04-17
- Product
- 4-BROMO-2-CHLOROACETANILIDE 3460-23-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-01