ChemicalBook > CAS DataBase List > 4-BROMO-2-CHLOROACETANILIDE

4-BROMO-2-CHLOROACETANILIDE

Product Name
4-BROMO-2-CHLOROACETANILIDE
CAS No.
3460-23-9
Chemical Name
4-BROMO-2-CHLOROACETANILIDE
Synonyms
BUTTPARK 83\07-60;SALOR-INT L168270-1EA;4-BROMO-2-CHLOROACETANILIDE;2-chloro-4-bromo acetanilide;2-chloro-4-bromo acetanillide;4'-Bromo-2'-chloroacetanilide;2-Chloro-4-bromophenylacetamide;4'-Bromo-2'-chloroacetanilide >4-Bromo-2-chloroacetanilide, 98+%;4'-Bromo-2'-chloro-N-phenylacetamide
CBNumber
CB0286695
Molecular Formula
C8H7BrClNO
Formula Weight
248.5
MOL File
3460-23-9.mol
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4-BROMO-2-CHLOROACETANILIDE Property

Melting point:
151-152°C
storage temp. 
Sealed in dry,Room Temperature
solubility 
Soluble in hot methanol (very faint turbidity).
form 
powder to crystal
color 
White to Light yellow
BRN 
2719133
CAS DataBase Reference
3460-23-9
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-22
Safety Statements 
26-37
HS Code 
2924297099
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B2413
Product name
4'-Bromo-2'-chloroacetanilide
Purity
>98.0%(GC)
Packaging
5g
Price
$44
Updated
2025/07/31
TCI Chemical
Product number
B2413
Product name
4'-Bromo-2'-chloroacetanilide
Purity
>98.0%(GC)
Packaging
25g
Price
$151
Updated
2025/07/31
TRC
Product number
B124915
Product name
N-(4-Bromo-2-chlorophenyl)acetamide
Packaging
100mg
Price
$60
Updated
2021/12/16
SynQuest Laboratories
Product number
4648-D-02
Product name
4-Bromo-2-chloroacetanilide
Packaging
25g
Price
$176
Updated
2021/12/16
AK Scientific
Product number
X5258
Product name
4-Bromo-2-chloroacetanilide
Packaging
100g
Price
$308
Updated
2021/12/16
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4-BROMO-2-CHLOROACETANILIDE Chemical Properties,Usage,Production

Uses

It is employed as a intermediate for pharmaceutical.

Synthesis

533-17-5

3460-23-9

General procedure for the synthesis of 4-bromo-2-chloro-N-acetylaniline from N-(2-chlorophenyl)acetamide: 1. HBr (40% aqueous, 0.08 mL, 0.55 mmol) was added to a stirred suspension of N-(2-chlorophenyl)acetamide (75 mg, 0.5 mmol) and Selectfluor (213 mg, 0.6 mmol) in water (3.0 mL). 2. the mixture was stirred at room temperature for 5 minutes until the ingredients were completely consumed (monitored by TLC). 3. Upon completion of the reaction, the reaction was quenched with saturated Na2S2O3 aqueous solution (2.0 mL) and water (20.0 mL). 4. The organic phase was extracted three times with CH2Cl2 (10.0 mL) and combined. 5. After evaporation of the solvent, the residue obtained was purified by silica gel column chromatography (eluent: petroleum ether-ethyl acetate=6:1, v/v) to afford 4-bromo-2-chloro-N-acetylaniline as a white solid (108 mg, 95% yield).

References

[1] Chemistry - A European Journal, 2017, vol. 23, # 5, p. 1044 - 1047
[2] Tetrahedron Letters, 2016, vol. 57, # 48, p. 5390 - 5394
[3] Journal of Chemical Research, Synopses, 1997, # 11, p. 432 - 433
[4] European Journal of Organic Chemistry, 2018, vol. 2018, # 43, p. 5972 - 5979
[5] Gazzetta Chimica Italiana, 1908, vol. 38 II, p. 22

4-BROMO-2-CHLOROACETANILIDE Preparation Products And Raw materials

Raw materials

Acetyl chloride Chloroform Bromine Dichloromethane 2-Chloroaniline Hexamethylenetetramine

Preparation Products

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4-BROMO-2-CHLOROACETANILIDE Suppliers

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View Lastest Price from 4-BROMO-2-CHLOROACETANILIDE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd
Product
4-BROMO-2-CHLOROACETANILIDE 3460-23-9
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2024-11-07
Shenzhen Nexcon Pharmatechs Ltd.
Product
4-BROMO-2-CHLOROACETANILIDE 3460-23-9
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
2000
Release date
2025-04-17
Shaanxi Dideu Medichem Co. Ltd
Product
4-BROMO-2-CHLOROACETANILIDE 3460-23-9
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-08-01

3460-23-9, 4-BROMO-2-CHLOROACETANILIDERelated Search:

2-Chloro-N-phenylacetamide 2'-Chloroacetanilide 4-BROMO-2-CHLOROACETANILIDE,4-BROMO-W-CHLOROACETANILIDE 2'-BROMO-4'-CHLOROACETANILIDE 4-BROMO-3-CHLOROACETANILIDE,4'-BROMO-3'-CHLOROACETANILIDE N-(4-bromo-2-chlorophenyl)-3-oxobutanamide 4-BROMO-2-CHLOROACETANILIDE N-(4-BROMO-2-CHLOROPHENYL)-2-CHLOROACETAMIDE BUTTPARK 50\07-87 N-(4-BROMO-2,6-DICHLOROPHENYL)ACETAMIDE 1-(4-BROMO-2-CHLORO-PHENYL)-PIPERIDIN-2-ONE 4-(4-BROMO-2-CHLOROANILINO)-4-OXOBUT-2-ENOIC ACID N-(4-BROMO-2-CHLOROPHENYL)MALEAMIC ACID N1-(4-BROMO-2-CHLOROPHENYL)-2-BROMOPROPANAMIDE

  • SALOR-INT L168270-1EA
  • 4-BROMO-2-CHLOROACETANILIDE
  • 4-Bromo-2-chloroacetanilide, 98+%
  • 4'-Bromo-2'-chloro-N-phenylacetamide
  • BUTTPARK 83\07-60
  • 4'-Bromo-2'-chloroacetanilide &gt
  • Acetamide, N-(4-bromo-2-chlorophenyl)-
  • 2-chloro-4-bromo acetanillide
  • 2-chloro-4-bromo acetanilide
  • 4'-Bromo-2'-chloroacetanilide
  • 2-Chloro-4-bromophenylacetamide
  • 4′-Bromo-2′-chloroacetanilide, CAS 3460-23-9
  • 3460-23-9
  • 2564-2-5
  • Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts
  • Anilines, Amides & Amines
  • Bromine Compounds
  • Chlorine Compounds