ChemicalBook > CAS DataBase List > (-)-Camphanic acid chloride

(-)-Camphanic acid chloride

Product Name
(-)-Camphanic acid chloride
CAS No.
39637-74-6
Chemical Name
(-)-Camphanic acid chloride
Synonyms
(+)-(1R,4S)-camphani;(-)-CAMPHANIC CHLORIDE;(-)-Camphanic Chloride;(-)-Camphanoyl chloride;(1S)-(-)CAMPHANYL CHLORIDE;(-)-Camphanic Chloride >(-)-CAMPHANIC ACID CHLORIDE;(1S)-(-)-CAMPHANIC CHLORIDE;(1S)-(-)-CAMPHANOYL CHLORIDE;(S)-(-)-1-CAMPHANYL CHLORIDE
CBNumber
CB0352910
Molecular Formula
C10H13ClO3
Formula Weight
216.66
MOL File
39637-74-6.mol
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(-)-Camphanic acid chloride Property

Melting point:
71-73 °C(lit.)
alpha 
-18 º (c=2, CCl4)
Boiling point:
310.92°C (rough estimate)
Density 
1.2072 (rough estimate)
refractive index 
1.5390 (estimate)
storage temp. 
2-8°C
solubility 
soluble in Dichloromethane, Ether, Ethyl Acetate, Methanol
form 
Powder
color 
Yellow to orange-brown
optical activity
[α]23/D 18°, c = 2 in carbon tetrachloride
Water Solubility 
decomposes
Sensitive 
Moisture Sensitive
BRN 
3590860
InChIKey
PAXWODJTHKJQDZ-RGURZIINSA-N
CAS DataBase Reference
39637-74-6(CAS DataBase Reference)
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Safety

Hazard Codes 
C,Xi
Risk Statements 
34-29
Safety Statements 
26-36/37/39-45-8-27
RIDADR 
UN 3261 8/PG 2
WGK Germany 
3
F 
10-21
HazardClass 
8
PackingGroup 
II
HS Code 
29322090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P363Wash contaminated clothing before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
21287
Product name
(1S)-(−)-Camphanic chloride
Purity
for chiral derivatization, LiChropur?, ≥98.0%
Packaging
5G
Price
$274
Updated
2022/05/15
Sigma-Aldrich
Product number
21287
Product name
(1S)-(−)-Camphanic chloride
Purity
for chiral derivatization, LiChropur?, ≥98.0%
Packaging
25g
Price
$1080
Updated
2022/05/15
TCI Chemical
Product number
C1022
Product name
(-)-Camphanic Chloride
Purity
>97.0%(T)
Packaging
1g
Price
$86
Updated
2024/03/01
TCI Chemical
Product number
C1022
Product name
(-)-Camphanic Chloride
Purity
>97.0%(T)
Packaging
5g
Price
$251
Updated
2024/03/01
Alfa Aesar
Product number
L14148
Product name
(1S)-(-)-Camphanic chloride, 95%
Packaging
1g
Price
$41.65
Updated
2024/03/01
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(-)-Camphanic acid chloride Chemical Properties,Usage,Production

Chemical Properties

Off-White Powder

Uses

An optically active resolving agent

Uses

(1S)-(-)-Camphanic chloride is used as a resolving agent for alcohols as the diastereomeric esters by crystallization or chromatography and as a chiral derivatization reagent for determination of enantiomeric excess of alcohols and amines.

Uses

(1S)-(-)-Camphanic chloride may be used in esterification of enantiomers in volatiles releasedf from wheat, in order to determine the proportion of enantiomers and also in quantifying the esters.

General Description

(1S)-(-)-Camphanic chloride is a chiral derivatizing agent. It can be prepared by reacting (-)-(1S,4R)-camphanic acid with thionyl chloride.

Purification Methods

It is soluble in toluene (50g/100mL at 0o) and crystallises from pet ether (b 40-60o). It sublimes at 70o/5mm, Store it dry at 0o, max (CCl4) 1805s and 1780m cm-1. Armarego et al. J Chem Soc, Perkin Trans I 2229 1976, Gerlach Helv Chim Acta 51 1587 1968, Gerlach Helv Chim Acta 68 1815 1985, Beilstein 18/8 V 101.]

(-)-Camphanic acid chloride Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (-)-Camphanic acid chloride manufacturers

Zibo Hangyu Biotechnology Development Co., Ltd
Product
(-)-Camphanic acid chloride 39637-74-6
Price
US $1.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
50000kg/month
Release date
2024-08-28
Hebei Weibang Biotechnology Co., Ltd
Product
(-)-Camphanic acid chloride 39637-74-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2022-11-17
Hebei Mojin Biotechnology Co., Ltd
Product
(-)-Camphanic acid chloride 39637-74-6
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-08-17

39637-74-6, (-)-Camphanic acid chlorideRelated Search:

Isovaleryl chloride 4-Methylvaleryl chloride (-)-Camphanic acid chloride 1-CHLORO-3,3-DIMETHYLBUTANE 4-Butoxyphenol 3-METHYLPENTANOYL CHLORIDE 6-Chlorohexanol 2-(CHLOROMETHYL)TETRAHYDROPYRAN Cyclopentanecarbonyl chloride ALPHA,ALPHA-DIMETHYL-GAMMA-BUTYROLACTONE 2-METHYLVALERYL CHLORIDE 1-Pentanol Acetoxyacetyl chloride Heptanoyl chloride DIHYDRO-4,4-DIMETHYL-2(3H)-FURANONE Tetrahydrofurfuryl chloride (S)-(-)-2-ACETOXYPROPIONYL CHLORIDE 2-Ethylbutyryl chloride

  • (-)-CAMPHANIC ACID CHLORIDE
  • (-)-CAMPHANIC CHLORIDE
  • (1S)-(-)-Camphanicacidchloride
  • 3-oxa-2-oxobornane-4-carbonyl chloride
  • (1S)-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carbonyl chlorid
  • (1S)-(-)-Camphanicchloride,95%
  • (1S,4R)-(-)-Camphanic chloride
  • (1S)-(-)-Camphanic chloride, 98% (99% EE)
  • (-)-CAMPHANIC ACID CHLORIDE 98%
  • 4,7,7-trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carbonyl chloride
  • (+)-(1R,4S)-Camphanoyl chloride
  • 2-Oxabicyclo2.2.1heptane-1-carbonyl chloride, 4,7,7-trimethyl-3-oxo-, (1S,4R)-
  • (-)-Camphanoyl chloride
  • (-)-Camphanoyl chloride, (1S)-3-Oxo-4,7,7-trimethyl-2-oxabicyclo[2.2.1]heptane-1-carbonyl chloride
  • 2-Oxabicyclo[2.2.1]heptane-1-carbonyl chloride, 4,7,7-trimethyl-3-oxo-, (1S)-
  • (1S,4R)-3-Oxo-4,7,7-trimethyl-2-oxabicyclo[2.2.1]heptane-1-carboxylic acid chloride
  • (1S,4R)-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carboxylic acid chloride
  • [1S,4R,(-)]-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carbonyl chloride
  • [1S,4R,(-)]-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carboxylic acid chloride
  • (-)-Camphanic acid chloride,98%
  • (+)-(1R,4S)-camphani
  • (-)-Camphanoyl chloride (-)-Camphanic acid chloride
  • (1S)-(-)-Camphanic chloride 98%
  • (1S)-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carbonyl chloride
  • [1S]-3-OXO-4,7,7-TRIMETHYL-2-OXABICYCLO[2.2.1]HEPTANE-1-CARBONYL CHLORIDE
  • (1S)-3-OXO-4,7,7-TRIMETHYL-2-OXABICYCLO[2.2.1]HEPTANE-1-CARBOXYL CHLORIDE
  • (1S)-(-)-CAMPHANIC CHLORIDE
  • (1S)-(-)-CAMPHANOYL CHLORIDE
  • (1S)-(-)CAMPHANYL CHLORIDE
  • (-)-(1S,4R)-CAMPHANOYL CHLORIDE
  • (IS)-(-)-Camphenic acid chloride
  • (-)-CaMphanic acid chloride, 98% 1GR
  • (S)-(-)-1-CAMPHANYL CHLORIDE
  • (-)-Camphanic Chloride &gt
  • (-)-Camphanic acid chloride, 98%, reagent grade
  • (1S)-4,7,7-Trimethyl-3-oxo-2-oxabicyclo[2.2.1]heptane-1-carbonyl chloride(Chunks or pellets)
  • TIANFU-CHEM (-)-Camphanic Chloride
  • (4S)-1,7,7-trimethyl-2-oxo-3-oxabicyclo[2.2.1]heptane-4-carbonyl chloride
  • (-)-Camphanic Chloride
  • (-)-(1S,4R)-Camphanoyl Chloride
  • 39637-74-6
  • C10H13ClO3
  • C10H13O3Cl
  • Analytical Chromatography Product Catalog
  • Asymmetric Synthesis
  • Organic Building Blocks
  • Acid Halides
  • Derivatization Reagents
  • Bicyclic Monoterpenes
  • Terpenes
  • for Resolution of Alcohols & Thiols
  • Optical Resolution
  • ACID CHLORIDE
  • Chiral Building Blocks
  • Chiral Derivatization
  • Chiral Reagents
  • Chiral Compound
  • FINE Chemical & INTERMEDIATES