(4-METHOXY-2-NITROPHENYL)ACETONITRILE
- Product Name
- (4-METHOXY-2-NITROPHENYL)ACETONITRILE
- CAS No.
- 105003-90-5
- Chemical Name
- (4-METHOXY-2-NITROPHENYL)ACETONITRILE
- Synonyms
- 4-METHOXY-2-NITRO-CYANOMETHYLBENZENE;(4-METHOXY-2-NITROPHENYL)ACETONITRILE;Benzeneacetonitrile, 4-methoxy-2-nitro-;2-(4-Methoxy-2-nitrophenyl)acetonitrile
- CBNumber
- CB0361466
- Molecular Formula
- C9H8N2O3
- Formula Weight
- 192.17
- MOL File
- 105003-90-5.mol
(4-METHOXY-2-NITROPHENYL)ACETONITRILE Property
- storage temp.
- Sealed in dry,Room Temperature
N-Bromosuccinimide Price
- Product number
- M340060
- Product name
- 2-(4-Methoxy-2-nitrophenyl)acetonitrile
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 1174AA
- Product name
- 2-(4-Methoxy-2-nitrophenyl)acetonitrile
- Packaging
- 1g
- Price
- $448
- Updated
- 2021/12/16
- Product number
- 126775
- Product name
- 2-(4-Methoxy-2-nitrophenyl)acetonitrile
- Purity
- >95%
- Packaging
- 1g
- Price
- $630
- Updated
- 2021/12/16
- Product number
- CHM0094263
- Product name
- (4-METHOXY-2-NITROPHENYL)-ACETONITRILE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1030.84
- Updated
- 2021/12/16
- Product number
- 10R0276
- Product name
- (4-Methoxy-2-nitro-phenyl)-acetonitrile
- Purity
- 97%
- Packaging
- 5g
- Price
- $1992
- Updated
- 2021/12/16
(4-METHOXY-2-NITROPHENYL)ACETONITRILE Chemical Properties,Usage,Production
Synthesis
65547-98-0
105003-90-5
General procedure for the synthesis of (4-methoxy-2-nitrophenyl)acetonitrile from the compound (CAS: 65547-98-0): an aqueous solution of compound S2 (4.5 g, 17.05 mmol) was mixed with Na2CO3 (30 mL, 1N) and stirred for 40 h at room temperature. After completion of the reaction, the mixture was extracted with EtOAc (50 mL). The organic layer was sequentially washed with brine, dried over Na2SO4, filtered and concentrated to dryness. The residue was purified by silica gel column chromatography with EtOAc/petroleum ether (1:5) as eluent to give compound S3 (2.5 g, 76.2% yield) as a light yellow solid.
References
[1] Patent: WO2017/35411, 2017, A1. Location in patent: Paragraph 0647
[2] Patent: US2011/230461, 2011, A1. Location in patent: Page/Page column 32
[3] Patent: WO2005/26128, 2005, A1. Location in patent: Page/Page column 17-18
[4] Patent: WO2006/20003, 2006, A2. Location in patent: Page/Page column 18
[5] Patent: US2004/97575, 2004, A1. Location in patent: Page 11
(4-METHOXY-2-NITROPHENYL)ACETONITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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