(4-METHOXY-2-NITROPHENYL)ACETONITRILE

Product Name: (4-METHOXY-2-NITROPHENYL)ACETONITRILE
CAS No.: 105003-90-5
Chemical Name: (4-METHOXY-2-NITROPHENYL)ACETONITRILE
Synonyms: 4-METHOXY-2-NITRO-CYANOMETHYLBENZENE;(4-METHOXY-2-NITROPHENYL)ACETONITRILE;Benzeneacetonitrile, 4-methoxy-2-nitro-;2-(4-Methoxy-2-nitrophenyl)acetonitrile
CBNumber: CB0361466
Molecular Formula: C9H8N2O3
Formula Weight: 192.17
MOL File: 105003-90-5.mol

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(4-METHOXY-2-NITROPHENYL)ACETONITRILE Property

storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H332Harmful if inhaled

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M340060
Product name: 2-(4-Methoxy-2-nitrophenyl)acetonitrile
Packaging: 50mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: 1174AA
Product name: 2-(4-Methoxy-2-nitrophenyl)acetonitrile
Packaging: 1g
Price: $448
Updated: 2021/12/16

Matrix Scientific

Product number: 126775
Product name: 2-(4-Methoxy-2-nitrophenyl)acetonitrile
Purity: >95%
Packaging: 1g
Price: $630
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0094263
Product name: (4-METHOXY-2-NITROPHENYL)-ACETONITRILE
Purity: 95.00%
Packaging: 1G
Price: $1030.84
Updated: 2021/12/16

J&W Pharmlab

Product number: 10R0276
Product name: (4-Methoxy-2-nitro-phenyl)-acetonitrile
Purity: 97%
Packaging: 5g
Price: $1992
Updated: 2021/12/16

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(4-METHOXY-2-NITROPHENYL)ACETONITRILE Chemical Properties,Usage,Production

Synthesis

65547-98-0

105003-90-5

General procedure for the synthesis of (4-methoxy-2-nitrophenyl)acetonitrile from the compound (CAS: 65547-98-0): an aqueous solution of compound S2 (4.5 g, 17.05 mmol) was mixed with Na2CO3 (30 mL, 1N) and stirred for 40 h at room temperature. After completion of the reaction, the mixture was extracted with EtOAc (50 mL). The organic layer was sequentially washed with brine, dried over Na2SO4, filtered and concentrated to dryness. The residue was purified by silica gel column chromatography with EtOAc/petroleum ether (1:5) as eluent to give compound S3 (2.5 g, 76.2% yield) as a light yellow solid.

References

[1] Patent: WO2017/35411, 2017, A1. Location in patent: Paragraph 0647
[2] Patent: US2011/230461, 2011, A1. Location in patent: Page/Page column 32
[3] Patent: WO2005/26128, 2005, A1. Location in patent: Page/Page column 17-18
[4] Patent: WO2006/20003, 2006, A2. Location in patent: Page/Page column 18
[5] Patent: US2004/97575, 2004, A1. Location in patent: Page 11

(4-METHOXY-2-NITROPHENYL)ACETONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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(4-METHOXY-2-NITROPHENYL)ACETONITRILE Suppliers

China 21 Germany 1 India 2 United Kingdom 1 United States 7 Global 32

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105003-90-5, (4-METHOXY-2-NITROPHENYL)ACETONITRILERelated Search:

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4-METHOXY-2-NITRO-CYANOMETHYLBENZENE

(4-METHOXY-2-NITROPHENYL)ACETONITRILE

2-(4-Methoxy-2-nitrophenyl)acetonitrile

Benzeneacetonitrile, 4-methoxy-2-nitro-

105003-90-5