2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE
- Product Name
- 2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE
- CAS No.
- 198205-95-7
- Chemical Name
- 2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE
- Synonyms
- AKOS BAR-1774;4-[2-(TRIFLUOROMETHYL)PHENYL]BENZALDEHYDE;2'-trifluoromethyl diphenyl-4-carbaldehyde;2'-Trifluoromethyl-biphenyl-4-carbaldehyde;2'-(TRIFLUOROMETHYL)[1,1'-BIPHENYL]-4-CARBALDEHYDE;2'-(Trifluoromethyl)-[1,1'-biphenyl]-4-carbaldehyde;2'-(Trifluoromethyl)[1,1'-biphenyl]-4-carboxaldehyde;[1,1'-Biphenyl]-4-carboxaldehyde, 2'-(trifluoromethyl)-;2′-Trifluoromethyl-biphenyl-4-carbaldehyde, CAS 198205-95-7
- CBNumber
- CB0381341
- Molecular Formula
- C14H9F3O
- Formula Weight
- 250.22
- MOL File
- 198205-95-7.mol
2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE Property
- Boiling point:
- 338.8±42.0 °C(Predicted)
- Density
- 1.251±0.06 g/cm3(Predicted)
- CAS DataBase Reference
- 198205-95-7(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- T797218
- Product name
- 2''-(Trifluoromethyl)-[1,1''-biphenyl]-4-carbaldehyde
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- T797218
- Product name
- 2''-(Trifluoromethyl)-[1,1''-biphenyl]-4-carbaldehyde
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 291331
- Product name
- 2'-Trifluoromethylbiphenyl-4-carbaldehyde
- Packaging
- 250mg
- Price
- $340
- Updated
- 2021/12/16
- Product number
- W4205
- Product name
- 2'-Trifluoromethyl-biphenyl-4-carbaldehyde
- Packaging
- 25g
- Price
- $691
- Updated
- 2021/12/16
- Product number
- 071873
- Product name
- 2'-Trifluoromethyl-biphenyl-4-carbaldehyde
- Purity
- 95+%
- Packaging
- 5g
- Price
- $759
- Updated
- 2021/12/16
2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE Chemical Properties,Usage,Production
Synthesis
392-83-6
87199-17-5
198205-95-7
A solution of tetrakis(triphenylphosphine)palladium (0.05 g) and sodium carbonate (0.7 g) in water (5 mL) was sequentially added to a stirred solution of o-bromobenzotrifluorotoluene (0.7 g, 2.75 mmol) and 4-formylbenzeneboronic acid (0.5 g, 3.3 mmol) in dioxane (20 mL) under nitrogen protection and at 80 °C. The reaction mixture was stirred at 100±5°C for 6 hours. Upon completion of the reaction, the solvent was removed by evaporation and the residue was diluted to 50 mL with ethyl acetate and washed with deionized water. The solvent was again removed by evaporation and the residue was purified by silica gel column chromatography (FCC) to afford 2'-(trifluoromethyl)-[1,1'-biphenyl]-4-carbaldehyde (0.61 g, 88% yield) as a milky white solid.1H-NMR (CDCl3) δ: 7.49 (d, 1H, J = 7.41 Hz); 7.48 (d, 2H, J = 8.13 Hz); 7.61-7.53 (m, 2H); 7.76 (d, 1H, J = 7.8 Hz); 7.91 (d, 2H, J = 8.34 Hz); 10.07 (s, 1H).
References
[1] Patent: WO2010/42998, 2010, A1. Location in patent: Page/Page column 95
2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2'-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE manufacturers
- Product
- 2"-TRIFLUOROMETHYL-BIPHENYL-4-CARBALDEHYDE 198205-95-7
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11