ChemicalBook > CAS DataBase List > 3-PYRIDIN-4-YL-BENZOIC ACID

3-PYRIDIN-4-YL-BENZOIC ACID

Product Name: 3-PYRIDIN-4-YL-BENZOIC ACID
CAS No.: 4385-78-8
Chemical Name: 3-PYRIDIN-4-YL-BENZOIC ACID
Synonyms: AKOS BAR-0604;3-(Pyridin-4-yl);3-PYRID-4-YLBENZOIC ACID;3-(4-Pyridyl)benzoic Acid;4-(3-Carboxyphenyl)pyridine;3-(4-PYRIDINYL)BENZOIC ACID;3-PYRIDIN-4-YL-BENZOIC ACID;3-(Pyridin-4-yl)benzoicacid97%;Benzoic acid, 3-(4-pyridinyl)-;3-(Pyridin-4-yl)benzoic acid 97%
CBNumber: CB0393328
Molecular Formula: C12H9NO2
Formula Weight: 199.21
MOL File: 4385-78-8.mol

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3-PYRIDIN-4-YL-BENZOIC ACID Property

Melting point:: 268 °C
Boiling point:: 405.0±28.0 °C(Predicted)
Density: 1.241±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 3.78±0.10(Predicted)
Appearance: White to off-white Solid
CAS DataBase Reference: 4385-78-8

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Safety

Hazard Codes: Xn
Risk Statements: 22
Hazard Note: Harmful
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: B525675
Product name: 3-(Pyridin-4-yl)benzoicAcid
Packaging: 50mg
Price: $60
Updated: 2021/12/16

TRC

Product number: B525675
Product name: 3-(Pyridin-4-yl)benzoicAcid
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: OR9726
Product name: 3-(Pyridin-4-yl)benzoicacid
Purity: 95%
Packaging: 250mg
Price: $26
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H21-1-D7
Product name: 3-(Pyridin-4-yl)benzoic acid
Purity: 95%
Packaging: 250mg
Price: $42
Updated: 2021/12/16

Apolloscientific

Product number: OR9726
Product name: 3-(Pyridin-4-yl)benzoicacid
Purity: 95%
Packaging: 1g
Price: $88
Updated: 2021/12/16

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3-PYRIDIN-4-YL-BENZOIC ACID Chemical Properties,Usage,Production

Definition

ChEBI: 3-Pyrid-4-ylbenzoic acid is a phenylpyridine.

Synthesis

1120-87-2

25487-66-5

4385-78-8

Example 165 Synthesis of A3-(pyridin-4-yl)benzoic acid: 3-Carboxyphenylboronic acid (1.5 g, 9 mmol) and 4-bromopyridine (1.5 g, 9.9 mmol) were dissolved in a mixed solvent of acetonitrile (40 mL) and water (40 mL), potassium carbonate (5.5 g, 40 mmol) and bis(triphenylphosphine)palladium(II) chloride (400 mg, 0.37 mmol). The reaction mixture was stirred under reflux conditions overnight. Upon completion of the reaction, the suspension was filtered while hot and the filtrate was concentrated to half the original volume. The concentrated aqueous phase was washed with dichloromethane. Subsequently, the aqueous phase was adjusted to pH=3 with 1 M hydrochloric acid, the solid was precipitated, filtered and the solid was washed with water. Finally, the solid residue was dried under vacuum to give 1.5 g of 3-(pyridin-4-yl)benzoic acid in 83% yield.LC-MS (ESI) m/z: 200(M+1)+.

References

[1] Patent: US2009/197863, 2009, A1. Location in patent: Page/Page column 76

3-PYRIDIN-4-YL-BENZOIC ACID Preparation Products And Raw materials

Raw materials

3-Bromobenzoic acid p-Toluenesulfonic acid N,N-Dimethylformamide Cesium carbonate Tetrahydrofuran Pyridine-4-boronic acid Palladium chloride Ethyl acetate Methanol Sodium hydroxide Triphenylphosphine Magnesium sulfate Thionyl chloride

Preparation Products

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View Lastest Price from 3-PYRIDIN-4-YL-BENZOIC ACID manufacturers

Career Henan Chemical Co

Product: 3-PYRIDIN-4-YL-BENZOIC ACID 4385-78-8
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-02

4385-78-8, 3-PYRIDIN-4-YL-BENZOIC ACIDRelated Search:

3-Pyrid-4-ylbenzaldehyde 4-(6-(Trifluoromethyl)pyridin-2-yl)benzoic acid 3-Pyridin-3-yl-benzoic acid ,97% 3-PYRIDIN-2-YL-BENZOIC ACID, 95+% 3-(5-NITROPYRIDIN-2-YL)BENZOIC ACID 3-(6-(Hydroxymethyl)pyridin-3-yl)benzoic acid,3-(6-(Trifluoromethyl)pyridin-3-yl)benzoic acid 4-(5-(Trifluoromethyl)pyridin-2-yl)benzoic acid,4-(4-(Trifluoromethyl)pyridin-2-yl)benzoic acid 2-(6-(trifluoromethyl)pyridin-3-yl)benzoic acid (3-PYRID-4-YLPHENYL)METHANOL 3-PYRIDIN-4-YL-BENZOIC ACID 4-(6-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,4-(4-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,4-(5-(Methoxycarbonyl)pyridin-3-yl)benzoic acid 4-[3-[2-(Dimethylamino-d6)-2-oxoethyl]-6-methylimidazo[1,2-a]pyridin-2-yl]benzoic Acid 3-(5,7-dioxo-5,7-dihydro-6H-pyrrolo[3,4-b]pyridin-6-yl)benzoic acid 3-(6-(Methoxycarbonyl)pyridin-3-yl)benzoic acid,3-(5-(Methoxycarbonyl)pyridin-3-yl)benzoic acid 2-(PYRIDIN-4-YL)BENZOIC ACID Zolpidem Phenyl-4-carboxylic Acid 2-(5-(trifluoromethyl)pyridin-2-yl)benzoic acid 2-PYRIDIN-3-YL-BENZOIC ACID

4-(3-Carboxyphenyl)pyridine

3-(Pyridin-4-yl)benzoicacid97%

3-(Pyridin-4-yl)

3-(Pyridin-4-yl)benzoic acid 97%

3-(2-(Methoxycarbonyl)pyridin-4-yl)benzoic acid

3-(2-Carbamoylpyridin-4-yl)benzoic acid

3-(2-Carboxypyridin-4-yl)benzoic acid

3-(2-Chloropyridin-4-yl)benzoic acid

3-(2-Fluoropyridin-4-yl)benzoic acid

3-(2-Methylpyridin-4-yl)benzoic acid

3-(3-(Methoxycarbonyl)pyridin-4-yl)benzoic acid

3-(3-Carboxypyridin-4-yl)benzoic acid

3-(3-Fluoropyridin-4-yl)benzoic acid

3-(3-Methylpyridin-4-yl)benzoic acid

AKOS BAR-0604

3-(4-PYRIDINYL)BENZOIC ACID

3-PYRID-4-YLBENZOIC ACID

3-PYRIDIN-4-YL-BENZOIC ACID

Benzoic acid, 3-(4-pyridinyl)-

3-(4-Pyridyl)benzoic Acid

4385-78-8

Phenyls & Phenyl-Het

Carboxylic Acids

Phenyls & Phenyl-Het

Carboxylic Acids