2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID
- Product Name
- 2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID
- CAS No.
- 35700-40-4
- Chemical Name
- 2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID
- Synonyms
- BUTTPARK 97\04-61;7-COUMARANCARBOXYLIC ACID;Dihydrobenzofurancarboxylicacid;2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC AID;2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID;2,3-Dihydro-7-benzofurancarboxylic acid;2,3-dihydro-1-benzofuran-7-carboxylicaci;7-benzofurancarboxylic acid, 2,3-dihydro-;2,3-Dihydrobenzofuran-7-carboxylicAcid>2,3-DIHYDROBENZO[B]FURAN-7-CARBOXYLIC ACID
- CBNumber
- CB0425951
- Molecular Formula
- C9H8O3
- Formula Weight
- 164.16
- MOL File
- 35700-40-4.mol
2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID Property
- Melting point:
- 169-171
- Boiling point:
- 330.6±31.0 °C(Predicted)
- Density
- 1.344±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- form
- powder to crystal
- pka
- 4.16±0.20(Predicted)
- color
- White to Orange to Green
- InChI
- InChI=1S/C9H8O3/c10-9(11)7-3-1-2-6-4-5-12-8(6)7/h1-3H,4-5H2,(H,10,11)
- InChIKey
- UHXBMSNEECJPSX-UHFFFAOYSA-N
- SMILES
- O1C2=C(C(O)=O)C=CC=C2CC1
- CAS DataBase Reference
- 35700-40-4(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- D2446
- Product name
- 2,3-Dihydrobenzofuran-7-carboxylic Acid
- Purity
- >98.0%(T)
- Packaging
- 1g
- Price
- $97
- Updated
- 2025/07/31
- Product number
- D2446
- Product name
- 2,3-Dihydrobenzofuran-7-carboxylic Acid
- Purity
- >98.0%(T)
- Packaging
- 5g
- Price
- $306
- Updated
- 2025/07/31
- Product number
- D454913
- Product name
- 2,3-Dihydrobenzofuran-7-carboxylic Acid
- Packaging
- 500mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- W5722
- Product name
- 2,3-Dihydrobenzofuran-7-carboxylic Acid
- Packaging
- 1g
- Price
- $178
- Updated
- 2021/12/16
- Product number
- FD121630
- Product name
- 2,3-Dihydro-1-benzofuran-7-carboxylic acid
- Packaging
- 2g
- Price
- $218
- Updated
- 2021/12/16
2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID Chemical Properties,Usage,Production
Synthesis
496-16-2
35700-40-4
1. Synthesis of 2,3-dihydrobenzo[b]furan-7-carboxylic acid (15a): N,N,N',N'-tetramethylethylenediamine (TMEDA) (24.3 g, 0.21 mol) was added dropwise to a solution of n-BuLi (1.7 M, 123 mL, 0.21 mol) in 400 mL of hexanes under argon protection followed by the addition of a solution of 2,3-dihydrobenzo[b ] furan (14) (12.56 g, 0.11 mol) solution in hexane (40 mL). The reaction mixture was stirred at room temperature for 4 hours. The reaction mixture was slowly poured into dry ice pre-washed with anhydrous ether, followed by stirring at room temperature overnight. After completion of the reaction, the organic and aqueous layers were separated by diluting the mixture with 300 mL of water. The aqueous layer was acidified to pH 1 with concentrated hydrochloric acid and precipitated as a white solid upon cooling. The precipitate was collected by filtration and recrystallized with dichloromethane (CH2Cl2) to give the target product 15a (9.43 g, 54.7% yield) as a white solid with a melting point of 167-169.5 °C.
References
[1] Patent: US4888353, 1989, A
[2] Patent: EP234872, 1991, B1
[3] Patent: US5122361, 1992, A
2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID Suppliers
- Tel
- 800-4238616
- Fax
- +1-888-520-1075 / +1-503-283-1987
- sales@tciamerica.com
- Country
- Americas
- ProdList
- 23653
- Advantage
- 75
View Lastest Price from 2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID manufacturers
- Product
- 2,3-Dihydro-1-benzofuran-7-carboxylic acid 35700-40-4
- Price
- US $0.00/kg
- Min. Order
- 25kg
- Purity
- 98%
- Supply Ability
- Inquiry
- Release date
- 2023-07-17
- Product
- 2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID 35700-40-4
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11
- Product
- 2,3-DIHYDROBENZOFURAN-7-CARBOXYLIC ACID 35700-40-4
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2020-01-06