ChemicalBook > CAS DataBase List > 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE

4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE

Product Name: 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE
CAS No.: 13104-56-8
Chemical Name: 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE
Synonyms: 4'-(4-Methoxyphenyl)-2,2':6',2;4'-(4-methoxyphenyl)-2.2:6,2"-Terpyridine;4'-(4-METHOXYPHENYL)-2,2':6',2'-TERPYRIDINE;4'-(4-Methoxyphenyl)-2,2':6',2"-terpyridine;4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine;4'-(p-Methoxyphenyl)-2,2':6',2''-terpyridine;2,6-Di[2-pyridyl-4-(p-methoxyphenyl)pyridine;4-(4-methoxyphenyl)-2,6-dipyridin-2-ylpyridine;2,2':6',2''-Terpyridine, 4'-(4-methoxyphenyl)-;2,6-bis(2'-pyridyl)-4-(p-methoxyphenyl)pyridine
CBNumber: CB0446792
Molecular Formula: C22H17N3O
Formula Weight: 339.39
MOL File: 13104-56-8.mol

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4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE Property

Melting point:: 167-168℃
Boiling point:: 504.5±50.0 °C(Predicted)
Density: 1.174±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.62±0.22(Predicted)
Appearance: White to off-white Solid
Water Solubility: Insoluble in water.
CAS DataBase Reference: 13104-56-8

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical

Product number: M2951
Product name: 4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine
Packaging: 200MG
Price: $69
Updated: 2025/07/31

TCI Chemical

Product number: M2951
Product name: 4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine
Packaging: 1G
Price: $208
Updated: 2025/07/31

American Custom Chemicals Corporation

Product number: CHM0012878
Product name: 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $503.33
Updated: 2021/12/16

Arctom

Product number: AS574753
Product name: 4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine
Purity: 97%
Packaging: 5g
Price: $517
Updated: 2021/12/16

Chemenu

Product number: CM126758
Product name: 4''-(4-methoxyphenyl)-2,2'':6'',2''''-terpyridine
Purity: 95%
Packaging: 5g
Price: $583
Updated: 2021/12/16

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4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE Chemical Properties,Usage,Production

Uses

4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine is used as an organic chemical synthesis intermediate.

Synthesis

1122-62-9

123-11-5

13104-56-8

Generic method: 4'-(3-methoxyphenyl)-2,2':6',2"-terpyridine (3-MeO-Phtpy), 4'-(2-methoxyphenyl)-2,2':6',2"-terpyridine (2-MeO-Phtpy) and 4'-(4-methoxyphenyl)-2,2':6',2"-terpyridine (4-MeO-Phtpy) The synthesis was carried out with reference to the method described in the literature [27-33]. The steps were as follows: 2-acetylpyridine (2.813 g, 23.2 mmol, 2 eq.) was added to a 50 mL ethanol solution dissolved in 2-methoxybenzaldehyde, 3-methoxybenzaldehyde or 4-methoxybenzaldehyde (11.6 mmol, 1 eq.). Subsequently, KOH pellets (46.5 mmol, 4 eq.) were added to this solution. The reaction mixture was stirred at room temperature for 10 minutes. NH3 (40 mL, 25% aqueous solution) was slowly added to the reaction mixture. After incubation at 37 °C for 24 h, 5 mL of 25% aqueous NH3 was added. The reaction mixture was cooled to -20 °C and the resulting white precipitate was separated by filtration and washed with cold ethanol. For further purification of each product, recrystallization was carried out using ethanol-H2O mixed solvent. After recrystallization, each product was recovered by filtration, washed sequentially with cold ethanol and petroleum ether, and finally dried under high vacuum for 24 h (Scheme 1).

References

[1] Applied Organometallic Chemistry, 2017, vol. 31, # 10,
[2] Applied Organometallic Chemistry, 2017, vol. 31, # 6,
[3] Chemistry - An Asian Journal, 2018, vol. 13, # 21, p. 3169 - 3172
[4] Chemistry Letters, 2005, vol. 34, # 5, p. 732 - 733
[5] Synthesis, 2005, # 18, p. 3045 - 3050

4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE Preparation Products And Raw materials

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View Lastest Price from 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE manufacturers

Shanghai UCHEM Inc.

Product: 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE 13104-56-8
Price: US $64.00-206.00/g
Min. Order: 5g
Purity: 0.98
Supply Ability: 25kg
Release date: 2025-07-08

13104-56-8, 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINERelated Search:

4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE 4-(4-Methoxyphenyl)pyridine 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE 4'-PHENYL-2,2':6',2''-TERPYRIDINE

2,6-Di(2-pyridinyl)-4-(4-methoxyphenyl)pyridine

2,6-Di[2-pyridyl-4-(p-methoxyphenyl)pyridine

4'-(p-Methoxyphenyl)-2,2':6',2''-terpyridine

2,2':6',2''-Terpyridine, 4'-(4-methoxyphenyl)-

4-(4-methoxyphenyl)-2,6-dipyridin-2-ylpyridine

4'-(4-Methoxyphenyl)-2,2':6',2

2,6-bis(2'-pyridyl)-4-(p-methoxyphenyl)pyridine

4'-(4-Methoxyphenyl)-2,2':6',2''-terpyridine

4'-(4-Methoxyphenyl)-2,2':6',2"-terpyridine

4'-(4-METHOXYPHENYL)-2,2':6',2'-TERPYRIDINE

4'-(4-methoxyphenyl)-2.2:6,2"-Terpyridine

13104-56-8