BUTTPARK 148\01-24
- Product Name
- BUTTPARK 148\01-24
- CAS No.
- 154532-34-0
- Chemical Name
- BUTTPARK 148\01-24
- Synonyms
- BUTTPARK 148\01-24;3-TERT-BUTYL-BENZONITRILE;3-(1,1-Dimethylethyl)benzonitrile;Benzonitrile, 3-(1,1-dimethylethyl)-
- CBNumber
- CB0674861
- Molecular Formula
- C11H13N
- Formula Weight
- 159.23
- MOL File
- 154532-34-0.mol
BUTTPARK 148\01-24 Property
- Boiling point:
- 238℃
- Density
- 0.95
- Flash point:
- 98℃
- storage temp.
- Sealed in dry,Room Temperature
- form
- liquid
- color
- Clear
Safety
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B813988
- Product name
- 3-tert-Butyl-benzonitrile
- Packaging
- 100mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 4837AD
- Product name
- 3-tert-Butylbenzonitrile
- Packaging
- 5g
- Price
- $94
- Updated
- 2021/12/16
- Product number
- 4837AD
- Product name
- 3-tert-Butylbenzonitrile
- Packaging
- 10g
- Price
- $178
- Updated
- 2021/12/16
- Product number
- 3737-1-31
- Product name
- 3-tert-Butylbenzonitrile
- Packaging
- 1g
- Price
- $210
- Updated
- 2021/12/16
- Product number
- 084935
- Product name
- 3-tert-Butylbenzonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $341
- Updated
- 2021/12/16
BUTTPARK 148\01-24 Chemical Properties,Usage,Production
Synthesis
557-21-1
201851-06-1
154532-34-0
Zinc cyanide (1.57 g, 13.40 mmol) was added to a solution of 3-tert-butylphenyl trifluoromethanesulfonate (1.5 g, 6.70 mmol) in N,N-dimethylformamide (DMF, 10 mL). The reaction mixture was heated to 120 °C and the reaction was stirred at this temperature for 4 hours. Upon completion of the reaction, the mixture was cooled to room temperature, diluted with ether (2500 mL) and subsequently washed twice with 2N ammonium hydroxide solution (50 mL x 2). The organic phase was separated, washed with saturated sodium chloride solution (20 mL), dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography with the eluent being hexane solution of 5% ethyl acetate to give 3-tert-butylbenzonitrile in 75% yield.
References
[1] Patent: WO2009/42694, 2009, A1. Location in patent: Page/Page column 91
[2] Patent: WO2006/74940, 2006, A2. Location in patent: Page/Page column 30
[3] Patent: US2008/132477, 2008, A1. Location in patent: Page/Page column 50
BUTTPARK 148\01-24 Preparation Products And Raw materials
Raw materials
Preparation Products
BUTTPARK 148\01-24 Suppliers
- Tel
- --
- Fax
- --
- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
- Tel
- --
- Fax
- --
- Country
- United Kingdom
- ProdList
- 6309
- Advantage
- 46
- Tel
- --
- Fax
- --
- info@manchesterorganics.com
- Country
- United Kingdom
- ProdList
- 6834
- Advantage
- 67
- Tel
- --
- Fax
- --
- 113707.50@compuserve.com
- Country
- United Kingdom
- ProdList
- 6078
- Advantage
- 30
View Lastest Price from BUTTPARK 148\01-24 manufacturers
- Product
- BUTTPARK 148\01-24 154532-34-0
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 200kgs
- Release date
- 2020-01-09