4-PYRROLIDIN-1-YLANILINE
- Product Name
- 4-PYRROLIDIN-1-YLANILINE
- CAS No.
- 2632-65-7
- Chemical Name
- 4-PYRROLIDIN-1-YLANILINE
- Synonyms
- AKOS BB-8560;AKOS B021942;ART-CHEM-BB B021942;TIMTEC-BB SBB009578;4-pyrrolidinoaniline;4-PYRROLIDIN-1-YLANILINE;4-(1-PYRROLIDINYL)ANILINE;1-(4-Aminophenyl)pyrrolidine;4-(1-pyrrolidinyl)phenylamine;4-PYRROLIDIN-1-YL-PHENYLAMINE
- CBNumber
- CB0674997
- Molecular Formula
- C10H14N2
- Formula Weight
- 162.23
- MOL File
- 2632-65-7.mol
4-PYRROLIDIN-1-YLANILINE Property
- Melting point:
- 51 °C
- Boiling point:
- 180-185 °C(Press: 16 Torr)
- Density
- 1.109±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 7.20±0.40(Predicted)
- Appearance
- Brown to black Solid
Safety
- HazardClass
- IRRITANT
- HS Code
- 2933998090
N-Bromosuccinimide Price
- Product number
- B525040
- Product name
- 4-Pyrrolidin-1-ylaniline
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 3H30-1-F9
- Product name
- 4-(Pyrrolidin-1-yl)aniline
- Packaging
- 1g
- Price
- $135
- Updated
- 2021/12/16
- Product number
- 033452
- Product name
- 4-(1-Pyrrolidinyl)aniline
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- 3H30-1-F9
- Product name
- 4-(Pyrrolidin-1-yl)aniline
- Packaging
- 250mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 2324AB
- Product name
- 4-(Pyrrolidin-1-yl)aniline
- Packaging
- 5g
- Price
- $251
- Updated
- 2021/12/16
4-PYRROLIDIN-1-YLANILINE Chemical Properties,Usage,Production
Synthesis
10220-22-1
2632-65-7
GENERAL PROCEDURE: The general method for the synthesis of 4-(pyrrolidin-1-yl)aniline from 1-(4-nitrophenyl)pyrrolidine is as follows: 1-(substituted)4-nitrophenyl derivatives IVa, b, e, f (0.01 mol) were dissolved in NH4OH (20 mL, 30%) and an aqueous solution of sodium conidiosulfite (7 g, 0.04 mol) was quickly added (30 mL). The reaction mixture was refluxed for 15 min. After completion of the reaction, the mixture was cooled and the crude product was obtained by filtration. The crude product was washed and crystallized from dichloromethane to give the target compounds Va, b, e, f. Among them, 4-(pyrrolidin-1-yl)aniline Vb was obtained in 80% yield as a yellow oily substance (in agreement with the literature report) [66].
References
[1] Bulletin of the Korean Chemical Society, 2015, vol. 36, # 7, p. 1863 - 1873
[2] Bioorganic Chemistry, 2014, vol. 57, p. 65 - 82
[3] Advanced Synthesis and Catalysis, 2018, vol. 360, # 11, p. 2131 - 2137
[4] Patent: US2005/49286, 2005, A1
[5] Justus Liebigs Annalen der Chemie, 1955, vol. 596, p. 1,151
4-PYRROLIDIN-1-YLANILINE Preparation Products And Raw materials
Raw materials
Preparation Products
4-PYRROLIDIN-1-YLANILINE Suppliers
- Tel
- --
- Fax
- --
- art-chem@art-chem.com
- Country
- Russia
- ProdList
- 6560
- Advantage
- 30
- Tel
- --
- Fax
- --
- asinex@asinex.com
- Country
- Russia
- ProdList
- 6615
- Advantage
- 66
View Lastest Price from 4-PYRROLIDIN-1-YLANILINE manufacturers
- Product
- 4-PYRROLIDIN-1-YLANILINE 2632-65-7
- Price
- US $1.00/KG
- Min. Order
- 1G
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-08-13