3,5-DIBROMO-2-METHYLTHIOPHENE
- Product Name
- 3,5-DIBROMO-2-METHYLTHIOPHENE
- CAS No.
- 29421-73-6
- Chemical Name
- 3,5-DIBROMO-2-METHYLTHIOPHENE
- Synonyms
- 3,5-DIBROMO-2-METHYLTHIOPHENE;2-METHYL-3,5-DIBROMO-THIOPHENE;Thiophene, 3,5-dibromo-2-methyl-;3,5-Dibromo-2-methylthiophene>
- CBNumber
- CB0694645
- Molecular Formula
- C5H4Br2S
- Formula Weight
- 255.96
- MOL File
- 29421-73-6.mol
3,5-DIBROMO-2-METHYLTHIOPHENE Property
- Melting point:
- -15°C(lit.)
- Boiling point:
- 230°C(lit.)
- Density
- 2
- refractive index
- 1.6120-1.6160
- storage temp.
- 0-10°C
- form
- clear liquid
- color
- Colorless to Yellow
- InChI
- InChI=1S/C5H4Br2S/c1-3-4(6)2-5(7)8-3/h2H,1H3
- InChIKey
- OGAJGUIMFMRGRB-UHFFFAOYSA-N
- SMILES
- C1(C)SC(Br)=CC=1Br
- CAS DataBase Reference
- 29421-73-6
Safety
- Hazard Codes
- Xi
- HS Code
- 2934999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D3999
- Product name
- 3,5-Dibromo-2-methylthiophene
- Purity
- >95.0%(GC)
- Packaging
- 5g
- Price
- $88
- Updated
- 2026/03/19
- Product number
- D3999
- Product name
- 3,5-Dibromo-2-methylthiophene
- Purity
- >95.0%(GC)
- Packaging
- 25g
- Price
- $302
- Updated
- 2026/03/19
- Product number
- D425930
- Product name
- 3,5-Dibromo-2-methylthiophene
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D425930
- Product name
- 3,5-Dibromo-2-methylthiophene
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD62792
- Product name
- 3,5-Dibromo-2-methylthiophene
- Packaging
- 1g
- Price
- $65
- Updated
- 2021/12/16
3,5-DIBROMO-2-METHYLTHIOPHENE Chemical Properties,Usage,Production
Uses
3,5-Dibromo-2-methylthiophene is a useful reagent for the preparation of arylthiophene-substituted norbornadienes.
Synthesis
At zero temperature, 120.0 mL of glacial acetic acid was used to dissolve the compound of formula 6, 2-methylthiophene (24.50 g, 250.00 mmol), and then placed into a 250.0 mL single-necked flask, and under rapid stirring, 30.0 mL of a mixture of liquid bromine and 30.0 mL of glacial acetic acid was added to it slowly through a constant-pressure funnel, and the mixture was slowly dripped out over a period of 5 h, and then the reaction continued for another 12 h. The reaction was completed with the addition of 100.0 mL of water. After the reaction was completed, 100.0 mL of water was added to terminate the reaction, so that the organic phase and the aqueous phase were separated, and the aqueous phase was adjusted to pH=7 with sodium hydroxide solution, and then extracted with ether, and all the organic phases were combined, and then washed with saturated sodium carbonate for 3 times, and added anhydrous drying for 12h, and a light-yellow color product was obtained by means of distillation under reduced pressure, 54.20g, with a yield of 82%.
3,5-DIBROMO-2-METHYLTHIOPHENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-DIBROMO-2-METHYLTHIOPHENE manufacturers
- Product
- 3,5-DIBROMO-2-METHYLTHIOPHENE 29421-73-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 97%
- Supply Ability
- 2000
- Release date
- 2025-04-18
- Product
- 3,5-DibroMo-2-Methylthiophene 29421-73-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 5mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-06