ChemicalBook > CAS DataBase List > 4-BROMOBENZYLSULFONYL CHLORIDE

4-BROMOBENZYLSULFONYL CHLORIDE

Product Name
4-BROMOBENZYLSULFONYL CHLORIDE
CAS No.
53531-69-4
Chemical Name
4-BROMOBENZYLSULFONYL CHLORIDE
Synonyms
4-BROMOBENZYLSULFONY;4-BROMOBENZYLSULFONYL CHLORIDE;4-Bromobenzylsulphonyl chloride;4-Bromobenzylsulphonyl chloride 97%;4-Bromo-α-toluenesulfonyl chloride, 95%;(4-Bromophenyl)methanesulphonyl chloride;(4-Bromophenyl)methylsulphonyl chloride;BENZENEMETHANESULFONYL CHLORIDE, 4-BROMO-;(4-BROMO-PHENYL)-METHANESULFONYL CHLORIDE;(4-Bromophenyl)methanesulphonylchloride97%
CBNumber
CB0713032
Molecular Formula
C7H6BrClO2S
Formula Weight
269.54
MOL File
53531-69-4.mol
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4-BROMOBENZYLSULFONYL CHLORIDE Property

Melting point:
117 °C
Boiling point:
116.5-121.5/
Density 
1.746±0.06 g/cm3(Predicted)
storage temp. 
-20°C, sealed storage, away from moisture
form 
powder
color 
White
CAS DataBase Reference
53531-69-4
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Safety

Hazard Codes 
C,Xn
Risk Statements 
22
RIDADR 
UN3261
Hazard Note 
Corrosive
HazardClass 
8
HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
B680873
Product name
4-Bromobenzylsulfonylchloride
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
B680873
Product name
4-Bromobenzylsulfonylchloride
Packaging
500mg
Price
$65
Updated
2021/12/16
TRC
Product number
B680873
Product name
4-Bromobenzylsulfonylchloride
Packaging
250mg
Price
$55
Updated
2021/12/16
SynQuest Laboratories
Product number
6762-D-X3
Product name
4-Bromobenzylsulfonyl chloride
Purity
97.0%
Packaging
1g
Price
$58
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0022279
Product name
4-(BROMO-PHENYL)-METHANE SULFONYL CHLORIDE
Purity
95.00%
Packaging
1G
Price
$479.85
Updated
2021/12/16
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4-BROMOBENZYLSULFONYL CHLORIDE Chemical Properties,Usage,Production

Synthesis

351003-15-1

53531-69-4

General procedure for the synthesis of p-bromobenzyl sulfonyl chloride from 4-bromo-α-toluene thioacetic acid: N-chlorosuccinimide (NCS, 3.3 g, 24.6 mmol) was added batchwise to a solution of acetonitrile (30 mL) containing 2 M HCl (1.547 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 5 min. Subsequently, a solution of 4-bromophenylmethanesulfonyl chloride (1.5 g, 6.15 mmol) in acetonitrile (3 mL) was added dropwise to the mixture at the same temperature, with the dropwise addition time being controlled at 1 min. After continuing to stir the reaction mixture for 10 minutes, anhydrous sodium sulfate (about 5 g) was added and the solid was removed by filtration. The filtrate was concentrated and the resulting residue was purified by silica gel column chromatography (petroleum ether/ethyl acetate = 10/1) to afford p-bromobenzylsulfonyl chloride (1.2 g, 73% yield) as a white solid.1H NMR (300 MHz, CDCl3): δ = 7.62 (d, J = 8.4 Hz, 2H), 7.37 (d, J = 8.4 Hz, 2H), 4.83 (s 2H).

References

[1] Patent: WO2018/132372, 2018, A1. Location in patent: Paragraph 01167
[2] Patent: US2014/163024, 2014, A1. Location in patent: Paragraph 0432
[3] Patent: US2014/163110, 2014, A1. Location in patent: Page/Page column 12
[4] Patent: WO2015/177325, 2015, A1. Location in patent: Page/Page column 52; 53

4-BROMOBENZYLSULFONYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMOBENZYLSULFONYL CHLORIDE Suppliers

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View Lastest Price from 4-BROMOBENZYLSULFONYL CHLORIDE manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
(4-Bromophenyl)methanesulfonyl chloride 53531-69-4
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%+
Supply Ability
100 tons
Release date
2020-01-06

53531-69-4, 4-BROMOBENZYLSULFONYL CHLORIDERelated Search:

(4-Bromo-1-methyl-1H-pyrazol-3-yl)methanol (4-Bromo-1-methyl-1H-pyrazol-3-yl)methanol Methanesulfonyl chloride alpha-Toluenesulfonyl chloride 2-BROMOBENZYLSULFONYL CHLORIDE 97% 2-BROMOBENZYLSULFONYL CHLORIDE 3-BROMOBENZYLSULFONYL CHLORIDE 4-BROMOBENZYLSULFONYL CHLORIDE

  • BENZENEMETHANESULFONYL CHLORIDE, 4-BROMO-
  • 4-BROMOBENZYLSULFONY
  • 4-Bromobenzylsulphonyl chloride 97%
  • 4-Bromo-α-toluenesulfonyl chloride, 95%
  • (4-BROMO-PHENYL)-METHANESULFONYL CHLORIDE
  • 4-BROMOBENZYLSULFONYL CHLORIDE
  • (4-Bromophenyl)methanesulphonyl chloride
  • (4-Bromophenyl)methanesulphonyl chloride 97%
  • (4-Bromophenyl)methylsulphonyl chloride
  • 4-Bromobenzylsulphonyl chloride
  • (4-Bromophenyl)methanesulphonylchloride97%
  • 4-BROMOBENZYLSULFONYL CHLORIDE ISO 9001：2015 REACH
  • 53531-69-4