6-Chloro-1-tetralone

ChemicalBook > CAS DataBase List > 6-Chloro-1-tetralone

6-Chloro-1-tetralone

Product Name: 6-Chloro-1-tetralone
CAS No.: 26673-31-4
Chemical Name: 6-Chloro-1-tetralone
Synonyms: 6-chloro-3,4-dihydronaphthalen-1(2H)-one;6-Chloro-3,4-dihydro-2H-naphthalen-1-one;6-chloro-3;5-CHLORO-1-INDOMONE;5-CHLORO-L-INDOMONE;6-Chloro-α-Tetralone;6-Chloro-1-tetralone;6-CHLORO-TETRAL-1-ON;6-Chloro-tetral-1-one;6-chlorotetralin-1-one
CBNumber: CB0766902
Molecular Formula: C10H9ClO
Formula Weight: 180.63
MOL File: 26673-31-4.mol

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6-Chloro-1-tetralone Property

Melting point:: 53 °C
Boiling point:: 150°C/0.7mmHg(lit.)
Density: 1.248±0.06 g/cm3(Predicted)
refractive index: 1.59
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder to lump
color: White to Yellow to Orange
CAS DataBase Reference: 26673-31-4

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Safety

HS Code: 2914390090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H302Harmful if swallowed

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: JRD0960
Product name: 6-Chloro-3,4-dihydronaphthalen-1(2H)-one
Packaging: 1g
Price: $345
Updated: 2024/03/01

TCI Chemical

Product number: C2917
Product name: 6-Chloro-1-tetralone
Purity: >96.0%(GC)
Packaging: 1g
Price: $134
Updated: 2024/03/01

TCI Chemical

Product number: C2917
Product name: 6-Chloro-1-tetralone
Purity: >96.0%(GC)
Packaging: 5g
Price: $466
Updated: 2024/03/01

TRC

Product number: C429283
Product name: 6-Chloro-1-tetralone
Packaging: 250mg
Price: $605
Updated: 2021/12/16

TRC

Product number: C429283
Product name: 6-Chloro-1-tetralone
Packaging: 100mg
Price: $320
Updated: 2021/12/16

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6-Chloro-1-tetralone Chemical Properties,Usage,Production

Uses

6-Chloro-1-tetralone is a novel and potent intermediate used for synthesis of pharmaceutical compounds.

Synthesis

A solution of sodium nitrite (173 mg, 2.51 mmol) in water (5 mL) at 0 °C (ice-bath) was added to a magnetically stirred suspension of 6-Amino-1-tetralone (360 mg, 2.23 mmol) in aqueous hydrochloric acid (10 mL, 6 M) at 0 °C. This reaction mixture was added dropwise to a solution of copper(I) chloride (267 mg, 2.70 mmol) in concentrated hydrochloric acid (5 mL) at 0 °C. It was allowed to warm up to room 100 temperature and stirred for a further 2 h after which it was neutralised with solid sodium carbonate, extracted with ethyl acetate (3 × 20 mL) and concentrated in vacuo to give slightly yellow oil. This material was subjected to flash chromatography (50% chloroform in hexane) and concentration of the appropriate fractions afforded 6-chloro-1-tetralone (180 mg, 45%) as a waxy solid.

6-Chloro-1-tetralone Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Chloro-1-tetralone Suppliers

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View Lastest Price from 6-Chloro-1-tetralone manufacturers

Henan Fengda Chemical Co., Ltd

Product: 5-chloro-l-indomone 26673-31-4
Price: US $200.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-30

R&D Scientific Inc.

Product: 6-Chloro-1-tetralone 26673-31-4
Price: US $490.00/g
Min. Order: 1g
Purity: 98
Supply Ability: 500 Kg
Release date: 2024-03-19

WUHAN FORTUNA CHEMICAL CO., LTD

Product: 6-Chloro-1-tetralone 26673-31-4
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 30tons/month
Release date: 2023-02-22

26673-31-4, 6-Chloro-1-tetraloneRelated Search:

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26673-31-4