ChemicalBook > CAS DataBase List > 6-Chloro-1-tetralone
6-Chloro-1-tetralone
- Product Name
- 6-Chloro-1-tetralone
- CAS No.
- 26673-31-4
- Chemical Name
- 6-Chloro-1-tetralone
- Synonyms
- 6-chloro-3,4-dihydronaphthalen-1(2H)-one;6-Chloro-3,4-dihydro-2H-naphthalen-1-one;6-chloro-3;5-CHLORO-1-INDOMONE;5-CHLORO-L-INDOMONE;6-Chloro-α-Tetralone;6-Chloro-1-tetralone;6-CHLORO-TETRAL-1-ON;6-Chloro-tetral-1-one;6-chlorotetralin-1-one
- CBNumber
- CB0766902
- Molecular Formula
- C10H9ClO
- Formula Weight
- 180.63
- MOL File
- 26673-31-4.mol
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6-Chloro-1-tetralone Property
- Melting point:
- 53 °C
- Boiling point:
- 150°C/0.7mmHg(lit.)
- Density
- 1.248±0.06 g/cm3(Predicted)
- refractive index
- 1.59
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- powder to lump
- color
- White to Yellow to Orange
- InChI
- InChI=1S/C10H9ClO/c11-8-4-5-9-7(6-8)2-1-3-10(9)12/h4-6H,1-3H2
- InChIKey
- WQKHERPPDYPMNX-UHFFFAOYSA-N
- SMILES
- C1(=O)C2=C(C=C(Cl)C=C2)CCC1
- CAS DataBase Reference
- 26673-31-4
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Safety
- HS Code
- 2914390090
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- JRD0960
- Product name
- 6-Chloro-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 1g
- Price
- $356
- Updated
- 2025/07/31
TCI Chemical
- Product number
- C2917
- Product name
- 6-Chloro-1-tetralone
- Purity
- >96.0%(GC)
- Packaging
- 1g
- Price
- $120
- Updated
- 2025/07/31
TCI Chemical
- Product number
- C2917
- Product name
- 6-Chloro-1-tetralone
- Purity
- >96.0%(GC)
- Packaging
- 5g
- Price
- $419
- Updated
- 2025/07/31
TRC
- Product number
- C429283
- Product name
- 6-Chloro-1-tetralone
- Packaging
- 100mg
- Price
- $320
- Updated
- 2021/12/16
TRC
- Product number
- C429283
- Product name
- 6-Chloro-1-tetralone
- Packaging
- 250mg
- Price
- $605
- Updated
- 2021/12/16
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6-Chloro-1-tetralone Chemical Properties,Usage,Production
Uses
6-Chloro-1-tetralone is a novel and potent intermediate used for synthesis of pharmaceutical compounds.
Synthesis
A solution of sodium nitrite (173 mg, 2.51 mmol) in water (5 mL) at 0 °C (ice-bath) was added to a magnetically stirred suspension of 6-Amino-1-tetralone (360 mg, 2.23 mmol) in aqueous hydrochloric acid (10 mL, 6 M) at 0 °C. This reaction mixture was added dropwise to a solution of copper(I) chloride (267 mg, 2.70 mmol) in concentrated hydrochloric acid (5 mL) at 0 °C. It was allowed to warm up to room 100 temperature and stirred for a further 2 h after which it was neutralised with solid sodium carbonate, extracted with ethyl acetate (3 × 20 mL) and concentrated in vacuo to give slightly yellow oil. This material was subjected to flash chromatography (50% chloroform in hexane) and concentration of the appropriate fractions afforded 6-chloro-1-tetralone (180 mg, 45%) as a waxy solid.
References
[1] Patent: US2015/105351, 2015, A1. Location in patent: Paragraph 0440
[2] ACS Medicinal Chemistry Letters, 2014, vol. 5, # 11, p. 1259 - 1262
[3] Organic Letters, 2011, vol. 13, # 24, p. 6488 - 6491
[4] Patent: US2012/302562, 2012, A1. Location in patent: Page/Page column 21
[5] Australian Journal of Chemistry, 2010, vol. 63, # 2, p. 211 - 226
6-Chloro-1-tetralone Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-Chloro-1-tetralone manufacturers
WUHAN FORTUNA CHEMICAL CO., LTD
- Product
- 6-Chloro-1-tetralone 26673-31-4
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-02-22
Henan Fengda Chemical Co., Ltd
- Product
- 5-chloro-l-indomone 26673-31-4
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30
R&D Scientific Inc.
- Product
- 6-Chloro-1-tetralone 26673-31-4
- Price
- US $490.00/g
- Min. Order
- 1g
- Purity
- 98
- Supply Ability
- 500 Kg
- Release date
- 2024-03-19
26673-31-4, 6-Chloro-1-tetraloneRelated Search:
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