3-(3-BROMO-PHENYL)-PROPAN-1-OL

Product Name: 3-(3-BROMO-PHENYL)-PROPAN-1-OL
CAS No.: 65537-54-4
Chemical Name: 3-(3-BROMO-PHENYL)-PROPAN-1-OL
Synonyms: BENZENEPROPANOL, 3-BROMO-;3-(3-Bromophenyl)-1-propanol;3-(3-BROMO-PHENYL)-PROPAN-1-OL
CBNumber: CB0807096
Molecular Formula: C9H11BrO
Formula Weight: 215.09
MOL File: 65537-54-4.mol

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3-(3-BROMO-PHENYL)-PROPAN-1-OL Property

Boiling point:: 299.9±15.0 °C(Predicted)
Density: 1.410±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.05±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B698533
Product name: 3-(3-Bromophenyl)propan-1-ol
Packaging: 500mg
Price: $265
Updated: 2021/12/16

AK Scientific

Product number: V7142
Product name: 3-(3-Bromophenyl)propan-1-ol
Packaging: 1g
Price: $291
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0351843
Product name: 3-(3-BROMOPHENYL)PROPAN-1-OL
Purity: 95.00%
Packaging: 5MG
Price: $499.66
Updated: 2021/12/16

ChemScene

Product number: CS-B0313
Product name: 3-(3-bromophenyl)propan-1-ol
Packaging: 250mg
Price: $53
Updated: 2021/12/16

ChemScene

Product number: CS-B0313
Product name: 3-(3-bromophenyl)propan-1-ol
Packaging: 5g
Price: $546
Updated: 2021/12/16

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3-(3-BROMO-PHENYL)-PROPAN-1-OL Chemical Properties,Usage,Production

Synthesis

42287-90-1

65537-54-4

A THF solution (50 mL) of 3-(3-bromophenyl)propionic acid (5 g, 21.83 mmol, 1.00 eq.) was added to a 250 mL three-necked round-bottomed flask under nitrogen protection. The reaction system was cooled to 0 °C and the borane tetrahydrofuran complex solution (1 mol/L, 75 mL, 74.22 mmol, 3.40 eq.) was slowly added dropwise with stirring. After the dropwise addition, the reaction mixture was gradually warmed to room temperature and stirred overnight. After completion of the reaction, the mixture was slowly poured into 150 mL of 1 mol/L HCl solution and extracted with dichloromethane (3 x 200 mL). The organic phases were combined, washed with 300 mL of saturated saline, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with dichloromethane/methanol (10:1, v/v) as eluent. The target fraction was collected and concentrated under reduced pressure to afford 3-(3-bromophenyl)propan-1-ol (1.3 g, 28% yield) as a colorless oil.1H NMR (DMSO-d6, 400 MHz) δ: 7.41-7.20 (m, 4H), 4.51-4.48 (t, 1H), 3.41-3.34 (m, 2H), 2.67-2.59 (m, 2H), 1.73-1.73 (m, 2H). 2H), 1.73-1.66 (m, 2H).

References

[1] Patent: US2004/10019, 2004, A1. Location in patent: Page 160; 167
[2] Patent: WO2006/101977, 2006, A2. Location in patent: Page/Page column 56
[3] Journal of Organic Chemistry, 2010, vol. 75, # 15, p. 5178 - 5194
[4] Angewandte Chemie - International Edition, 2018, vol. 57, # 15, p. 4058 - 4062
[5] Angew. Chem., 2018, vol. 130, p. 4122 - 4126,5

3-(3-BROMO-PHENYL)-PROPAN-1-OL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(3-BROMO-PHENYL)-PROPAN-1-OL manufacturers

Career Henan Chemical Co

Product: 3-(3-BROMO-PHENYL)-PROPAN-1-OL 65537-54-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kg
Release date: 2018-12-25

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3-(3-Bromophenyl)-1-propanol

3-(3-BROMO-PHENYL)-PROPAN-1-OL

BENZENEPROPANOL, 3-BROMO-

65537-54-4