N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine
- Product Name
- N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine
- CAS No.
- 105-84-0
- Chemical Name
- N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine
- Synonyms
- N,N'-dimethyl-N-[2-(;1,4,7-TRIMETHYLDIETHYLENETRIAMINE;Methylbis[2-(methylamino)ethyl]amine;N,N',N''-Trimethyldiethylenetriamine;N,N',N''-trimethyldiethylenetriamine;1,4,7-Trimethyldiethylenetriamine,97%;N,N',N''-Trimethyldiethylenetriamine >N,N-Bis[2-(methylamino)ethyl]methylamine;2,2'-(Methylimino)bis(N-methylethanamine);2,2'-Bis(methylamino)-N-methyldiethylamine
- CBNumber
- CB0940265
- Molecular Formula
- C7H19N3
- Formula Weight
- 145.25
- MOL File
- 105-84-0.mol
N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine Property
- Boiling point:
- 56°C/0.1mmHg(lit.)
- Density
- 0.9135 (estimate)
- refractive index
- 1.4500 to 1.4540
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 10.41±0.10(Predicted)
- form
- Liquid
- color
- Pale yellow
- CAS DataBase Reference
- 105-84-0(CAS DataBase Reference)
- EPA Substance Registry System
- 1,2-Ethanediamine, N,N'-dimethyl-N-[2-(methylamino)ethyl]- (105-84-0)
Safety
- RIDADR
- UN 2735 8/PG II
- TSCA
- Yes
- HS Code
- 2921.29.0055
- HazardClass
- 8
- PackingGroup
- II
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- S388483
- Product name
- 1,4,7-TRIMETHYLDIETHYLENETRIAMINE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $185
- Updated
- 2025/07/31
- Product number
- S388483
- Product name
- 1,4,7-TRIMETHYLDIETHYLENETRIAMINE
- Purity
- AldrichCPR
- Packaging
- 250MG
- Price
- $179
- Updated
- 2024/03/01
- Product number
- B4304
- Product name
- N,N',N''-Trimethyldiethylenetriamine
- Purity
- >95.0%(GC)(T)
- Packaging
- 5mL
- Price
- $285
- Updated
- 2025/07/31
- Product number
- T797633
- Product name
- 1,4,7-Trimethyldiethylenetriamine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 1306AA
- Product name
- N1,N2-Dimethyl-N1-(2-(methylamino)ethyl)ethane-1,2-diamine
- Packaging
- 250mg
- Price
- $81
- Updated
- 2021/12/16
N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine Chemical Properties,Usage,Production
Synthesis
1204417-39-9
105-84-0
The general procedure for the synthesis of N,N',N''-trimethyldiethylenetriamine from the compound (CAS: 1204417-39-9) is as follows: Step 1: N,N-(2,2'-(methylureido)bis(ethane-2,1-diyl))bis(N-methyl-2-nitrobenzenesulfonamide) 7a (1.24 g, 2.405 mmol), cesium carbonate (2.35 g, 7.215 mmol, 3 eq.), and benzenethiol (795 mg, 7.215 mmol, 3 eq.) were dissolved in DMF (25 mL ) in DMF (25 mL) and the reaction was stirred at room temperature for 1 hour. Step 2: Upon completion of the reaction, the reaction mixture was filtered and the filtrate was upsampled onto an MP-TsOH column pre-washed with dichloromethane (DCM). Step 3: The cartridge was washed several times with DCM until the eluate was colorless, followed by elution of the target product with a methanol solution containing NH3. Step 4: The eluate was collected and concentrated to afford N,N'-dimethyl-N-(2-(methylamino)ethyl)ethane-1,2-diamine 7b (220 mg, 63% yield), which was used directly in the next step of the reaction; Mass Spectrum (m/z) = 146 (M + H)+.
References
[1] Patent: WO2010/3658, 2010, A1. Location in patent: Page/Page column 47-48
N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine manufacturers
- Product
- N,N'-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine 105-84-0
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2024-08-05
- Product
- N,N"-dimethyl-N-[2-(methylamino)ethyl]ethylenediamine 105-84-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11
- Product
- 1,4,7-Trimethyldiethylenetriamine 105-84-0
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 200kgs
- Release date
- 2020-01-09