ChemicalBook > CAS DataBase List > 1,3-Adamantanediamine

1,3-Adamantanediamine

Product Name
1,3-Adamantanediamine
CAS No.
10303-95-4
Chemical Name
1,3-Adamantanediamine
Synonyms
13AD;1,3-Adamantanediamine;1,3-Diaminoadamantane;1, 3-Amantadane Diamine;4. 1,3-diaminoadamantane;Adamantan-1,3-diyldiamin;10303-95-4 1,3-Adamantanediamine;1,3-Adamantanediaminewith2HClsalt;Benzeneethanol,5-amino-β,β-dimethyl-;Tricyclo[3.3.1.13,7]decane-1,3-diamine
CBNumber
CB11030056
Molecular Formula
C10H18N2
Formula Weight
166.26
MOL File
10303-95-4.mol
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1,3-Adamantanediamine Property

Boiling point:
249 °C
Density 
1.153
Flash point:
122 °C
pka
10.73±0.40(Predicted)
form 
powder to crystal
color 
White to Almost white
CAS DataBase Reference
10303-95-4(CAS DataBase Reference)
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Safety

HS Code 
2921.30.5000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical
Product number
A3265
Product name
Adamantane-1,3-diamine
Packaging
1G
Price
$134
Updated
2024/03/01
TCI Chemical
Product number
A3265
Product name
Adamantane-1,3-diamine
Packaging
5G
Price
$536
Updated
2024/03/01
TRC
Product number
A220263
Product name
1,3-Adamantanediamine
Packaging
100mg
Price
$90
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA170085
Product name
Adamantane-1,3-diamine
Packaging
100mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA170085
Product name
Adamantane-1,3-diamine
Packaging
250mg
Price
$100
Updated
2021/12/16
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1,3-Adamantanediamine Chemical Properties,Usage,Production

Uses

1,3-Adamantanediamine is used in preparation method of SSZ-13 molecular sieve from β molecular sieve.

Preparation

1,3-Adamantanediamine synthesis: 1,3-Adamantane dicarboxylic acid (12 g) was mixed with 50 mL of SOCl2 and the mixture was refluxed for 3 h. Excessive SOCl2 was evaporated and 1,3-adamantane dicarbonyl dichloride was obtained as white solid, dissolved in dried benzene and added to cold ammonia solution slowly, during which a white precipitate was formed gradually filtered and then washed the precipitate several times with water to give 1,3-disaminoacyladamantane as white solid, recrystallized from ethanol. White solid, yield 10.58 g (89 %).

Purification Methods

Purify it by zone refining. The dibenzoyl derivative has m 248o, and the dihydrochloride salt has m 310o (360o) after recrystallisation from aqueous EtOH or EtOH/Et2O. [Prelog & Seiwerth Chem Ber 74 1769 1941, Stetter & Wulff Chem Ber 93 1366 1960.]

1,3-Adamantanediamine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,3-Adamantanediamine manufacturers

Shanghai Qyubiotech Co., Ltd.
Product
1,3-Adamantanediamine 10303-95-4
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
99%+
Supply Ability
10000kg per month
Release date
2023-04-19
SHAANXI LIGHTE OPTOELECTRONICS MATERIAL CO., LTD
Product
1,3-Adamantanediamine 10303-95-4
Price
US $0.00-0.00/Kg
Min. Order
1Kg
Purity
99% HPLC
Supply Ability
20 tons
Release date
2022-11-09
Zhuozhou Wenxi import and Export Co., Ltd
Product
1,3-Adamantanediamine 10303-95-4
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-11

10303-95-4, 1,3-AdamantanediamineRelated Search:


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