1,3-Adamantanediamine
- Product Name
- 1,3-Adamantanediamine
- CAS No.
- 10303-95-4
- Chemical Name
- 1,3-Adamantanediamine
- Synonyms
- 13AD;1,3-Adamantanediamine;1,3-Diaminoadamantane;1, 3-Amantadane Diamine;4. 1,3-diaminoadamantane;Adamantan-1,3-diyldiamin;10303-95-4 1,3-Adamantanediamine;1,3-Adamantanediaminewith2HClsalt;Benzeneethanol,5-amino-β,β-dimethyl-;Tricyclo[3.3.1.13,7]decane-1,3-diamine
- CBNumber
- CB11030056
- Molecular Formula
- C10H18N2
- Formula Weight
- 166.26
- MOL File
- 10303-95-4.mol
1,3-Adamantanediamine Property
- Boiling point:
- 249 °C
- Density
- 1.153
- Flash point:
- 122 °C
- pka
- 10.73±0.40(Predicted)
- form
- powder to crystal
- color
- White to Almost white
- CAS DataBase Reference
- 10303-95-4(CAS DataBase Reference)
Safety
- HS Code
- 2921.30.5000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- A3265
- Product name
- Adamantane-1,3-diamine
- Packaging
- 1G
- Price
- $134
- Updated
- 2024/03/01
- Product number
- A3265
- Product name
- Adamantane-1,3-diamine
- Packaging
- 5G
- Price
- $536
- Updated
- 2024/03/01
- Product number
- A220263
- Product name
- 1,3-Adamantanediamine
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FA170085
- Product name
- Adamantane-1,3-diamine
- Packaging
- 250mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- CS-0094364
- Product name
- Adamantane-1,3-diamine
- Packaging
- 1g
- Price
- $464
- Updated
- 2021/12/16
1,3-Adamantanediamine Chemical Properties,Usage,Production
Uses
1,3-Adamantanediamine is used in preparation method of SSZ-13 molecular sieve from β molecular sieve.
Preparation
1,3-Adamantanediamine synthesis: 1,3-Adamantane dicarboxylic acid (12 g) was mixed with 50 mL of SOCl2 and the mixture was refluxed for 3 h. Excessive SOCl2 was evaporated and 1,3-adamantane dicarbonyl dichloride was obtained as white solid, dissolved in dried benzene and added to cold ammonia solution slowly, during which a white precipitate was formed gradually filtered and then washed the precipitate several times with water to give 1,3-disaminoacyladamantane as white solid, recrystallized from ethanol. White solid, yield 10.58 g (89 %).
Purification Methods
Purify it by zone refining. The dibenzoyl derivative has m 248o, and the dihydrochloride salt has m 310o (360o) after recrystallisation from aqueous EtOH or EtOH/Et2O. [Prelog & Seiwerth Chem Ber 74 1769 1941, Stetter & Wulff Chem Ber 93 1366 1960.]
1,3-Adamantanediamine Preparation Products And Raw materials
Raw materials
Preparation Products
1,3-Adamantanediamine Suppliers
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View Lastest Price from 1,3-Adamantanediamine manufacturers
- Product
- 1,3-Adamantanediamine 10303-95-4
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%+
- Supply Ability
- 10000kg per month
- Release date
- 2023-04-19
- Product
- 1,3-Adamantanediamine 10303-95-4
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1Kg
- Purity
- 99% HPLC
- Supply Ability
- 20 tons
- Release date
- 2022-11-09
- Product
- 1,3-Adamantanediamine 10303-95-4
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11