1-(2-METHOXY-PHENYL)-ETHYLAMINE
- Product Name
- 1-(2-METHOXY-PHENYL)-ETHYLAMINE
- CAS No.
- 40023-74-3
- Chemical Name
- 1-(2-METHOXY-PHENYL)-ETHYLAMINE
- Synonyms
- AURORA KA-7736;ASINEX-REAG BAS 05269105;2-Methoxy-α-methylbenzylamine;1-(2-METHOXYPHENYL)ETHANAMINE;1-(2-METHOXY-PHENYL)-ETHYLAMINE;2-Methoxy-α-methylbenzenemethanamine;2-Methoxy-α-methylbenzenemethanamine;Benzenemethanamine, 2-methoxy-α-methyl-;Benzenemethanamine, 2-methoxy-a-methyl-;BenzeneMethanaMine, 2-Methoxy-.alpha.-Methyl-
- CBNumber
- CB1104943
- Molecular Formula
- C9H13NO
- Formula Weight
- 151.21
- MOL File
- Mol file
1-(2-METHOXY-PHENYL)-ETHYLAMINE Property
- Boiling point:
- 244.1±23.0 °C(Predicted)
- Density
- 1.003±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 9.13±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P363Wash contaminated clothing before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M350150
- Product name
- 1-(2-Methoxyphenyl)ethylamine
- Packaging
- 500mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 018697
- Product name
- 1-(2-Methoxy-phenyl)-ethylamine
- Packaging
- 1g
- Price
- $299
- Updated
- 2021/12/16
- Product number
- CHM0032873
- Product name
- 1-(2-METHOXY-PHENYL)-ETHYLAMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $852.55
- Updated
- 2021/12/16
- Product number
- 018697
- Product name
- 1-(2-Methoxy-phenyl)-ethylamine
- Packaging
- 5g
- Price
- $885
- Updated
- 2021/12/16
- Product number
- CHM0032873
- Product name
- 1-(2-METHOXY-PHENYL)-ETHYLAMINE
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1227.82
- Updated
- 2021/12/16
1-(2-METHOXY-PHENYL)-ETHYLAMINE Chemical Properties,Usage,Production
Synthesis
579-74-8
40023-74-3
GENERAL PROCEDURE: To a saturated NH4OAc ethanol solution (40 mL) was added activated zinc powder (5 eq.), 2'-methoxyacetophenone (1 eq.), NaBH3CN (3 eq.), and 30% aqueous ammonia solution (10 mL), in that order. The reaction mixture was stirred at 80 °C for 36 hours. After completion of the reaction, it was cooled to room temperature and concentrated under reduced pressure. The residue was dissolved with dichloromethane and adjusted to alkaline with 1 M NaOH aqueous solution (50 mL). The organic phase was separated and the aqueous phase was back-extracted with dichloromethane (2 x 25 mL). The organic phases were combined and acidified with HCl to pH 2.0. The organic layer was separated and the aqueous layer was extracted with dichloromethane (2 x 25 mL). After the aqueous layer was adjusted to pH 10.0 with NaOH, the organic layer was extracted with dichloromethane (3 × 25 mL). The organic layers were combined, dried with anhydrous Na2SO4 and the solvent was evaporated under reduced pressure to obtain the target product 1-(2-methoxyphenyl)ethylamine.
References
[1] Science, 2017, vol. 358, # 6361, p. 326 - 332
[2] Chemistry - A European Journal, 2014, vol. 20, # 1, p. 245 - 252
[3] Farmaco, 1991, vol. 46, # 7-8, p. 861 - 872
[4] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 13, p. 3592 - 3602
[5] Chirality, 2018, vol. 30, # 7, p. 900 - 906
1-(2-METHOXY-PHENYL)-ETHYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-(2-METHOXY-PHENYL)-ETHYLAMINE manufacturers
- Product
- 1-(2-METHOXY-PHENYL)-ETHYLAMINE 40023-74-3
- Price
- US $1.00-2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100000KG
- Release date
- 2024-08-16