Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI)

Product Name: Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI)
CAS No.: 819069-57-3
Chemical Name: Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI)
Synonyms: 3-broMo-6-Methoxy-2,4-diMethylpyridine;Pyridine, 3-bromo-6-methoxy-2,4-dimethyl-;Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI)
CBNumber: CB11059888
Molecular Formula: C8H10BrNO
Formula Weight: 216.08
MOL File: 819069-57-3.mol

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Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) Property

Boiling point:: 243℃
Density: 1.39
Flash point:: 101℃
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B429363
Product name: 3-bromo-6-methoxy-2,4-dimethylpyridine
Packaging: 10mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: 2683AC
Product name: 3-Bromo-6-methoxy-2,4-dimethylpyridine
Packaging: 250mg
Price: $437
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0364630
Product name: 3-BROMO-6-METHOXY-2,4-DIMETHYLPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $499.27
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB170455
Product name: 3-Bromo-6-methoxy-2,4-dimethylpyridine
Packaging: 100mg
Price: $500
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB170455
Product name: 3-Bromo-6-methoxy-2,4-dimethylpyridine
Packaging: 250mg
Price: $750
Updated: 2021/12/16

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Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) Chemical Properties,Usage,Production

Synthesis

89694-55-3

74-88-4

819069-57-3

Step 2: Synthesis of 3-bromo-6-methoxy-2,4-dimethylpyridine In a 500 mL three-necked round-bottomed flask, nitrogen displacement was performed and an inert atmosphere was maintained. To the flask was added 5-bromo-4,6-dimethylpyridin-2(1H)-one (3.90 g, 19.30 mmol, 1.00 eq.), dichloromethane (150 mL) and silver carbonate (Ag2CO3, 7.34 g, 0.0266 mol, 1.40 eq.). Iodomethane (Mel, 28.4 g, 0.2 mol, 10.50 eq.) was slowly added to the mixture with stirring. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the solid was collected by filtration and the filter cake was washed with dichloromethane (50 mL). The combined filtrates were concentrated under reduced pressure to give 3.91 g (94% yield) of 3-bromo-6-methoxy-2,4-dimethylpyridine as a brown oil. Mass Spectrometry (ESI) m/z measured value: C8H10BrNO [M + H]+: 216.

References

[1] Patent: US2015/315198, 2015, A1. Location in patent: Paragraph 0393; 0394
[2] Journal of Organic Chemistry, 2004, vol. 69, # 26, p. 9215 - 9223

Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) Suppliers

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View Lastest Price from Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) manufacturers

Career Henan Chemical Co

Product: Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI) 819069-57-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%-99%
Supply Ability: 1ton
Release date: 2020-01-08

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Pyridine, 3-bromo-6-methoxy-2,4-dimethyl- (9CI)

3-broMo-6-Methoxy-2,4-diMethylpyridine

Pyridine, 3-bromo-6-methoxy-2,4-dimethyl-

819069-57-3

METHYL