ChemicalBook > CAS DataBase List > 1-Aminopyrene

1-Aminopyrene

Product Name: 1-Aminopyrene
CAS No.: 1606-67-3
Chemical Name: 1-Aminopyrene
Synonyms: pyren-1-amine;1-Pyrenamin;1-PYRENAMINE;3-AMINOPYRENE;1-AMINOPYRENE;Pyrene, amino-;pyren-1-ylamine;1-Aminopyrene,97%;1-AMinopyrene 97%;1-Aminopyrene >
CBNumber: CB1107595
Molecular Formula: C16H11N
Formula Weight: 217.27
MOL File: 1606-67-3.mol

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1-Aminopyrene Property

Melting point:: 115-117 °C (lit.)
Boiling point:: 347.82°C (rough estimate)
Density: 1.1227 (rough estimate)
refractive index: 1.8230 (estimate)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), Methanol (Sparingly)
form: Powder
pka: 4.32±0.30(Predicted)
color: Yellow to green
Water Solubility: Insoluble in water (0.576 mg/L at 25°C).
BRN: 1875737
Stability:: Stable. Incompatible with strong oxidizing agents.
InChIKey: YZVWKHVRBDQPMQ-UHFFFAOYSA-N
CAS DataBase Reference: 1606-67-3(CAS DataBase Reference)
NIST Chemistry Reference: 1-Aminopyrene(1606-67-3)
EPA Substance Registry System: 1-Pyrenamine (1606-67-3)

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Safety

Hazard Codes: Xn
Risk Statements: 22-40-21/22
Safety Statements: 45-36/37
WGK Germany: 3
RTECS: UR2275000
TSCA: Yes
HS Code: 29214990
Toxicity: mouse,LD50,intraperitoneal,250mg/kg (250mg/kg),Archives Internationales de Pharmacodynamie et de Therapie. Vol. 135, Pg. 376, 1962.

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: A77903
Product name: 1-Aminopyrene
Purity: 97%
Packaging: 1g
Price: $95.4
Updated: 2025/07/31

TCI Chemical

Product number: A0632
Product name: 1-Aminopyrene
Purity: >98.0%(HPLC)(T)
Packaging: 1g
Price: $67
Updated: 2025/07/31

TCI Chemical

Product number: A3241
Product name: 1-Aminopyrene (purified by sublimation)
Packaging: 1G
Price: $131
Updated: 2025/07/31

TCI Chemical

Product number: A0632
Product name: 1-Aminopyrene
Purity: >98.0%(HPLC)(T)
Packaging: 5g
Price: $223
Updated: 2025/07/31

TCI Chemical

Product number: A0632
Product name: 1-Aminopyrene
Purity: >98.0%(HPLC)(T)
Packaging: 25g
Price: $780
Updated: 2025/07/31

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1-Aminopyrene Chemical Properties,Usage,Production

Chemical Properties

yellow-green powder

Uses

It acts as a precursor molecule for production of other fluorescent probes such as 1-Azidopyrene, APTS, and N-(1-Pyrene)iodoacetamide.

Uses

1-Aminopyrene is used in the synthesis of novel fluorescent nanoscale ionic silicate platelets for use in bacterial detection and other biosensor applications.

General Description

Colorless crystals. Yellow needles from hexane, melting point 117-8°C.

Reactivity Profile

1-Aminopyrene neutralizes acids in exothermic reactions to form salts plus water. May be incompatible with isocyanates, halogenated organics, peroxides, phenols (acidic), epoxides, anhydrides, and acid halides. May generate hydrogen, a flammable gas, in combination with strong reducing agents such as hydrides.

Fire Hazard

1-Aminopyrene is probably combustible.

Synthesis

5522-43-0

1606-67-3

Under argon protection and magnetic stirring conditions, 1-nitropyrene (1.00 g, 4.0 mmol) was dissolved in 60 mL of ethyl acetate with tin(II) chloride dihydrate (4.35 g, 19.2 mmol) in a 250 mL three-necked round-bottomed flask. The reaction mixture was heated to reflux for 6 hours. After the reaction was completed, it was cooled to room temperature and the pH was adjusted to 8.0 by slowly adding 20% (m/v) aqueous sodium carbonate solution and continued stirring for 1 hour. The reaction mixture was extracted three times with ethyl acetate, the organic phases were combined and dried with anhydrous magnesium sulfate. The desiccant was removed by filtration and the solvent was evaporated under reduced pressure to give a light green solid product 1-aminopyrene 0.80 g (90% yield). The product was characterized by the following data: melting point 115-116 °C (literature value: 115-117 °C); IR (KBr) νmax/cm?1: 3345-3387 (N-H stretching vibration), 3036 (aromatic C-H stretching vibration), 1623-1512 (C=C stretching vibration); 1H NMR (400 MHz, DMSO-d?) δ: 8.24 (d, 1H, J=9.4 Hz, Ar-H), 7.97 (d, 2H, J=7.8 Hz, Ar-H), 7.94 (d, 1H, J=7.8 Hz, Ar-H), 7.89 (d, 1H, J=9.0 Hz, Ar-H), 7.86 (d, 1H, J=8.6 Hz, Ar-H), 7.85 (t, 1H, J=7.6 Hz, Ar-H), 7.69 (d, 1H, J=8.6 Hz, Ar-H), 7.34 (d, 1H, J=8.2 Hz, Ar-H), 6.33 (s, 2H, NH?).

Purification Methods

1-Aminopyrene [1606-67-3] M 217.3, m 117-118o, pK 1 2.91 (50% aqueous EtOH), pK 2 2.77 (50% aqueous EtOH). Crystallise it from hexane. [Beilstein 12 IV 3460.]

References

[1] Analytical Chemistry, 1988, vol. 60, # 3, p. 194 - 199
[2] Organic and Biomolecular Chemistry, 2018, vol. 16, # 41, p. 7663 - 7673
[3] Tetrahedron Letters, 1998, vol. 39, # 40, p. 7243 - 7246
[4] Synthetic Communications, 1991, vol. 21, # 2, p. 161 - 165
[5] Bioorganic and Medicinal Chemistry, 2001, vol. 9, # 3, p. 593 - 605

1-Aminopyrene Preparation Products And Raw materials

Raw materials

Sodium hypochlorite Sodium azide Acetyl chloride Pyrene Aluminum chloride Bromine Dichloromethane Methanol Sodium hydroxide Pyridine Thionyl chloride Ammonia

Preparation Products

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View Lastest Price from 1-Aminopyrene manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: 1-Aminopyrene 1606-67-3
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98.0%
Supply Ability: 10000KGS
Release date: 2025-03-06

Hebei Xinsheng New Material Technology Co., LTD.

Product: 1-Aminopyrene 1606-67-3
Price: US $35.00-25.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 Ton
Release date: 2023-10-07

Hebei Xinsheng New Material Technology Co., LTD.

Product: 1-Aminopyrene 1606-67-3
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 30000 Kg
Release date: 2023-11-17

1606-67-3, 1-AminopyreneRelated Search:

4-Amino-benzenesulfonic acid monosodium salt Glucosamine EC 2.6.1.2 Sulfamic acid Acetaminophen Aminopyrine N-(1-PYRENYL)MALEIMIDE 1,6-DINITROPYRENE APTS 1,8-DINITROPYRENE 1-Nitropyrene 1,6-DIAMINOPYRENE 1,3-DINITROPYRENE Pyrene 1-PYRENEISOTHIOCYANATE 6-BROMO-1-AMINOPYRENE 6-NITROBENZ(A)PYRENE 1,8-DIAMINOPYRENE

3-AMINOPYRENE

1-PYRENAMINE

1-AMINOPYRENE

TIMTEC-BB SBB003375

1-Pyrenamin

Pyrene, amino-

pyren-1-ylamine

pyren-1-amine

1-Pyrenamine, 3-Aminopyrene

1-Aminopyrene,97%

1-AMINOPYRENE PURUM 98%

1-AMinopyrene, 97% 250MG

1-AMinopyrene 97%

1-Aminopyrene (purified by sublimation)

1-Aminopyrene≥ 98% (HPLC)

1-Aminopyrene &gt

1606-67-3

1606-76-3

C16H11N

Organic Building Blocks

Nitrogen Compounds

Pyrenes

C11 to C37

Building Blocks

Amines

Pyrenes

Aromatic Hydrocarbons (substituted) & Derivatives