ChemicalBook > CAS DataBase List > 2-Pyrimidinamine, N-methyl- (9CI)

2-Pyrimidinamine, N-methyl- (9CI)

Product Name
2-Pyrimidinamine, N-methyl- (9CI)
CAS No.
931-61-3
Chemical Name
2-Pyrimidinamine, N-methyl- (9CI)
Synonyms
NSC 102272;N-Methyl-2-pyrimidinamine;2-PyriMidinaMine, N-Methyl-;methyl(pyrimidin-2-yl)amine;2-Pyrimidinamine, N-methyl- (9CI);2-Pyrimidinamine, N-methyl- (9CI) ISO 9001：2015 REACH
CBNumber
CB11081371
Molecular Formula
C5H7N3
Formula Weight
109.13
MOL File
931-61-3.mol
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2-Pyrimidinamine, N-methyl- (9CI) Property

Melting point:
60-62℃
Boiling point:
216℃
Density 
1.144
Flash point:
85℃
storage temp. 
2-8°C(protect from light)
form 
Solid
pka
3.90±0.10(Predicted)
Appearance
White to yellow Solid
InChI
InChI=1S/C5H7N3/c1-6-5-7-3-2-4-8-5/h2-4H,1H3,(H,6,7,8)
InChIKey
BQNXHDSGGRTFNX-UHFFFAOYSA-N
SMILES
C1(NC)=NC=CC=N1
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Safety

HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
M103138
Product name
N-methylpyrimidin-2-amine
Packaging
5mg
Price
$45
Updated
2021/12/16
TRC
Product number
M103138
Product name
N-methylpyrimidin-2-amine
Packaging
10mg
Price
$60
Updated
2021/12/16
ChemScene
Product number
CS-0061723
Product name
N-Methylpyrimidin-2-amine
Packaging
250mg
Price
$71
Updated
2021/12/16
AK Scientific
Product number
J55249
Product name
2-(Methylamino)pyrimidine
Packaging
100mg
Price
$77
Updated
2021/12/16
ChemScene
Product number
CS-0061723
Product name
N-Methylpyrimidin-2-amine
Packaging
1g
Price
$142
Updated
2021/12/16
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2-Pyrimidinamine, N-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

1722-12-9

74-89-5

931-61-3

Step 1: Synthesis of N-methylpyrimidin-2-amine To a solution of 2-chloropyrimidine (1 g, 8.7 mmol) in methanol (10 mL) was slowly added a methanolic solution of 2Methylamine (13.2 mL, 26.2 mmol) followed by potassium carbonate (2.5 g, 18 mmol). The reaction flask was sealed and the reaction was stirred at 80 °C overnight. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated by rotary evaporator to remove volatile solvents. The residue was extracted by liquid-liquid partition with distilled water and dichloromethane. The organic layer was separated, dried over anhydrous sodium sulfate, filtered and concentrated to give 2-methylaminopyrimidine (290 mg, 30% yield) as a brown oil.

References

[1] Bulletin of the Chemical Society of Japan, 1998, vol. 71, # 8, p. 1973 - 1991
[2] Journal of Medicinal Chemistry, 2013, vol. 56, # 17, p. 6626 - 6637
[3] Molecules, 2004, vol. 9, # 7, p. 520 - 526
[4] Patent: WO2011/71716, 2011, A1. Location in patent: Page/Page column 99
[5] Journal of the American Chemical Society, 1954, vol. 76, p. 1065,1067

2-Pyrimidinamine, N-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Pyrimidinamine, N-methyl- (9CI) manufacturers

Dideu Industries Group Limited
Product
2-Pyrimidinamine, N-methyl- (9CI) 931-61-3
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-13
Career Henan Chemical Co
Product
2-Pyrimidinamine, N-methyl- (9CI) 931-61-3
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
25kg
Release date
2019-07-12

931-61-3, 2-Pyrimidinamine, N-methyl- (9CI)Related Search:

Pirimiphos ethyl ETHIRIMOL Dipyridamole 2-Cyanoamino-4,6-dihydroxypyrimidine Pirimicarb Pipemidic acid 2-(1-Piperazinyl)pyrimidine Pirimiphos-methyl BUPIRIMATE N-[(4-methoxyphenyl)methyl]pyrimidin-2-amine 2-DIMETHYLAMINO-6-HYDROXYPURINE 2-PHENYLAMINOADENOSINE 2-CYANIMINO-4-METHYLPYRIMIDINE 2-ACETOACETAMINOPYRIMIDINE 2-CYANOAMINO-4-HYDROXY-6-METHYLPYRIMIDINE 4-AMINO-2-CYANIMINO-6-HYDROXYPYRIMIDINE 2-(1H-BENZIMIDAZOL-2-YLAMINO)-6-METHYL-4-PYRIMIDINOL N-(4-METHYLQUINAZOLIN-2-YL)GUANIDINE

  • 2-Pyrimidinamine, N-methyl- (9CI)
  • N-Methyl-2-pyrimidinamine
  • methyl(pyrimidin-2-yl)amine
  • NSC 102272
  • 2-PyriMidinaMine, N-Methyl-
  • 2-Pyrimidinamine, N-methyl- (9CI) ISO 9001：2015 REACH
  • 931-61-3
  • PYRIMIDINE