ChemicalBook > CAS DataBase List > 2-BROMO-3-AMINOANISOLE

2-BROMO-3-AMINOANISOLE

Product Name: 2-BROMO-3-AMINOANISOLE
CAS No.: 112970-44-2
Chemical Name: 2-BROMO-3-AMINOANISOLE
Synonyms: SA021377;2-Bromo-3-methoxyaniline;2-bromo-3-methoxybenzenamine;2-Bromo-3-methoxy-phenylamine;BenzenaMine, 2-broMo-3-Methoxy-;3-AMino-2-broMoanisole[2-BroMo-3-Methoxyaniline]
CBNumber: CB11091985
Molecular Formula: C7H8BrNO
Formula Weight: 202.05
MOL File: 112970-44-2.mol

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2-BROMO-3-AMINOANISOLE Property

Boiling point:: 273.1±20.0 °C(Predicted)
Density: 1.531±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: Off white/cream, fluffy/wooly flakes
pka: 2.11±0.10(Predicted)
Appearance: Gray to black Solid

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Safety

HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B416658
Product name: 2-Bromo-3-methoxyaniline
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142812
Product name: 2-Bromo-3-methoxyaniline
Packaging: 250mg
Price: $67.5
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4656-9-17
Product name: 2-Bromo-3-methoxyaniline
Packaging: 1g
Price: $74
Updated: 2021/12/16

Oakwood

Product number: 223772
Product name: 2-Bromo-3-methoxyaniline
Purity: 95+%
Packaging: 250mg
Price: $82
Updated: 2021/12/16

Apolloscientific

Product number: OR70043
Product name: 2-Bromo-3-methoxyaniline
Packaging: 5g
Price: $187
Updated: 2021/12/16

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2-BROMO-3-AMINOANISOLE Chemical Properties,Usage,Production

Uses

2-Bromo-3-methoxyaniline can be used to treat epilepsy.

Synthesis

67853-37-6

112970-44-2

Step 1. Synthesis of 2-bromo-3-methoxyaniline (C23) Iron powder (1.94 g, 34 mmol) was added to an ethanol solution (18 mL) of 2-bromo-1-methoxy-3-nitrobenzene (2.50 g, 10.77 mmol) followed by concentrated hydrochloric acid (1 mL). The reaction mixture was heated to reflux for 1.5 hours. Upon completion of the reaction, the mixture was cooled to room temperature, filtered through a pad of diatomaceous earth, and the filtrate was concentrated under vacuum to afford the title compound 2-bromo-3-methoxyaniline as a solid. Yield: 2.57 g (10.77 mmol, 100%). LCMS m/z: 202.1 [M + H]+. 1H NMR (400 MHz, CD3OD) δ: 3.77 (s, 3H), 6.30 (d, J = 8.0 Hz, 1H), 6.43 (d, J = 8.0 Hz, 1H), 6.98 (dd, J = 8.0, 8.0 Hz, 1H).

References

[1] Patent: US2012/252758, 2012, A1. Location in patent: Page/Page column 27
[2] Journal of Medicinal Chemistry, 2015, vol. 58, # 23, p. 9287 - 9295
[3] Patent: US2007/78147, 2007, A1. Location in patent: Page/Page column 67
[4] Patent: WO2018/13774, 2018, A1. Location in patent: Page/Page column 318
[5] Patent: EP3239143, 2017, A2. Location in patent: Paragraph 0441

2-BROMO-3-AMINOANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMO-3-AMINOANISOLE manufacturers

Career Henan Chemical Co

Product: 2-BROMO-3-AMINOANISOLE 112970-44-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-05-23

112970-44-2, 2-BROMO-3-AMINOANISOLERelated Search:

2,6-Dibromo-3,4,5-trimethoxyaniline 2-BROMO-4-CHLORO-3,6-DINITROPHENYL METHYL ETHER N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)-2-CHLOROBENZAMIDE 2-Bromo-3-nitroanisole N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)-2-FURAMIDE N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)-1-BENZOFURAN-2-CARBOXAMIDE 2',4',5',7'-TETRABROMORHODAMINE 123 BROMIDE AURORA KA-4062 N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)PENTANAMIDE 2-BROMO-3-AMINOANISOLE 2-Bromo-3,4,5-trimethoxyaniline AURORA KA-4057 Methyl3-Bromo-4,5-dimethoxyanthranilate N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)-2-METHYLPROPANAMIDE N-(4-AMINO-3,5-DIBROMO-2-METHOXYPHENYL)THIOPHENE-2-CARBOXAMIDE AURORA KA-5558

2-Bromo-3-methoxyaniline

2-bromo-3-methoxybenzenamine

2-Bromo-3-methoxy-phenylamine

SA021377

BenzenaMine, 2-broMo-3-Methoxy-

3-AMino-2-broMoanisole[2-BroMo-3-Methoxyaniline]

112970-44-2