7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Product Name
- 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- CAS No.
- 923282-39-7
- Chemical Name
- 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Synonyms
- 7-chloro-1-methylpyrazolo[4,3-d]pyrimidine;7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine;1H-Pyrazolo[4,3-d]pyrimidine, 7-chloro-1-methyl-
- CBNumber
- CB11094173
- Molecular Formula
- C6H5ClN4
- Formula Weight
- 168.58
- MOL File
- 923282-39-7.mol
7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine Property
- Boiling point:
- 294.6±20.0 °C(Predicted)
- Density
- 1.59±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 1.73±0.30(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C374203
- Product name
- 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- C374203
- Product name
- 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- FC144367
- Product name
- 7-Chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Packaging
- 50mg
- Price
- $120
- Updated
- 2021/12/16
- Product number
- FC144367
- Product name
- 7-Chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine
- Packaging
- 100mg
- Price
- $180
- Updated
- 2021/12/16
- Product number
- NUC0001112
- Product name
- 7-CHLORO-1-METHYL-1H-PYRAZOLO[4,3-D]PYRIMIDINE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $347.55
- Updated
- 2021/12/16
7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine Chemical Properties,Usage,Production
Synthesis
314021-93-7
923282-39-7
Procedure for the synthesis of compound 9: To a 10 mL solution of thionyl chloride of 1-methyl-1H-pyrazolo[4,3-d]pyrimidin-7-ol (8, 0.835 g, 5.5 mmol) was added 0.5 mL of N,N-dimethylformamide (DMF). The reaction mixture was heated to 90 °C under nitrogen protection with continuous stirring for 1 hour. Upon completion of the reaction, the mixture was cooled to room temperature and the solvent was subsequently removed by distillation under reduced pressure. Water was added to the resulting residue and extracted with dichloromethane (3 x 10 mL). The organic phases were combined, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure to afford 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine (9, 0.94 g, 100% yield). The product was detected by electrospray mass spectrometry (ES-MS) and showed m/e = 169 ([M + H]+).
References
[1] Patent: US2007/27166, 2007, A1. Location in patent: Page/Page column 80
7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine Preparation Products And Raw materials
Raw materials
Preparation Products
7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine Suppliers
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View Lastest Price from 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine manufacturers
- Product
- 7-Chloro-1-Methyl-1H-pyrazolo[4,3-d]pyriMidine 923282-39-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2020-05-15
- Product
- 7-chloro-1-methyl-1H-pyrazolo[4,3-d]pyrimidine 923282-39-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-12-17