(3S,4S)-Pyrrolidine-3,4-diol
- Product Name
- (3S,4S)-Pyrrolidine-3,4-diol
- CAS No.
- 90481-32-6
- Chemical Name
- (3S,4S)-Pyrrolidine-3,4-diol
- Synonyms
- EOS-62153;(3S,4S)-3,4-Pyrrolidinediol;(3s,4s)-pyrrolidine-3,4-dio;(3S,4S)-Pyrrolidine-3,4-diol;3,4-Pyrrolidinediol, (3S,4S)-;1,4-dideoxy-1,4-iminothreitol;(3S,4S)-3,4-Dihydroxypyrrolidine
- CBNumber
- CB11267603
- Molecular Formula
- C4H9NO2
- Formula Weight
- 103.12
- MOL File
- 90481-32-6.mol
(3S,4S)-Pyrrolidine-3,4-diol Property
- Boiling point:
- 232 °C
- Density
- 1.309
- Flash point:
- 144 °C
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- solid
- pka
- 14.08±0.40(Predicted)
- Appearance
- White to off-white Solid
- optical activity
- 20.6°(C=1.10g/100ml MEOH)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- P999933
- Product name
- (3S,4S)-Pyrrolidine-3,4-diol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- P999933
- Product name
- (3S,4S)-Pyrrolidine-3,4-diol
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 4H56-1-821
- Product name
- (3S,4S)-Pyrrolidine-3,4-diol
- Purity
- 97.0%
- Packaging
- 250mg
- Price
- $340
- Updated
- 2021/12/16
- Product number
- 224938
- Product name
- (3S,4S)-Pyrrolidine-3,4-diol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- Z5315
- Product name
- (3S,4S)-Pyrrolidine-3,4-diol
- Packaging
- 100mg
- Price
- $131
- Updated
- 2021/12/16
(3S,4S)-Pyrrolidine-3,4-diol Chemical Properties,Usage,Production
Synthesis
90365-74-5
90481-32-6
General procedure for the synthesis of (3S,4S)-pyrrolidine-3,4-diol from (3S,4S)-1-benzylpyrrolidine-3,4-diol: 10% palladium-carbon catalyst (100 mg) and acetic acid (10 mL) were added to a solution of (3S,4S)-1-benzylpyrrolidine-3,4-diol (522 mg) in ethanol (15 mL). The mixture was placed in a Parr hydrogenation unit and reacted at 40 psi hydrogen pressure for 7 hours at room temperature. Upon completion of the reaction, the reaction solution was filtered through diatomaceous earth and the filtrate was concentrated under reduced pressure. To the concentrated residue was added 4N hydrochloric acid-dioxane solution and concentrated again under reduced pressure to give (3S,4S)-pyrrolidine-3,4-diol (373 mg) as a yellow solid in 99% yield. Mass spectrum (APCI) m/z: 104 [M + H]+.
References
[1] Synthetic Communications, 2008, vol. 38, # 14, p. 2374 - 2384
[2] Patent: EP2390254, 2011, A1. Location in patent: Page/Page column 86
[3] Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 16, p. 2385 - 2390
[4] Angewandte Chemie, 1984, vol. 96, # 6, p. 425 - 426
[5] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 12, p. 3965 - 3973
(3S,4S)-Pyrrolidine-3,4-diol Preparation Products And Raw materials
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View Lastest Price from (3S,4S)-Pyrrolidine-3,4-diol manufacturers
- Product
- (3S,4S)-Pyrrolidine-3,4-diol 90481-32-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-09-26