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2-PHENYLETHYLMETHANESULPHONATE

Product Name
2-PHENYLETHYLMETHANESULPHONATE
CAS No.
20020-27-3
Chemical Name
2-PHENYLETHYLMETHANESULPHONATE
Synonyms
3-phenylpropane-1-sulfonate;2-PHENYLETHYLMETHANESULPHONATE;2-phenylethyl methanesulfonate;Methanesulfonic acid, 2-phenylethyl ester
CBNumber
CB11445065
Molecular Formula
C9H12O3S
Formula Weight
200.25
MOL File
20020-27-3.mol
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2-PHENYLETHYLMETHANESULPHONATE Property

Boiling point:
358.1±21.0 °C(Predicted)
Density 
1.205±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Abosyn
Product number
61-10142
Product name
Phenethylmethanesulfonate
Purity
95-98%
Packaging
1g
Price
$225
Updated
2021/12/16
Alichem
Product number
20020273
Product name
Phenethylmethanesulfonate
Packaging
5g
Price
$352.8
Updated
2021/12/16
Crysdot
Product number
CD12098755
Product name
Phenethylmethanesulfonate
Purity
98%
Packaging
5g
Price
$356
Updated
2021/12/16
Crysdot
Product number
CD12098755
Product name
Phenethylmethanesulfonate
Purity
98%
Packaging
10g
Price
$594
Updated
2021/12/16
Alichem
Product number
20020273
Product name
Phenethylmethanesulfonate
Packaging
10g
Price
$594
Updated
2021/12/16
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2-PHENYLETHYLMETHANESULPHONATE Chemical Properties,Usage,Production

Synthesis

60-12-8

124-63-0

20020-27-3

GENERAL METHOD: Phenylethanol (2.14 mmol) was dissolved in anhydrous dichloromethane (6 mL) with triethylamine (0.36 mL, 2.59 mmol) under nitrogen protection and cooled to 0 °C. Subsequently, methanesulfonyl chloride (0.18 mL, 2.31 mmol) was slowly added dropwise and the reaction temperature was maintained at 0 °C for 1 hour. After that, the reaction mixture was gradually warmed up to room temperature and stirring was continued for 3 hours. After completion of the reaction, the reaction mixture was extracted with dichloromethane (3 x 30 mL). The organic phases were combined and washed sequentially with 10% aqueous hydrochloric acid and saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure, and the resulting crude product was purified by silica gel column chromatography, sequentially using dichloromethane and chloroform as eluents, to obtain the target product, phenethyl methanesulfonate, the structure of which was confirmed by the method described in the Supplementary Material.

References

[1] European Journal of Medicinal Chemistry, 2011, vol. 46, # 7, p. 3000 - 3012
[2] Synthetic Communications, 2011, vol. 41, # 5, p. 748 - 753
[3] Journal of Organic Chemistry, 1993, vol. 58, # 1, p. 272 - 274
[4] Tetrahedron, 2016, vol. 72, # 49, p. 8022 - 8030
[5] Journal of Medicinal Chemistry, 1990, vol. 33, # 10, p. 2807 - 2813

2-PHENYLETHYLMETHANESULPHONATE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-PHENYLETHYLMETHANESULPHONATE Suppliers

China 27 India 1 United States 4 Global 32
Guangzhou Isun Pharmaceutical Co., Ltd
Tel
020-39119399 18927568969
Fax
020-39119999
Email
isunpharm@qq.com
Country
China
ProdList
4720
Advantage
55
Shanghai Xingui Biotechnology Co., Ltd.
Tel
15121041756
Email
xingui2022@126.com
Country
China
ProdList
9968
Advantage
58
Shandong Xiya Chemical Co., Ltd.
Tel
4009903999 13395398332
Fax
0539-6365991
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sales@xiyashiji.com
Country
China
ProdList
20794
Advantage
60
MQ (shanghai) Pharmaceuticals Co., Ltd.
Tel
13761635123
Fax
1014988033@qq
Email
1014988033@qq.com
Country
China
ProdList
4941
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55
Aikon International Limited
Tel
025-58859352 18068836627
Fax
(5)02557626880
Email
dt3@aikonchem.com
Country
China
ProdList
15493
Advantage
58
Shanghai Jizhi Biochemical Technology Co. Ltd.
Tel
4009004166/18616739031 18616739031
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3007523370@qq.com
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China
ProdList
52687
Advantage
58
Nanjing xiangrui technology co. LTD
Tel
021-021-00000000 15715199582
Email
njrich168@163.com
Country
China
ProdList
768
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58
Changzhou Yinghao Technology Development Co., Ltd
Tel
15151934985
Email
sales@yingsapharm.com
Country
China
ProdList
4531
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58
Energy Chemical
Tel
021-58432009 400-005-6266
Fax
021-58436166
Email
marketing@energy-chemical.com
Country
China
ProdList
44918
Advantage
58
Shandong Territorial sea Biological Technology Co., LTD
Tel
15092083467
Email
18660263263@163.com
Country
China
ProdList
2785
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58

20020-27-3, 2-PHENYLETHYLMETHANESULPHONATERelated Search:

(R)-(-)-1-PHENYL-1,2-ETHANEDIOL 2-TOSYLATE (S)-(+)-1-PHENYL-1,2-ETHANEDIOL 2-TOSYLATE 2-INDANYL P-TOLUENESULFONATE 2-(4-NITROPHENYL)-ETHYLTOSYLATE PENTAFLUOROBENZYL P-TOLUENESULFONATE 4-BROMOPHENACYL-TRIFLUOROMESYLATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,5-DIMETHOXYBENZENESULFONATE 2-(4-ETHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 4-CHLOROBENZENESULFONATE 2-(4-ETHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 4-BROMOBENZENESULFONATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 4-(TERT-BUTYL)BENZENESULFONATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,5-DICHLOROBENZENESULFONATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,3,4,5,6-PENTAMETHYLBENZENESULFONATE 2-(4-methoxyphenyl)-4-oxo-4H-chromen-3-yl methanesulfonate 2-(4-ETHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,4,6-TRIMETHYLBENZENESULFONATE 2-(4-ETHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,5-DICHLOROBENZENESULFONATE 2-(4-ETHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 4-FLUOROBENZENESULFONATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 4-METHOXYBENZENESULFONATE 2-(4-METHOXYPHENYL)-4-OXO-4H-CHROMEN-3-YL 2,4-DICHLOROBENZENESULFONATE

  • 2-PHENYLETHYLMETHANESULPHONATE
  • 3-phenylpropane-1-sulfonate
  • Methanesulfonic acid, 2-phenylethyl ester
  • 2-phenylethyl methanesulfonate
  • 20020-27-3