ChemicalBook > CAS DataBase List > 2,5-DIMETHOXYBENZOYL CHLORIDE

2,5-DIMETHOXYBENZOYL CHLORIDE

Product Name
2,5-DIMETHOXYBENZOYL CHLORIDE
CAS No.
17918-14-8
Chemical Name
2,5-DIMETHOXYBENZOYL CHLORIDE
Synonyms
BUTTPARK 48\04-28;2,5-DIMETHOXYBENZOYL CHLORIDE;Benzoyl chloride, 2,5-dimethoxy-;2,5-Dimethoxybenzoic acid chloride;2,5-DIMETHOXYBENZENE-1-CARBONYL CHLORIDE;carbamic acid [5-[(3-nitrophenyl)thio]-4-propan-2-yl-1-prop-2-enyl-2-imidazolyl]methyl ester
CBNumber
CB1163469
Molecular Formula
C9H9ClO3
Formula Weight
200.62
MOL File
17918-14-8.mol
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2,5-DIMETHOXYBENZOYL CHLORIDE Property

Melting point:
53-54 °C(Solv: ligroine (8032-32-4))
Boiling point:
179°C/10mm
Density 
1.224±0.06 g/cm3(Predicted)
CAS DataBase Reference
17918-14-8(CAS DataBase Reference)
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Safety

HS Code 
2918999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
D368060
Product name
2,5-dimethoxybenzoylchloride
Packaging
50mg
Price
$130
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0019678
Product name
2,5-DIMETHOXYBENZOYL CHLORIDE
Purity
95.00%
Packaging
1G
Price
$794.58
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0019678
Product name
2,5-DIMETHOXYBENZOYL CHLORIDE
Purity
95.00%
Packaging
5G
Price
$1609.73
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0019678
Product name
2,5-DIMETHOXYBENZOYL CHLORIDE
Purity
95.00%
Packaging
10G
Price
$2576.19
Updated
2021/12/16
Alichem
Product number
17918148
Product name
2,5-Dimethoxybenzoylchloride
Packaging
500mg
Price
$823.15
Updated
2021/12/16
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2,5-DIMETHOXYBENZOYL CHLORIDE Chemical Properties,Usage,Production

Preparation

AlCl3 (4.0 g, 30 mmol) was suspended in dichloromethane (30 mL). To this mixture, a solution of 1,4- dimethoxybenzene (1.38 g, 10 mmol) and triphosgene (5.94 g, 20 mmol) in dichloromethane (30 mL) was added dropwise over a period of 30 min. The resulting mixture was stirred under reflux for 7 days. It was then poured into crushed ice/ water (50 mL) and stirred with pyridine (0.5 mL) at 0 ℃ for 10 min. The layers were separated and the aqueous phase was extracted with dichloromethane (2 ×20 mL). The combined organic layers were washed with ice-cold 0.5 m HCl (30 mL) and with ice-cold water (2×10 mL), and dried over sodium sulfate. The solvent was evaporated in vacuo and the residue was purified by chromatography on silica gel, eluting with hexane/ethyl acetate (4:1→3:1→2:1→1:1), to afford 1.23 g (60%) of 2,5-dimethoxybenzoyl chloride.

2,5-DIMETHOXYBENZOYL CHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,5-DIMETHOXYBENZOYL CHLORIDE Suppliers

Riedel-de Haen AG
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Matrix Scientific
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View Lastest Price from 2,5-DIMETHOXYBENZOYL CHLORIDE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd
Product
2,5-DIMETHOXYBENZOYL CHLORIDE 17918-14-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-11
Career Henan Chemical Co
Product
2,5-DIMETHOXYBENZOYL CHLORIDE 17918-14-8
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kgs
Release date
2020-01-29