ChemicalBook > CAS DataBase List > N-BENZYL-2-CYANOACETAMIDE

N-BENZYL-2-CYANOACETAMIDE

Product Name: N-BENZYL-2-CYANOACETAMIDE
CAS No.: 10412-93-8
Chemical Name: N-BENZYL-2-CYANOACETAMIDE
Synonyms: AKOS B028851;AURORA KA-4818;AKOS BBS-00006378;Agomelatine Impurity 33;Agomelatine Impurity 49;N-BENZYL-2-CYANOACETAMIDE;N-Benzyl-2-cyanoacetamide;Allisartan Isoproxil Impurity 25;2-cyano-N-(phenylmethyl)ethanamide;2-Cyano-N-(phenylMethyl)-acetaMide
CBNumber: CB1187711
Molecular Formula: C10H10N2O
Formula Weight: 174.2
MOL File: 10412-93-8.mol

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N-BENZYL-2-CYANOACETAMIDE Property

Melting point:: 120-122
Boiling point:: 425.2±38.0 °C(Predicted)
Density: 1.126±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 6.12±0.10(Predicted)
form: solid
Appearance: Off-white to light yellow Solid

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Safety

Hazard Codes: Xi
HazardClass: IRRITANT
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B124760
Product name: N-Benzyl-2-cyanoacetamide
Packaging: 250mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 037347
Product name: N-Benzyl-2-cyanoacetamide
Packaging: 500mg
Price: $95
Updated: 2021/12/16

AK Scientific

Product number: 7948AC
Product name: N-Benzyl-2-cyanoacetamide
Packaging: 1g
Price: $111
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB117043
Product name: N-Benzyl-2-cyanoacetamide
Packaging: 1g
Price: $128
Updated: 2021/12/16

Apolloscientific

Product number: OR14083
Product name: N-Benzyl-2-cyanoacetamide
Packaging: 5g
Price: $131
Updated: 2021/12/16

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N-BENZYL-2-CYANOACETAMIDE Chemical Properties,Usage,Production

Synthesis

105-56-6

100-46-9

10412-93-8

GENERAL METHOD: Dissolve sodium ethoxide (0.1 mmol) in ethanol (3 mL), add ethyl cyanoacetate (10 mmol) and benzylamine (10 mmol), and stir the reaction at room temperature. For primary amines, the reaction time was 1 hour; for secondary amines, the reaction time was extended to 2 hours. Upon completion of the reaction, the resulting precipitate was separated by filtration, washed with diethyl ether and recrystallized in ethanol, resulting in N-benzyl-2-cyanoacetamide as a white solid.

References

[1] Organic Letters, 2009, vol. 11, # 9, p. 2003 - 2006
[2] Chemical Communications, 2017, vol. 53, # 12, p. 2020 - 2023
[3] Organic Letters, 2014, vol. 16, # 7, p. 2018 - 2021
[4] Tetrahedron, 2011, vol. 67, # 8, p. 1540 - 1551
[5] Angewandte Chemie - International Edition, 2015, vol. 54, # 9, p. 2849 - 2853

N-BENZYL-2-CYANOACETAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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10412-93-8, N-BENZYL-2-CYANOACETAMIDERelated Search:

AURORA KA-4818

AKOS BBS-00006378

AKOS B028851

N-BENZYL-2-CYANOACETAMIDE

2-Cyano-N-(phenylMethyl)-acetaMide

2-cyano-N-(phenylmethyl)ethanamide

Acetamide, 2-cyano-N-(phenylmethyl)-

Agomelatine Impurity 49

Agomelatine Impurity 33

Allisartan Isoproxil Impurity 25

<i>N</i>-Benzyl-2-cyanoacetamide

10412-93-8