1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE
- Product Name
- 1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE
- CAS No.
- 32863-33-5
- Chemical Name
- 1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE
- Synonyms
- BUTTPARK 154\50-77;CHEMBRDG-BB 4003957;5-ForMylbenzofurazan;5-ForMyl-2,1,3-benzoxadiazole;2,1,3-Benzoadiazole-5-carbaldehyde;1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE;2,1,3-BENZOXADIAZOLE-5-CARBALDEHYDE;2,1,3-BENZOXADIAZOLE-5-CARBOXALDEHYDE;1,2,3-benzoxadiazole-5-carboxaldehyde;2,1,3-Benzoxadiazole-5-carboxaldehyde97%
- CBNumber
- CB1199541
- Molecular Formula
- C7H4N2O2
- Formula Weight
- 148.12
- MOL File
- 32863-33-5.mol
1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE Property
- Melting point:
- 58 °C
- Boiling point:
- 277.3±32.0 °C(Predicted)
- Density
- 1.417±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -1.68±0.36(Predicted)
- Appearance
- White to light yellow Solid
- CAS DataBase Reference
- 32863-33-5
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B335320
- Product name
- 2,1,3-Benzoxadiazole-5-carbaldehyde
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- Y8734
- Product name
- 2,1,3-Benzoxadiazole-5-carbaldehyde
- Packaging
- 250mg
- Price
- $148
- Updated
- 2021/12/16
- Product number
- 4H15-1-0M
- Product name
- 2,1,3-Benzoxadiazole-5-carboxaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $160
- Updated
- 2021/12/16
- Product number
- 4H15-1-0M
- Product name
- 2,1,3-Benzoxadiazole-5-carboxaldehyde
- Purity
- 97%
- Packaging
- 250mg
- Price
- $63
- Updated
- 2021/12/16
- Product number
- 040349
- Product name
- 2,1,3-Benzoxadiazole-5-carbaldehyde
- Packaging
- 500mg
- Price
- $189
- Updated
- 2021/12/16
1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE Chemical Properties,Usage,Production
Synthesis
19164-42-2
32863-33-5
Compound 15 (CAS: 19164-42-2, 10 g, 0.061 mol) was used as starting material and dissolved in dichloromethane (50 mL). A solution of triphenylphosphine (16 g, 0.061 mol) in dichloromethane (50 mL) was slowly added dropwise at 0 °C in an ice bath. After the dropwise addition was completed, the reaction mixture was continued to be stirred at 0 °C for 30 min. Upon completion of the reaction, the solvent was removed by rotary evaporator under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography using ethyl acetate/petroleum ether (1:20, v/v) as eluent. The target fraction was collected and concentrated to give benzo[c][1,2,5]oxadiazole-5-carbaldehyde (product 16, 6.3 g, 70% yield) as white needle-like crystals. The melting point is 55-56°C (literature values are consistent).
References
[1] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 4, p. 657 - 667
1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE manufacturers
- Product
- 1,2,3-BENZOXADIAZOLE-5-CARBALDEHYDE 32863-33-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-13