BENZYL 3-BROMOPROPYL ETHER

Product Name: BENZYL 3-BROMOPROPYL ETHER
CAS No.: 54314-84-0
Chemical Name: BENZYL 3-BROMOPROPYL ETHER
Synonyms: DK816;DKSI050;DKFELEX0213;Benzyl 3-bromopropyl;3-benzyloxybromopropane;Benzyl 3-bromoethyl ether;3-benzyloxy-1-broMopropane;1-bromo-3-benzyloxypropane;BENZYL 3-BROMOPROPYL ETHER;3-Benzyloxypropane bromide
CBNumber: CB1233500
Molecular Formula: C10H13BrO
Formula Weight: 229.11
MOL File: 54314-84-0.mol

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BENZYL 3-BROMOPROPYL ETHER Property

Boiling point:: 130-132 °C8 mm Hg(lit.)
Density: 1.298 g/mL at 25 °C(lit.)
refractive index: n20/D 1.531(lit.)
Flash point:: >230 °F
storage temp.: Inert atmosphere,Room Temperature
form: Liquid
color: Colorless
Water Solubility: Slightly soluble in water.
InChI: InChI=1S/C10H13BrO/c11-7-4-8-12-9-10-5-2-1-3-6-10/h1-3,5-6H,4,7-9H2
InChIKey: PSUXTZLDBVEZTD-UHFFFAOYSA-N
SMILES: C1(COCCCBr)=CC=CC=C1
CAS DataBase Reference: 54314-84-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
WGK Germany: 3
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 382043
Product name: Benzyl 3-bromopropyl ether
Purity: 98%
Packaging: 1g
Price: $34.65
Updated: 2025/07/31

Sigma-Aldrich

Product number: 382043
Product name: Benzyl 3-bromopropyl ether
Purity: 98%
Packaging: 10g
Price: $62.32
Updated: 2025/07/31

TCI Chemical

Product number: B2818
Product name: Benzyl 3-Bromopropyl Ether
Purity: >95.0%(GC)
Packaging: 5g
Price: $102
Updated: 2025/07/31

TCI Chemical

Product number: B2818
Product name: Benzyl 3-Bromopropyl Ether
Purity: >95.0%(GC)
Packaging: 25g
Price: $356
Updated: 2025/07/31

TRC

Product number: B267895
Product name: 1-Benzyloxy-3-bromopropane
Packaging: 25g
Price: $445
Updated: 2021/12/16

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BENZYL 3-BROMOPROPYL ETHER Chemical Properties,Usage,Production

Chemical Properties

Clear colorless to yellow liquid

Uses

Benzyl 3-bromopropyl ether may be used in the studies of preparation of (2S,3S)-1-[(triisopropylsilyl)oxy]-7-(benzyloxy)-2,3-(isopropylidenedioxy)-4(Z)-heptene, Ppeparation of 5-(3-Benzyloxypropoxy)psoralen (PAP-7), total synthesis of zincophorin and (+)-anatoxin-a.

General Description

Benzyl 3-bromopropyl ether is an ether.

Synthesis

4799-68-2

54314-84-0

GENERAL STEPS: To a dry reaction flask equipped with a magnetic stirrer under nitrogen protection, copper catalyst (2 mg, 0.002 mmol, 0.01 equiv), 3-benzyloxy-1-propanol (0.20 mmol, 1.0 equiv), carbon tetrabromide (131.6 mg, 0.4 mmol, 2.0 equiv) and sodium bromide (41 mg. 0.40 mmol, 2.0 equiv). The reaction vial was sealed and anhydrous DMF (1.5 mL) was added using a syringe. The reaction mixture was stirred under the light of a purple LED (394 nm) for 24 hours. Upon completion of the reaction, the mixture was transferred to a dispensing funnel and extracted by adding ether (10 mL) and water (10 mL). The organic phase was separated and the aqueous phase was further extracted with ether (2 x 10 mL). The organic phases were combined and washed sequentially with saturated aqueous NaHCO3 solution, Na2S2O3 solution and brine, dried with anhydrous Na2SO4 and concentrated under reduced pressure. Finally, the target product 3-benzyloxypropyl bromide was purified by silica gel column chromatography (100% hexane).

References

[1] Journal of the American Chemical Society, 2008, vol. 130, # 18, p. 6018 - 6024
[2] Beilstein Journal of Organic Chemistry, 2018, vol. 14, p. 2730 - 2736
[3] Patent: WO2008/157726, 2008, A1. Location in patent: Page/Page column 220
[4] Tetrahedron Letters, 2016, vol. 57, # 13, p. 1486 - 1488
[5] Journal of the American Chemical Society, 1982, vol. 104, # 4, p. 1054 - 1068

BENZYL 3-BROMOPROPYL ETHER Preparation Products And Raw materials

Raw materials

Preparation Products

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BENZYL 3-BROMOPROPYL ETHER Suppliers

Americas 1 Belgium 1 China 189 Europe 1 France 2 Germany 2 India 12 Japan 1 Switzerland 2 Ukraine 1 United Kingdom 10 United States 29 Global 251

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View Lastest Price from BENZYL 3-BROMOPROPYL ETHER manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: BENZYL 3-BROMOPROPYL ETHER 54314-84-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-12-09

Zhuozhou Wenxi import and Export Co., Ltd

Product: BENZYL 3-BROMOPROPYL ETHER 54314-84-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: BENZYL 3-BROMOPROPYL ETHER 54314-84-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1kg,5kg,100kg
Release date: 2019-07-04

54314-84-0, BENZYL 3-BROMOPROPYL ETHERRelated Search:

BENZYL 3-BROMOPROPYL ETHER 2,3,4,6-TETRA-O-BENZOYL-ALPHA-D-GLUCOPYRANOSYL BROMIDE 1-(((S)-2-(Bromomethyl)-3-methylbutoxy)methyl)benzene BENZOYL BROMIDE 2 3 5-TRI-O-BENZOYL-ALPHA-D-ARABINO-FURA BROMO 2,3,4-TRI-O-BENZOYL-L-FUCOPYRANOSE BENZYL 2,3-DIBROMOPROPANOATE C-(2,3,4,6-TETRA-O-BENZOYL-1-BROMO-1-DEOXY-BETA-D-GLUCOPYRANOSYL) FORMAMIDE 3-BENZYLOXY-1-BROMO-2-METHYLPROPANE 2,3,4,6-TETRA-O-BENZOYL-1-BROMO-1-DEOXY-BETA-D-GLUCOPYRANOSYL CYANIDE Methyl 2,3,4,-Tri-O-benzyl-6-bromo-6-deoxy-D-galactopyranoside 2,3,4-Tri-O-benzoyl-L-fucopyranosylbromide METHYL-2,3,4-TRI-O-BENZOYL-6-BROMO-6-DEOXY-ALPHA-D-GLUCOPYRANOSIDE 5,6-DIBROMO-2-(2,4-DICHLOROPHENYL)-1,3-DIOXEPANE 2,3,4,6-TETRA-O-BENZOYL-BETA-D-GLUCOPYRANOSYL BROMIDE 4-BROMO-2-(BROMOMETHYL)-5-(4-METHOXYPHENYL)-2-METHYLDIHYDROFURAN-3(2H)-ONE 2,3,4-TRI-O-BENZOYL-5-BROMO-A-D-GLUCURONIC ACID METHYL ESTER 4-(BENZOYLOXY)-2-[(BENZOYLOXY)METHYL]-6-BROMO-5-OXOTETRAHYDRO-2H-PYRAN-3-YL BENZOATE

BENZYL 3-BROMOPROPYL ETHER

3-(BENZYLOXY)PROPYL BROMIDE

(3-BROMOPROPOXYMETHYL)BENZENE

1-[(3-BROMOPROPOXY)METHYL]BENZENE

Benzyl 3-bromopropyl

1-bromo-3-benzyloxypropane

Benzyl 3-bromopropyl ether,98%

Benzyl 3-bromoethyl ether

[(3-bromopropoxy)methyl]benzene(SALTDATA: FREE)

[(3-Bromopropoxy)methyl]benzene 96%

3-benzyloxy-1-broMopropane

(3-Bromopropoxymethyl)benzene 3-(Benzyloxy)propyl Bromide

Benzyl (3-bromoprop-1-yl) ether

Benzyl 3-BroMopropyl Ether , 95.0%(GC)

Benzyl 3-bromopropyl ether 98%

Benzyl 3-Bromopropyl Ether &gt

Benzene, [(3-bromopropoxy)methyl]-

3-benzyloxybromopropane

DK816

DKFELEX0213

DKSI050

3-Benzyloxypropane bromide

54314-84-0

51314-84-0

C6H5CH2OCH23Br

Building Blocks

HALOGEN

Ethers

Organic Building Blocks

Oxygen Compounds

alkyl bromide

Phenyls & Phenyl-Het

Ethers

Organic Building Blocks

Oxygen Compounds